提高Cr12MoV钢冷作模具寿命的措施

从原材料改锻、预备热处理、淬火及回火、深冷处理、表面强化处理等方面分析介绍了提高Cr12MoV钢冷作模具寿命的一些方法和措施 ,并通过实例表明 ,采用这些方法和措施可较大幅度地提高模具寿命     

模具钢深冷处理的应用研究

研究了Cr12MoV钢拉深凸模经不同工艺热处理后的性能变化。结果表明，深冷处理是提高模具寿命的可靠途径。     

3Cr2W8V钢强韧化处理研究

本文从强韧化机制方面，研究了用于铝合金型材挤压模具的３Ｃｒ２Ｗ８Ｖ钢在不同热处理工艺条件下的金相组织，显微结构与断口，常温与高温下的力学性能。结果表明，采用１２５０℃以上超高温淬火加４００－５００℃中温回火的强韧化处理工艺，可使该钢同时获得具有良好力学性能和较好韧性、热强性、热稳定性、热疲劳性、耐磨性等相结合的综合性能。     

光催化TiO2涂层在金属防腐蚀中的应用研究现状

介绍了TiO2的特点、应用概况及金属光催化防腐蚀作业的原理，对光催化TiO2涂层在金属防腐蚀方面的应用研究进展进行了综述。指出了TiO2薄膜在这一领域应用中的优势及存在的问题。     

Reaction process of monazite and bastnaesite mixed rare earth minerals calcined by CaO-NaCl-CaCl2

The decomposition reactions of monazite and bastnaesite mixed rare earth minerals calcined by CaO-NaCl-CaCl2 were studied by means of TG-DTA and XRD. The results show that the process of the minerals decomposed by CaO involves two steps. The first step occurs in the temperature range of 425-540 ℃, and the main reactions are bastnaesite decomposition, i.e. REOF reacts with CaO to produce RE2O3 and CaF2, and Ce2O3 is oxidized to CeO2. During this step, CaCO3 is formed at about 500 ℃. The second step takes place in the temperature range of 610-700 ℃, and the reactions are monazite decomposition into RE2O3, Ca5F（PO4）3 and Ca3（PO4）2 by CaO and CaF2. In this process, the decomposition ability is improved because CaO from CaCO3 decomposing has high chemical activity. In calcining process, the new formed Ca5F（PO4）3 restrains fluorine that can escape in form of gaseous compound. The decomposition ratio of the mixed rare earth minerals reaches 90.8% at 700 ℃.     

硅溶胶型壳的制壳工艺参数--对硅溶胶型壳的几点认识之二

硅溶胶型壳的面层和背层对硅溶胶和耐火粉料的要求是不一样的。分析了硅溶胶胶粒直径和分布、锆英粉中(ZrHf)O2和Fe2O3的含量、耐火粉料的粒度等对型壳质量的影响：面层和背层制壳对干燥室的温度、湿度、风速有不同的要求，应分别制订不同的工艺规范。     

P2P网络中的匿名电子拍卖协议研究*

在P2P网络中实现电子拍卖的功能对于P2P技术具有重要意义,这将意味着电子商务同样可以在P2P网络中广泛应用.然而,匿名性、投标价保密性、抗勾结性等安全问题一直是电子拍卖研究的难点问题,一种合理的解决方法是将盲签名、知识证明、可验证的数字签名加密算法引入到电子拍卖协议中.这样不仅可以很好地解决P2P网络无中心服务器的不足,还使得系统的安全性能得到显著提高.     

Coordinated Recovery of Middleware Services:A Framework and Experiments

Being the most popular runtime infrastructure for distributed systems, middleware can be viewed as a collection of common services. Since the development, deployment and maintenance of distributed systems rely largely on middleware services, the failure of middleware services puts a significant impact on the reliability and availability of the whole system. Though recovery-based fault tolerance is an effective way to improve the reliability of middleware services, it is far away from practice mainly because of the high complexity and cost of the recovery of correlated failures between interdependent services. In this paper,a framework for detecting and recovering the correlated failures of middleware services in an automated way is presented. First, the problem is investigated from two perspectives, i.e.,analyzing the role and impact of middleware services and illustrating a set of correlated failures in J2EE standard services as motivating examples. Then, a general coordinated recovery model is constructed with the elements necessary and su±cient for detecting and recovering correlated failures in middleware services. The supporting framework is demonstrated on three J2EE application servers, i.e., PKUAS, JBoss and JOnAS, one by one without fundamental modifications. Finally, based on the three enhanced application servers, many cases on J2EE common services, including the transaction service, database service, naming and directory service, security service and messaging service, are studied. The experiment results show the effectiveness and applicability of the framework presented in this paper.     

超临界CO2对钢材的腐蚀实验研究

采用静态高温高压釜及SEM现代分析测试手段,在分析超临界CO2存在形式及与原油、水交互作用的基础上,进行了超临界CO2对钢材的腐蚀实验研究。结果表明,在腐蚀系统SCF-CO2气相中,存在CO2腐蚀现象;液相中,腐蚀速率随压力增加而上升,12MPa达到峰值后下降。在纯水中12MPa时,液相和气相中的腐蚀速率趋于一致,腐蚀形貌表现为腐蚀瘤。30％的原油含量可在液相促进钢材腐蚀。腐蚀形貌表现为腐蚀瘤与腐蚀坑并存;但随含油量增加,会抑制钢材腐蚀。     

锐钛型介孔纳米二氧化钛粉体的制备与表征

采用沉淀法,以水溶液为反应体系,无机物（硫酸氧钛和氢氧化钠）为主要原料,加入少量模板剂,制备出锐钛型介孔纳米二氧化钛粉体。通过正交实验分析优选出最佳工艺。采用比表面仪、原子力显微镜（AFM）、高分辨场发射透射电镜等仪器对产品的结构进行了表征,得到了具有较高热稳定性,比表面积为121 m2·g-1,晶粒尺寸为12 nm,介孔平均孔径为10 nm,粉体粒径＜100 nm等特征的锐钛型介孔纳米二氧化钛粉体。