Separation of di- and tripeptides with solvent extraction and an emulsion liquid membrane

The extraction equilibria of various di- and tripeptides with di-2-ethylhexylphosphoric acid (D2EHPA) were studied at low pH values. The complex extracted to organic phase consisted of one molecule of peptide and two molecules of D2EHPA dimer. The extraction constants of the peptides correlated well with the distribution coefficients of peptides between 1-octanol and water, which is a measure of hydrophobicity. The permeation rates of peptides through an emulsion liquid membrane were examined by using D2EHPA as a carrier, Span 80 as an emulsifier and kerosene as a diluent. The rates varied considerably with peptide type, depending upon the hydrophobicity.     

中温低氰液体碳氮共渗及其应用效果

通过金相、硬度、耐磨性等测试分析表明，在“６０３”液体渗碳基础上研制出的新型中温低氰液体碳氮共渗剂对薄片件进行薄层碳氮共渗．能完全满足技术要求，并且取得了良好经济和社会效益．     

硼酸铝钕(NAB)晶体光学均匀性的测量

NAB晶体是一种综合性能较好的新型激光工作物质,有希望做成高效的小型固体激光器。本文介绍一种测量这种晶体光学均匀性的方法。 一般都采用在干涉仪上观测干涉图样来判定激光棒的光学均匀性。NAB晶体的吸收光谱曲线显示出其在可见光光谱区内有多个吸收峰。我们注意到:通常用做激光干涉仪光源的He-Ne激光器发射的632.8nm谱线正位于NAB晶体的一个吸收峰,并用输出约为45mW     

β—BBO晶体的电光性能

用干涉法测量了β－ＢＢＯ晶体的电光系数：γ２２＝２．６，γ３３＝０．２３，γ３１＝０．２５，γ５１＝－３．５×１０－１２ｍ／Ｖ。结果表明如果在Ｙ方向加电场，Ｚ方向通光，β—ＢＢＯ晶体可能制作成有应用价值的光开关。     

Sixty years of dislocations

It is well-known that with the appearance of three independent papers by Taylor, Polanyi and Orowan in the year 1934, the concept of crystal dislocations was born. Since then, dislocation theory has had many spectacular successes. It is quite appropriate therefore to be aware of the state of development of this exciting subject, sixty years after its discovery. A flavour for the vast subject of the applications of dislocation mechanisms to real materials is presented by choosing three examples, one each, drawn from metallurgy, physics and electronics. The topic of ‘Strength of metals and alloys’ is the first one, as this is also the author’s area of research. The phenomenon of solidification and crystal growth forms the next topic, especially in view of the seminal contributions made by A R Verma and his school from India. Dislocations play a useful role in the strengthening of solids, but how influential are they in affecting the performance of modern semiconductor devices? In the third example, the interesting and painstaking work done to settle this question is reviewed. Can we regard carbon fibre as thetransistor of dislocation theory? How shall we understand the long-established effects such as corrosion-fatigue, superplasticity and shape memory as well as the electrochemical and electro-mechanical properties of dislocations in semiconductor and non-metallic crystals? Answers to these questions belong to the realms of the future developments in dislocations. The talk is concluded with a discussion of these topics.     

Crystallization and Drying in Thin Sucrose Films During Panning

Sucrose crystallization in thin films (50–55 μm) was studied, using a videomicroscopy technique, at conditions encountered during hard panning processes. No nucleation occurred in unseeded films, while a linear increase in seeded crystals occurred during drying. Crystal growth rate increased with temperature (25–30°C) and with air velocity (2.4–12.5 m/sec), but did not change with varying sucrose concentrations (70–76% w/w) and relative humidities (0–66% at 30°C). FD & C Yellow No. 5 food coloring in the dye form (0.05–0.5 g/100 mL) showed no effects while similar concentrations in the lake form inhibited crystal growth rate.     

棉铃宝高效液相色谱分析方法研究

本法采用同一色谱条件反相高效液相色谱法测定棉铃宝中甲基对硫磷和辛硫磷的含量，方法简单易行，具有较高的精密度和准确度，其回收率分析为甲基对硫磷９９．５９％，辛硫磷１０１．０％。     

结晶器液面自动控制系统在唐钢板坯连铸机的应用

介绍了涡流法和同位素法2种结晶器钢水液面自动控制检测方式,及其在唐钢板坯连铸机的应用.     

Growth and optical property of zinc oxide thornballs

A new microstructure, thornball, of zinc oxide (ZnO) was synthesized by a very simple solid vapor deposition process under lead oxide (PbO) atmosphere. The microthornballs consist of numerous needles, which extend outwards in all directions symmetrically. They have dimensions of 120 μm in diameter, while the average diameter of the needles is about 100-200 nm. The needles on the balls grow along the 〈0 0 0 1〉 orientation and have gradient compositions along radial. Control experiments proved that PbO played an important role in the growth. Additionally, photoluminescence property was observed and provided the evidence that PbO did not deteriorate the optical properties of ZnO thornballs. This kind of microstructures has potential applications in the field of photochemical catalysis.     

高频脉冲电铸Ni-Co纳米复合块体微观结构分析

采用高频脉冲电铸工艺制备出了镍钴纳米复合块体材料，利用场发射扫描电镜、能谱和X射线衍射的方法，重点研究了复合块体沉积层的表面形貌、相结构和结晶取向。结果表明．高频率和润湿剂的添加对沉积层的细化有重要影响，高频脉冲电铸能够获得微观组织致密、均匀的复合块体材料。