提高Cr12MoV钢冷作模具寿命的措施

从原材料改锻、预备热处理、淬火及回火、深冷处理、表面强化处理等方面分析介绍了提高Cr12MoV钢冷作模具寿命的一些方法和措施 ,并通过实例表明 ,采用这些方法和措施可较大幅度地提高模具寿命     

关于输气管线内衬聚乙烯管可防止其腐蚀的商榷

本文参照德国一实例，即利用多种类型PE衬层，在一定温差及有气体扩散阻挡层和无气体扩散阻挡层的条件下，详细地叙述了高压酸性气体对其进行长期渗透作用的试验。结果显示：水蒸气和腐蚀性气体（如H2S）的渗透作用是不能忽视的，甚至当PE层为5mm时亦有一定渗透性；此外，在衬层底部尚产生了化学腐蚀作用，从而促使人们必须考虑须正确选择PE下边的防腐底层。     

低碳马氏体强化工艺的应用

低碳钢及低碳合金钢的淬火马氏体具有良好的综合力学性能。本文简述了08F，Q235-A，20，20Cr，高强度螺栓用钢ML15，25CrMnSiA和ZG28SMnVCu钢的低碳马氏体强化工艺及其应用。     

冠脉造影图像血管增强及减影的优化方法

针对于传统X射线冠状动脉造影序列图像的血管的减影包含严重伪影以及减影结果不完整等问题,提出了冠脉造影图像血管增强以及减影优化的方法。基于冠脉造影序列图像的时空特性,将相同时相的图像匹配进行减影,得到初步减影结果。针对初步减影部分缺失,对有导管遮挡没有被识别的单根血管进行二次增强处理。增强方法为:运用区域生长确定被导管遮挡的血管部分,以此部分为基础按规定模板扩展,形成覆盖导管区域,区分血管和导管,改变两部分的灰度值,增大对比度。最后采用灰度线性变换、中值滤波等步骤,得到优化的冠脉血管减影。实验表明,本减影及优化方法可以从冠脉造影序列图中提取较为完整清晰的冠脉血管并且具有很好的可控性和鲁棒性。     

Importance of Low-Temperature Melt-Mixing on the Construction of Stereocomplex Crystallites with Superior Nucleation Efficiency in Asymmetric Poly(l-lactide)/Poly(d-lactide) Blends

The nucleation efficiency (NE) of stereocomplex crystallites (SCs) formed in asymmetric poly(L-lactide)/poly(D-lactide) (PLLA/PDLA) blends is generally unsatisfactory because the competition between stereocomplexation and chain mixing involved in the melt-mixing process can cause low formation efficiency and even severe aggregation of SCs. Herein, it is attempted to achieve high-efficient formation of finely dispersed SCs particles by designing a unique melt-mixing procedure, where the mixing of PLLA with 0.75 wt% PDLA is first performed at elevated temperatures (far above the melting temperature of SCs) to allow the homogeneous mixing of PLLA/PDLA chains and then at a low temperature (slightly above that of homocrystallites) to permit the full stereocomplexation of the premixed chains. It is found that the SCs formed in the blends exhibit unexpectedly low NEs (e.g., 54.5%), much inferior to that (73.6%) in the counterpart without undergoing premixing. This is because the introduction of premixing leads to a remarkable deterioration in the amount of SCs particles formed, despite decreased particle size, highlighting that the direct mixing at low temperatures of 170–180 °C (about 20–30 °C lower than that used in common melt-processing of PLA) is more effective for the construction of SCs with superior NE. The mechanisms for these striking findings are discussed.     

A Dual Physical Cross-Linking Strategy to Construct Tough Hydrogels with High Strength,Excellent Fatigue Resistance,and Stretching-Induced Strengthening Effect

Hydrogels with excellent stiffness, toughness, anti-fatigue, and self-recovery properties are regarded as promising water-containing materials. In this work, a dual physically cross-linked (DPC) sodium alginate (SA)/poly[acrylamide (AAm)-acrylic acid (AAc)-octadecyl methacrylate (OMA)]-Fe³⁺ hydrogel is reported, which is constructed by hydrophobic association (HA) and ionic coordination (IC). The optimal DPC hydrogel demonstrates excellent mechanical performance: tensile modulus of 0.65 MPa, tensile strength of 3.31 MPa, elongation at break of 1547%, and toughness of 27.8 MJ m^–3. SA/P(AAm-AAc-OMA)-Fe³⁺ DPC hydrogels also exhibit prominent anti-fatigue and self-recovery performance (99.1–109.7% modulus recovery and 90.4–108.9% dissipated energy recovery after resting for 5 min without additional stimuli at ambient temperature) through the reconstruction of reversible physical cross-linking. Some of the SA/P(AAm-AAc-OMA)-Fe³⁺ DPC hydrogels even exhibit a stretching-induced strengthening effect, which is similar to the performance of muscle—“the more training, the more strength.” Hence, the combination of HA and IC will provide an effective approach to design DPC hydrogels with desirable mechanical performances and a longer service life for wider applications of soft materials.     

原材料对水泥砂浆性能的影响研究

水泥和砂的质量、引气剂的种类均会对水泥砂浆性能产生影响,其中水泥中高吸附性材料对制备的砂浆工作性能影响较大,需严格加以控制。不同引气剂的起泡、稳泡能力和气泡尺寸不同,对砂浆的稠度、分层度和强度会造成不同影响,采用摇泡试验可快速甑选出合适的引气剂。另外,砂的细度模数,甚至洁净程度（泥灰含量）和堆积密度也会对砂浆性能产生较大影响,在控制水泥的砂浆性能时,应验证并确保重新配制试验用砂的稳定性。     

水质稳定剂HPDP缓蚀阻垢性能评定

用静态阻垢，旋转挂片失得法实验研究了ＨＰＤＰ对ＣａＣＯ３，Ｃａ３（ＰＯ４）２等的阻垢性能以及对Ｑ２３５碳钢的缓蚀性能等。试验证明，ＨＰＤＰ是一种优良的阻垢缓蚀剂，适用于高温，高碱，高ＰＨ，高浓缩倍数的循环冷却水处理，具有广阔的应用前景。     

机械活化-湿化学合成LiMn2O4的组成、结构与表征

以MnO2和LiOH·H2O为原料,采用机械活化与湿化学集成的方法,在水溶液中直接合成了结晶态的尖晶石锂锰氧化物.当锂含量介于3.78%～4.35%之间时,所得锂锰氧化物为纳米级球形粉末,以尖晶石结构为主,含极少量的Mn3O4杂相;在300～800℃温度范围内热处理后,Mn3O4杂相消失,尖晶石结构更趋完善.所合成的含锂5.80%的高锂样品则以LiMnO2层状结构为主,含少量Mn3O4杂相,其SEM形貌为片状;在300～700℃下热处理8 h后,层状LiMnO2转变成尖晶石LiMn2O4,Mn3O4杂相峰明显减弱并随热处理温度的升高而消失;当温度升高至700～800℃时,开始出现缺锂的Li1-xMn2O4相.结果表明:该法制备锂锰氧化物可实现锂、锰、氧在原子级水平的均匀混合,所得产物的热稳定性能良好,其化学计量组成与结构易于调整和控制.     

硬质合金冷挤压凹模的热处理强化

本文叙述了ＷＣ－Ｃｏ硬质合金特别是ＹＧ２５牌号硬质合金的渗硼淬火热处理强化工艺和不同钴含量的合金的强化处理效果以及强化处理的合金应用效果，并对其强化机理进行了讨论。