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81.
Graft copolymers of sodium alginate (NaAlg) with N‐vinyl‐2‐pyrrolidone were prepared using azobisisobutyronitrile as initiator. The graft copolymers (NaAlg‐g‐PVP) were characterized with Fourier transform infrared spectroscopy, elemental analysis, and differential scanning calorimetry. Polymeric hydrogel beads of NaAlg and NaAlg‐g‐PVP were prepared by crosslinking method using glutaraldehyde (GA) as a crosslinker in the hydrochloric acid catalyst (HCl) and these beads were used to deliver anti‐inflammatory drug, indomethacin (IM). Chemical stability of the IM after encapsulation into beads was confirmed by FTIR. Preparation conditions of the NaAlg‐g‐PVP beads were optimized by considering the percentage entrapment efficiency, particle size, swelling capacity and their release data. In vitro release studies were performed in simulated gastric fluid (pH 1.2) for the initial 2 h, followed by simulated intestinal fluid (pH 7.4) for 4 h. Effects of GA concentration, exposure time to GA, drug/polymer (d/p) ratio, and concentration of HCl on the release of IM were discussed. It was observed that IM release from the beads decreased with increasing GA concentration and exposure time. IM release also decreases with increasing d/p ratio and HCl concentration. The highest IM release was obtained to be 77% for beads crosslinked with 0.027M GA. Swelling experiments were also performed to compute molecular mass between crosslinks of the beads. © 2008 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
82.
Crystal phase transition between the low- and high-temperature phases has been investigated for ethylene (E)-tetrafluoroethylene (TFE) alternating copolymer (ETFE) containing the third monomeric species by the temperature dependent measurements of wide-angle X-ray diffraction (WAXD) and small-angle X-ray scattering (SAXS) and differential scanning calorimetry. Nonafluoro-1-hexene (NFH) and hexafluoropropylene (HFP) were chosen as the third monomers, where they are different in the side-branch length, -(CF2)3CF3 and -CF3, respectively. In the case of E/TFE/NFH copolymer (ET-C4F9), the crystal phase transition temperature of the original ETFE two-components copolymer was not very much affected by the existence of NFH in the range of NFH content from 0.7 to 3 mol%. Contrarily, the crystal phase transition temperature of E/TFE/HFP copolymer (ET-CF3) was found to decrease drastically with increasing HFP content. The melting temperature and the higher-order structure were also affected sensitively depending on the HFP content. This difference in phase transition behavior between ET-C4F9 and ET-CF3 copolymers is reasonably interpreted as follows: the short side groups (-CF3) of HFP monomeric unit are included in the crystal lattice of E/TFE chains and the unit cell is expanded gradually with an increment of the HFP content, resulting in the decrease in phase transition point because of easier thermal motion of the chains. On the other hand, the long side groups [-(CF2)3CF3] of NFH monomeric units are excluded out of the crystal lattice and located on the lamellar surfaces or in the amorphous region and do not affect very much the phase transition temperature even when the NFH content is increased. In association with such a change in crystal structure, the long period of stacked lamellar structure was found to decrease remarkably in the case of NFH, whereas it does not change very much for HFP, consistent with the interpretation of the above-mentioned WAXD data. 相似文献
83.
通过对锯切装置的改进,提高了锯切性能,降低了锯条成本,保证了锯切质量,使设备更加高效、安全的工作。 相似文献
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86.
给出了感应电机内部物理过程的框图描述。这种描述准确地反映了电机学中主、漏磁路分别处理的一般方法,感应电机内部各物理量之间的数量关系和电机学所基于的若干基本电磁定律,感应电机内部物理量之间的关系。 相似文献
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ROI-based Watermarking Scheme for JPEG 2000 总被引:1,自引:0,他引:1
Yu-Cheng Fan Arvin Chiang Jan-Hung Shen 《Circuits, Systems, and Signal Processing》2008,27(5):763-774
A new region of interest (ROI)-based watermarking method for JPEG 2000 is presented. The watermark is embedded into the host
image based on the characteristics of the ROI to protect rights to the images. This scheme integrates the watermarking process
with JPEG 2000 compression procedures. Experimental results have demonstrated that the proposed watermark technique successfully
survives JPEG 2000 compression, progressive transmission, and principal attacks. 相似文献
89.
90.
报道以甲基丙烯酸羟乙酯与甲基丙烯酸甲酯的共聚物为载体膜材料,研制成非酶标记的T4免疫传感器,并对载体膜材料的共聚方法及共聚物共聚比与传感器灵敏度的关系进行了探讨。 相似文献