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111.
Véronique Baroghel-Bouny Patrick Belin Matthias Maultzsch Dominique Henry 《Materials and Structures》2007,40(8):759-781
Within the framework of the evaluation and the prediction of chloride-induced corrosion risks, simple and rapid AgNO3 spray tests can be proposed for various issues. This paper forms the first part of a series. In this first part, the Maultzsch
procedure (spraying of 0.1-N AgNO3 solution + K2CrO4) as well as the procedure based on the use of a sole AgNO3 solution have been investigated on a broad range of concretes. These procedures have also been compared to the Collepardi
procedure (spraying of 0.1-N AgNO3 + fluoresceine). The feasibility of these colorimetric techniques on saturated specimens cast in laboratory, after non-steady-state
diffusion tests carried out in various conditions, is discussed. In addition, the results obtained from applying such spray
tests in field conditions on cores drilled out from various RC test specimens exposed to a marine environment (tidal zone)
and to a road and cold environment (freezing-thawing cycles and spraying of deicing salts) are presented. Colorimetric methods
have in particular been applied here to the assessment of the average chloride penetration depth and of its evolution versus
time (kinetics). Moreover, the detection threshold of these techniques has been investigated in various environments. The
possible sources of discrepancy on the results have been analysed. 相似文献
112.
Fresh niobium hydroxide was first precipitated from NbF5 solution using an aqueous ammonium hydroxide under basic conditions. Then a simple procedure of mixing lithium and niobium hydroxides together and heating at a low temperature (400 °C) produced pure ultrafine single phase LiNbO3 (LN). In the literature, this is the lowest temperature so far reported on the formation of LN. The phase content and lattice parameters are determined by X-ray diffraction (XRD). The average particle size and morphology were studied by transmission electron microscopy (TEM). 相似文献
113.
化学成分和固溶温度对1Cr17Mn9Ni4N不锈钢组织和性能的影响 总被引:3,自引:1,他引:2
为提高1Crl7Mn9Ni4N钢固溶处理后的力学性能(特别是钢的强度),研究了化学成分及固溶处理温度对其组织和性能的影响。结果表明,1000—1125℃固溶处理后,该钢的组织为单相奥氏体。在标准成分范围内,随着镍、锰含量的增加,该钢的强度降低,塑性有所改善。氮明显提高该钢的强度。根据试验结果,每增加0.01%的氮钢的室温强度可提高大约5MPa,且塑性基本上不受影响。当合金成分(质量分数,%)控制在C0.08—0.12、Crl6.5—17.5、Ni3.5—4.2、Mn8.0—9.0、N0.22—0.28时,1Crl7Mn9Ni4N钢经1050—1100℃固溶处理后强度较高、塑性好,室温强度σ0.2和σb可分别达到400MPa和800MPa。 相似文献
114.
115.
Effects of austenitizing treatment temperatures on aqueous corrosion properties of martensitic stainless steels were investigated by electrochemical tests (potentiodynamic test, potentiostatic test and electrochemical impedance spectroscopy), and surface analyses (optical microscopy and XRD). The results of potentiodynamic test revealed that the breakdown potential increased with the increased austenitizing temperature, indicating increased relative resistance to initiation of localized corrosion. EIS measurements showed that MSS3 (1030 °C) exhibits larger polarization resistance value than MSS1 (970 °C) and MSS2 (1000 °C) at passive and breakdown states. This was caused by decreasing the amount of Cr-rich M23C6 carbide which acts as preferential sites for pitting corrosion. 相似文献
116.
Two-phase (B2+L12) nickel aluminide intermetallic compounds were synthesized by the pressure-assisted volume combustion synthesis (CS). The production and characterization of the samples containing NiAl+Ni3Al were investigated. Aluminum (99% pure, 15 μm) and carbonyl nickel (99.8 pure, 4-7 μm) powders were used. The production of intermetallic compound was carried out at 1050 °C under 150 MPa uniaxial pressure in open air atmosphere in an electrical resistance furnace for 60 min. The formation temperature of intermetallic compound was determined by differential scanning calorimeter (DSC) analysis, and exothermic temperature of powder mixture was determined as 653 °C. The characterization of samples was confirmed by optical microscope, SEM and XRD analysis. It was observed that the structure of compound has very low porosity and the formation of NiAl was completed successfully. The relative density of test materials measured according to Archimedes’ principle was 98.04%. The microhardness of test materials was about 351 HVN1. 相似文献
117.
采用SE 3 0为固定液进行色谱柱分离 ,用外标定量法测定泥土中的微量六氯环戊二烯 ,结果最小检知量为 0 .18× 10 - 6 ,相关系数为 0 .99992。 相似文献
118.
119.
巴彦浩特探区钻井液技术初探 总被引:1,自引:1,他引:0
巴彦浩特探区钻井液工艺技术的重点是,解决疏松砂砾岩地层水涌漏同层、侏罗系地层水的HCO3^-污染及可能出现的火成岩地层井塌复杂。结合内蒙古巴彦浩特探区地层和井身结构特点,采用了两性聚合物/氯化钾钻井液和氯化钾/石膏-聚磺钻井液体系。该体系抑制能力强,性能稳定.容易实现低固相、低密度近平衡钻井,保护储层效果好。对复杂情况采取了有针对性的处理办法:平稳操作和合理的钻井工程措施是预防水层涌漏同层和火成岩井塌复杂的重要手段;用井场易得的固井水泥或石膏配合烧碱处理HCO3^-污染简便易行;处理火成岩井塌复杂,控制合适的钻井液性能是必要的。 相似文献
120.
陈训浩 《冶金标准化与质量》2003,41(1):5-8
从碳素结构钢热轧钢带各向异性的事实出发 ,阐述不同试样位向导致同一钢带不同的拉伸性能 ,因而影响钢带合格与否的判定。在全面考虑钢带和焊管标准的基础上 ,提出解决钢带判定的两种方法。同时 ,还对标准中存在的缺点作了说明 ,提出改进意见 ,供标准修订时参考。 相似文献