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51.
泥浆制备中工艺改造的研究 总被引:1,自引:0,他引:1
根据室条件下粉磨试验结果,发现球磨过程中筛上料变化存在的突变范围,提出两次加料一次加水可改变泥浆颗粒分布,并找出适宜的加料种类与时间。另外给予测粒度分布提供了宝贵的试验基础数据。 相似文献
52.
采用复合靶及离子微波控制共溅射方法制备了银(Ag)硅(Si)复合物薄膜。透射电观察表明,银晶体小颗粒(1-3nm)镶嵌于非晶基体中。近紫外、可见光及近红外吸收光谱分析表明,当银含量低于50at%时,薄膜显示典型非晶半导体光谱特征;当银含量高于50at%时,在近紫外及可见波段显示两个吸收峰,讨论了其可能的吸收机制 相似文献
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A new method for analysis of trace mercury in water samples was developed, based on the combination of preconcentration/separation using dithizone-modified nanometer titanium dioxide (TiO2) as a solid phase extractant and determination by cold vapor atomic adsorption spectrometry (CVAAS). Dithizone was dissolved with alcohol and loaded on the surface of nano-sized TiO2 powders by stirring. The static adsorption behavior of Hg2 on the dithizone-modified nanoparticles was investigated in detail. It was found that excellent adsorption ratio for Hg2 could be obtained in the pH range of 7-8 with an oscillation time of 15 min, and a 5 mL of 3.5 mol·L-1 HCl solution could quantitatively elute Hg2 from nanometer TiO2 powder. Common coexisting ions caused no obvious influence on the determination of mercury. The mechanisms for the adsorption and desorption were discussed. The detection limit (3σ) for Hg2 was calculated to be 5 ng·L-1. The proposed method was applied to the determination of Hg2 in a mineral water sample and a Zhujiang River water sample. By the standard addition method, the average recoveries were found to be 94.4%-108.3% with RSD (n = 5) of 2.9%-3.5%. 相似文献
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用图象分析仪测定聚烯烃中云母聚集体数均粒径的结果表明,乙烯等离子体处理云母提高其在聚烯烃中的分散性;强化处理条件有利于云母在LDPE中分散,而对HDPE则不然;云母在PS中的分散性优于在HDPE和LDPE中。 相似文献
59.
Observation and Analysis of Gypsum Particleboard using SEM 总被引:2,自引:0,他引:2
冯谦 《武汉理工大学学报(材料科学英文版)》2007,22(1):44-47
The microstructures of gypsum board and gypsum particleboard were observed by SEM. The effects of retarder and waterproof agent on the shape and the average dimension of the gypsum crystal were discussed. The mechanism was investigated as well. Four typical instances, i e, the gypsum crystal shape, the gypsum combined with particles on the particles surface, the gypsum combined with particles on the wood cross section and the gypsum combined with particles inside the wood cell cavity were selected and observed. Furthermore, the agglomeration and cementation mechanism between gypsum and particle were studied. 相似文献
60.
Composite coatings made of nano-Y203/cobalt-based alloy and produced by crosscurrent CO2 laser on Ni-based superalloy are introduced. Cross-section or surface of the coatings was examined to reveal their microstructure using optical microscope, SEM, including EDS microanalysis, TEM and XRD. The results show that some equilibrium or non-equilibrium phases, such as γ-C0, Cr23C6, Y203 and ε-Co exist in the coatings. Fine and short dendritic microstructure andcolumnar to equiaxed transition (CET) occurred by adding nano-Y203 particles. With the increasing amount of nano-Y203(1%, mass fraction), fully equiaxed crystallization appeared. These are caused by nano-Y203 particles acting as new nucleation site and rapid solidification of the melt. The results also show that inhomogeneous dispersion of nano-Y203 resultsin the formation of ε-Co phase in the coatings. The sub-microstructure of the clad is stacking fault. The mechanism of theformation of equiaxed grains is also analyzed. 相似文献