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11.
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The bonding of β'-Al2O3 and pyrex glass to Al matrix composites by anodic bonding process is achieved. The microstructure of the bonded interface and the joining mechanisms are analyzed with scanning electron microscope (SEM), energy dispersive X-ray fluorescence spectrometer (EDX). It is observed that the bonding region across the interface consists of the metal layer, oxide transitional layer and the ceramic layer, with the transitional layer composed of surface region and sub-surface region. The bonding process can mainly be categorized into anodic bonding process and solid state diffusing process. The pile-up of the ions and its drift in the interface area are the main reasons for anode oxidation and joining of the interface. The temperature, voltage and the drift ions in the ceramic or glass during the bonding process are the essential conditions to solid state diffusing and oxide bonding at the interface. The voltages, temperature, pressure as well as the surface state are the main factors that influence the anodic bonding. 相似文献
13.
Wang Xuegang Yan Fengjie Yan Qian Li Xingeng 《Frontiers of Materials Science in China》2007,1(2):225-227
An iron-based amorphous foil (FeNiCrSiB) was used as an interlayer for the amorphous diffusion bonding of low carbon steel
pipes under argon flux. The microstructure and mechanical properties of the joint were analyzed using an electron probe micro-analyzer
(EPMA), tensile test, bending test and impact test. The results show that the joint microstructure resembles that of the base
metal and no precipitates form at the joint. Melting point depressants (B, Si) diffuse far away from the joint and the base
metal element is homogenous across the joint. The joint impact toughness is greater than the base metal toughness and the
mechanical properties of the joint are similar around the pipe. 相似文献
14.
采用全因素试验法,对马尾松木材进行过热乙醇溶液脱脂处理,以获取马尾松木材高效脱脂工艺技术。试验结果显示:(1)脱脂温度对马尾松松脂溶出量的影响极显著,且溶出量随着脱脂温度的升高而增大;(2)脱脂时间对马尾松松脂溶出量的影响极显著,且溶出量随着脱脂时间的延长呈先增大后减小的趋势;(3)脱脂浴比对马尾松松脂溶出量的影响极显著,且溶出量随着脱脂浴比的延长呈先增大后减小的趋势;(4)利用过热乙醇溶液对马尾松木材进行脱脂,其最佳工艺是脱脂时间为130℃、脱脂时间为8h、浴比1:8。 相似文献
15.
The structural properties and hydrogen bonding of undoped and phosphorous doped polycrystalline silicon produced by step-by-step laser dehydrogenation and crystallization technique were investigated using Raman spectroscopy and hydrogen effusion measurements. At low laser fluences, EL, a two-layer system is created. This is accompanied by the change in hydrogen bonding. The intensity of the Si–H vibration mode at 2000 decreases faster than the one at 2100 cm−1. This is even more pronounced in phosphorous-doped specimens. The laser crystallization results in an increase of the hydrogen binding energy by approximately 0.2–0.3 eV compared to the amorphous starting materials. 相似文献
16.
This study describes a laboratory method for the estimation of emission from preservative-treated wood in the different situations where emissions could enter the environment for use classes 3 (not in contact with ground) and 4 and 5 (in contact with the ground, fresh water or sea water) according to OECD Guidelines. Samples of scotch pine sapwood (Pinus sylvestris L.) were treated with CCA (1% and 2%), ACQ-1900 (3% and 7%), ACQ-2200 (2%), Tanalith E 3491 (2% and 2.8%), and Wolmanit CX-8 (2%). 相似文献
17.
18.
通过对国内外大量石油套管螺纹参数的测量和全尺寸的模拟试验,以及对测量和试验数据的理论分析,找出了影响国产套管发生粘扣的原因,并在实际生产中实施验证。采取相应的措施改善了套管的抗粘结性能,同时套管的密封和抗滑脱性能并未下降。 相似文献
19.
We succeeded in the fabrication of bonded laser crystals composed of a neodymium-doped YVO4 laser crystal (Nd:YVO4) and its host crystals YVO4 by a newly developed dry etching technique using an argon ion beam. The optical distortion caused by the bonded interface of size 5 mm × 6 mm was estimated to be 0.05λ at 633 nm. From the comparison of laser performance pumped by a laser diode, the bonded crystals could increase the laser output power by nearly twice that of the non-bonded crystals with the same degree of polarization of 99.2%. To analyze the mechanism of the enhanced reduction of the thermal load in the bonded crystals, numerical simulations with a finite-element method were also performed. 相似文献
20.
通过正交试验研究了各工艺量数以钢/铝合金液固相复合性能的影响,最佳工艺条件为铝合金液体温度790℃,钢板表面处理为酸洗+钢刷+5%的氟钛酸钾助焊剂,复合压力为39.2MPa,组织观察表面界面脆性化合物的形成是导致结合强度降低的一个重要因素。 相似文献