The axial and radial distributions of solid and gas holdups were investigated in an air‐water‐glass bead circulating fluidized bed (GLSCFB) using a new ultrasonic technique, with a new method based on signal fluctuations. The cross‐sectional averaged gas and solid holdups measured at two axial positions appear to be similar at all studied operating conditions. The radial non‐uniformity decreases with increasing liquid velocity but does not change with an increasing solid circulating rate. The radial distribution of gas holdup was more uniform for 1.3 mm beads than for 433 µm glass beads. 相似文献
A method of measurement of solids holdup in a three-phase reactor by analyzing the shape and the phase lag or lead of an ultrasonic wave has been proposed. The solids holdup in a solids-dilute three-phase fluidized bed could be measured without being affected by the presence of gas bubbles. The experimental values of solids axial dispersivity measured by the ultrasonic technique are in reasonable agreement with an empirical correlation of previous data obtained by other methods. The possibility of the application of the ultrasonic technique to the measurement of solids holdup in a three-phase fluidized bed has been suggested. 相似文献
Summary: A new technique, ultrasonically initiated in situ emulsion polymerization, was employed to prepare intercalated polystyrene/Na+‐MMT nanocomposites. FTIR, XRD, and TEM results confirm that the hydrophobic PS can easily intercalate into the galleries of hydrophilic montmorillonite via ultrasonically initiated in situ emulsion polymerization, taking advantages of the multi‐effects of ultrasonic irradiation, such as dispersion, pulverization, activation, and initiation. Properly reducing SDS concentration is beneficial to widen the d‐spacing between clay layers. However, the Na+‐MMT amount has little effect on the d‐spacing of nanocomposites. The glass transition temperature of nanocomposites increased as the percentage of clay increased, although the average molecular weight of PS decreased, and the decomposition temperature of the 1obtained nanocomposites moves to higher temperature.
TEM of PS/Na+‐MMT nanocomposite prepared by ultrasonically initiated in situ emulsion polymerization. 相似文献
The ultrasonic velocity and density measurements of europium soaps in a mixture of benzene and methanol (3:2, vol/vol) were
used to evaluate various acoustic parameters and molar volume and to determine the critical micelle concentration. The results
showed that the ultrasonic velocity, specific acoustic impedance, molar sound velocity, and molar compressibility increase,
and intermolecular free length, adiabatic Compressibility, and relative association decrease with increasing concentration
and chainlength of the soap. The results were interpreted in terms of soap-solvent interaction. 相似文献