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51.
52.
This paper reports the development of a method for simultaneously measuring zeolite, silicate, and phosphate in laundry detergent
products by inductively coupled plasma atomic emission spectrometry. A sample is decomposed under alkaline oxidative conditions
to decompose zeolite, silicate, phosphate, and organic substances. Then hydrochloric acid is added to the decomposed solution
to dissolve aluminum hydroxide precipitate before analysis. This sample preparation procedure was investigated by using a
total organic carbon analyzer and was confirmed to be applicable to simultaneous measurements of zeolite, silicate, and phosphate.
Relative standard deviation for the analysis is less than 2.1%, recovery is more than 99.0%, and the calibration curve gives
a correlation coefficient ofR=1.000. The detection limit of this method for aluminum and silicon is 0.1%, and for phosphorus, 0.2% by weight in the product.
This method is applicable to various laundry detergent products that contain zeolite, silicate, or phosphate and is five times
faster than the three wet chemical methods. 相似文献
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采用拟薄水铝石和非晶态超细SiO_2微粉为原料。以溶胶-凝胶工艺制取莫来石凝胶,通过干燥、煅烧研制得片状结晶莫来石粉。初步研究了凝胶法莫来石粉在钛酸铝陶瓷和烧结刚玉砖中的应用。实验结果表明:凝胶粉起到了促进烧结、降低烧成温度的作用,并使钛酸铝——莫来石复相陶瓷和刚玉砖的强度得到了显著提高。 相似文献
55.
采用铝型材厂污泥和粘土为原料合成莫来石刚玉复相材料,主要探讨不同Al2O3/SiO2比值对形成的晶相结构影响。采用XRD和SEM表征各样品的晶相,结果表明各样品都形成2种晶相:莫来石固溶体和刚玉相,其中No.2配方中莫来石和刚玉的比例为:71.6:28.4,莫来石在扫描电镜下呈柱状交织,为较佳配方。 相似文献
56.
57.
为了提高轿车侧面耐撞性,设计耐撞性能强的B柱成为主要课题之一.目前的优化方法很难将B柱侵入量和侵入速度同时控制在理想范围内.因此,提出泡沫铝材料填充在汽车B柱内代替B柱加强板的方法,缓冲侧面碰撞冲击.通过建立泡沫铝有限元模型与材料特性分析,确定仿真泡沫铝主要材料参数.进而根据中国新车评价规程C-NCAP要求,建立轿车整车侧面碰撞有限元模型,采用LS-DYNA软件进行仿真分析.结果表明,泡沫铝填充后的B柱侵入量和侵入速度都有明显降低.泡沫铝材料塑性变形和整体弯曲变形能够吸收1.51kJ的能量,是B柱加强板的3倍.填充泡沫铝前后仿真结果表明,轿车B柱填充泡沫铝是一种提高轿车侧面耐撞性的方法. 相似文献
58.
Following our previous papers on mechanism of cyclic esters' polymerization coinitiated by tin(II) octoate [tin(II) bis-(2-ethylhexanoate), (Sn(Oct)2)] in the presence of either the low molar mass coinitiator (an alcohol, hydroxy acid, or H2O) or a macromolecule fitted with a hydroxy end group (ROH), the present work deals with ?-caprolactone (CL) and l,l-lactide (LA) polymerizations coinitiated with zinc octoate (Zn(Oct)2) or aluminum acetylacetonate (Al(Acac)3). A series of kinetic measurements revealed that similarly as in the Sn(Oct)2 coinitiated process, these polymerizations proceed by simple monomer insertion into the …Mt-OR bond, reversibly formed in the reaction -Mt-L + ROH ? …-Mt-OR + LH (where Mt = Sn, Zn or Al; L = Oct or Acac), taking place throughout the whole polymerization process. MtLn itself does not play an active role in the polymerization. Applicability of the commercially available Zn(Oct)2 or Al(Acac)3 for the aliphatic polyester (103 ≤ Mn ≤ 4 × 105) synthesis is also discussed. 相似文献
59.
LC4铝合金高温变形规律的探讨 总被引:1,自引:0,他引:1
研究LC4铝合金的高温变形规律 ,拟合出具有较高精度的高温本构模型。并应用所开发的一套数值模拟软件系统 ,对LC4铝合金的高温压缩规律及压缩过程进行了分析。 相似文献
60.
Exfoliation corrosion of aluminum alloys is a form of localized corrosion which affects many industries, specially aeronautics. The study of this corrosion mode using only electrochemical techniques is not fully efficient for the detection and control on line of this phenomenon. Therefore, we developed a non-destructive testing technique based on the acoustic emission recordings in order to follow-up this form of corrosion on aluminum alloys. Indeed, recent works have shown the interest of the acoustic emission for the detection, the monitoring and the localization of pitting corrosion on aluminum alloys. This pitting corrosion phenomenon is currently well understood and the experimental methodology acquired during that study is transposed to the study of exfoliation corrosion of aluminum alloys.The present study is conducted on two aluminum alloys: (Al 2024 T3, and Al 7449 T6 and T7). Samples are immersed 4 days in the modified ASTM STP 1134 saline solution. Observations of the structures after tests show that the exfoliation corrosion sensitivity of alloy 7449 T6 is more important than for alloy 7449 T7 which exhibits only the presence of small and non-occluded pits. Very severe exfoliation corrosion was also observed on Al 2024 T3, but after a longer immersion time or in a more acid solution.The recording of the acoustic emission activity shows evident links between this activity and the exfoliation corrosion rate. The analysis of the signal's characteristics reveals a population corresponding to the release of hydrogen bubbles. A few more energetic signals have also been observed. Their source can be either, the cracking resulting from the separation of sheets of metal, or the development and evolution of hydrogen bubbles formed inside blisters during exfoliation corrosion. 相似文献