Flow behavior and microstructure evolution of TB8 alloy during hot deformation process

Hot compression tests of metastable β titanium alloy TB8 were carled out using a Gleeble-1500 thermal simulation testing machine in the temperature range of 750-1 100 ℃, at constant strain rate from 0.01 s^-1 to l S^-1 and with height direction reduction of 60%. Flow stress behavior and microstructure evolution during hot compression of TB8 alloy were investigated. The hyperbolic-sine-type constitutive model of TB8 alloy was obtained to provide basic data for determining reasonable forming process. The results indicate that hot deformation behavior of TB8 alloy is highly sensitive to the temperature and strain rate. An analysis of the flow stress dependence on strain rate and temperature gives a stress exponent of n=3.416 19 and a deformation activation energy of Ω=227.074 4 kJ/mol. According to the deformation microstructure, no dynamic recrystallization happens below r-phase transus temperature and as a result dynamic recovery is the predominant softening mechanism. On the other hand, the main softening mechanism is characterized as dynamic recrystallization at a slow strain rate above r-phase transus temperature.     

Dry friction and wear characteristics of MoSi2 against ahoy steels

The dry friction and wear characteristics of three kinds of friction couples under different loads, MoSi2/45 tempered steel, MoSi2/45 quenched steel, and MoSi2/CrWMn steel, were investigated by using a friction and wear tester. SEM and X-ray diffraction were employed to analyze the microphotograph of the worn surface and the phase of worn pieces in order to reveal the wear mechanisms of MoSi2 material. The results show that MoSi2/CrWMn steel friction pair has good dry friction and wear properties under the load of 80 N, where the friction coefficient is 0.255 and the wear rate of MoSi2 is only 14.72 mg.km-1. But under the load of 150 N, it is MoSi2/45 tempered steel friction pair that has good tribological properties,MoSi2 under low loads is brittle fracture. With the increase of load, the main wear mechanism of MoSi2 against 45 quenched steel or CrWMn steel is adhesive wear. However, the wear mechanism of MoSi2 against 45 tempered steel is changed from oxidation-fatigue wear to adhesive wear.     

磷酸盐系溶液中钛合金微弧氧化涂层生长与组织结构

采用常流脉冲控制方式于(NaPO3)6-NaF-NaAlO2溶液中用微弧氧化法在Ti6Al4V表面制备了陶瓷化涂层, 研究了涂层的生长过程及组织结构变化.结果表明: 氧化过程中涂层的生长经历了由快到慢的过程, 在前10min涂层以较快速度生长(约3μm/min), 随着时间的延长涂层生长速度逐渐减慢; 生长过程中涂层表面微孔数目减少, 微孔孔径增大, 涂层表面气孔率增大; 涂层主要由二氧化钛的两种不同变体(锐钛矿及金红石)以及磷化物相AlPO4组成; 随着氧化的进行, 锐钛矿含量降低, 金红石含量增加, 氧化过程中发生了锐钛矿相到金红石相的相转变; 结晶AlPO4相是通过水合多聚磷酸铝在放电区附近发生高温热解反应而进入涂层.     

LF2铝合金搅拌摩擦焊接接头的组织与性能

对10 mm厚LF2铝合金搅拌摩擦焊接进行了研究.结果表明:焊接厚板时,为防止出现隧道型缺陷,须在较低的焊速和转速下进行.当焊速为9 mm/min,转速为950 r/mln,焊接输入能量为6 230 W时,接头强度值最高,其值与母材强度值相等.接头处由平均尺寸约为15 μm的均匀细小的晶粒组成;热影响区平均晶粒尺寸较大,其最大值约为28 μm;热机械影响区内组织细长,局部区域最大长度可达到85 μm.焊核区平均硬度与母材相当,中心最高硬度可达HV95,近缝区硬度低于母材硬度.     

Effect of strontium on columnar growth of dendritic α phase in near-eutectic Al-11.6%Si alloys

For Al-11.6 % Si alloy, the influence of the addition of Sr on the morphology of the dendrite α phase was investigated, and the characteristic parameters of the dendrite α phase, the primary dendrite spacing and the secondary dendrite arm spacing, were also measured. The addition of strontium promotes the columnar dendrite growth and leads to a decrease of both the primary dendrite spacing and secondary dendrite arm spacing with the increase of the content of strontium in the modified near-eutectic Al-Si alloys. It is thought that the addition of Sr leads to a reduction of the solid-liquid interfacial energy of the dendrite α phase, consequently resulting in a decrease of the growth undercooling of dendrite tips. And hence, the nucleation of the equiaxed grains in the liquid in front of the columnar dendrite tips is restrained, thus the addition of strontium in Al-Si alloys promotes the growth of the columnar dendrites. The reduction of the solid-liquid interfacial energy also leads to the decreases in the primary dendrite spacing and the secondary dendrite arm spacing.     

7075铝合金高温流变行为的研究

采用圆柱试样在Gleeble-1500热模拟机上进行高温压缩变形实验，研究了7075铝合金在高温塑性变形过程中流变应力的变化规律。实验在温度为250－500℃、应变速率为0．05－50s^-1的条件下进行。结果表明：应变速率和变形温度的变化强烈影响着合金流变应力的大小，流变应力随变形温度升高而降低，随就变速率提高而增大，可用ZenerHollomon参数的双曲正弦形式来描述7075铝合金高温压缩变形时的流变应力行为。     

钙磷层对NiTi形状记忆合金与骨组织结合特性的影响

用化学处理的方法 ,在NiTi合金表面生成钙磷 (Ca P)层 ,再将试样植入日本大耳兔的股骨中考察其生物相容性。试验结果表明 :经表面处理的试样和骨组织结合良好 ,并能传导新生骨的形成 ,表明经处理后有良好的生物相容性。而未经处理的试样 ,在实验范围内 ,没有观察到成骨细胞的存在及新生骨的形成     

用稀土添加剂改善中硅铝合金性能的研究

用一种稀土添加剂(自制)向ZAlSi7MglA铸造铝合金中加入稀土元素，以改善合金的性能。结果表明：该法使稀土元素的加入操作变得简单易行，烧损小，合金性能改善效果明显，在一定RE浓度范围内随着合金中RE含量增加合金的Rm和A同步增长。通过试验得到了最佳效果的稀土加入量。     

喷射成形Al10.8Zn2.8Mg1.8Cu合金沉淀析出强化行为

采用喷射成形技术制备Al10.8Zn2.8Mg1.8Cu高强铝合金,利用力学性能测试、高分辨透射电镜(HREM)、选区衍射(SAED)等手段系统研究120℃下该合金的时效曲线和沉淀析出行为。研究结果表明:该合金在120℃时效4h强度即可达到800MPa以上;16h达到峰时效状态,强度可达820MPa,此阶段GPⅠ区和GPⅡ区联合强化起主导作用;44h后存在长时间的时效平台,强度在800MPa左右,此阶段η′相和η相起主导强化作用。     

挤压铸造ZA27合金的凝固特性及组织分析

研究了ZA27合金挤压铸造的凝固特性和组织.差热分析表明挤压铸造可以使锌铝合金的凝固过程发生变化,压力在750MPa以上可抑制共晶反应的发生.压力下凝固,可大大减少ZA27合金的缩孔、缩松、气孔等缺陷,提高合金致密度,细化和改善组织,减轻枝晶偏析,使铸件整体的成分均匀.