显微组织对ZIRLO锆合金耐腐蚀性的影响

将ZIRLO锆合金样品分别进行1000℃-0.5h／560℃-10h、1000℃-0.5h／冷轧／560℃-10h和750℃-0.5h、750℃-0.5h/560℃-10h、750℃-0.5h／冷轧／560℃-10h的不同处理。用透射电镜观察了它们的显微组织，将它们放入高压釜中，研究了在350℃，16.8MP,0.04M LiOH水溶液中的耐腐蚀性能，结果表明，在本文所有的变形及热处理条件下中，750℃-0.5/冷轧／560℃-10h处理后样品的耐腐蚀性能最好，其原因在于样品经过这样处理后，基体αZr中固溶的Nb含量较低，并获得了纳米尺寸分布的βNb(含Fe)第二相粒子，后者对改善耐腐蚀性能尤为重要。样品在最终560℃加热处理之前的冷轧变形，可以促进βZr分解时的形核，是获得纳米尺寸βNb的必要措施。     

Preparation and characterization of Ni/Co bimetallic nano-clusters

Ni/Co bimetallic nano-cluters have been prepared from the aqueous solution by reducing their corresponding metal salts under suitable conditions. The experimental conditions including the type and concentration of protective agent, feeding order and the pH of the solution that influence the average particle size have been studied in detail. Transmission electron microscopy (TEM) indicates that the shape of those bimetallic nano-cluster particles is spheroid. The alloy structure has been shown by X-ray powder diffraction (XRD). The X-ray photoelectron spectroscopic (XPS) data have confirmed that the nickel and cobalt in the bimetallic nano-clusters are in the zero-valence state.     

非晶Fe-Zr-B薄膜穆斯堡尔谱学研究

用X射线衍射分析、X射线光电子能谱(XPS)和穆斯堡尔谱学研究了直流磁控溅射法制备的Fe-Zr-B薄膜。X射线衍射分析结果表明制备态的薄膜是非晶的;X射线光电子能谱(XPS)结果表明样品表面氧化较明显,深层部分Fe, Zr, B结合占主导地位;穆斯堡尔谱学结果表明薄膜中Fe原子周围Zr、B原子的存在使Fe原子核内场值有所下降并导致超精细场分布P(H)出现双峰结构,薄膜中存在两种不同的局域微结构。     

快淬贮氢合金的活化性能与寿命

主要讨论了快淬钛基合金具有良好活化性能及较差循环寿命的机理。研究结果表明:快淬钛基合金电极浸泡在碱液中,合金元素V、Zr、Ti、Mn、Ni以不同速度溶解,其中Ni的溶解速度最慢,使合金电极表面富Ni。富Ni电极表面具有良好的动力学性能,快淬钛基贮氢合金的放电容量急剧衰退与损失大量可吸氢的V、Zr元素密切相关。     

金属粉末注射成形粘结剂的发展

概括了金属注射成形粘结剂的功能与发展过程，并对几种典型粘结剂及其脱除工艺进行了适用性与经济性分析。     

铅基板栅合金综合性能探析

在Pb-Ca-Sn-Al合金的基础上尝试添加第五种合金元素，测试其电化学性能，并在理论上讨论了其性能提高的原因。     

尼龙-11粉末涂料

本文简要地介绍了我国粉末涂料的发展概况，并概述了热固性和热塑性粉末涂料的应用领域．文章重点介绍了尼龙－１１粉末涂料的优点及其制造法，阐述了其在管道防腐、船体防护和建筑行业等领域的应用     

RESEARCH ON A NEW FORGING TECHNIQUE—SHORT-HOLLOW-RAPID DIE FORGING

TherearethreeproblemsinTi--Alalloyforging:(1)Crystallinestructuredefects;(2)Highresistanceofdeformation;(3)Deepscratchesonthediescausedbytheforgedpiece.Thenewshort--hollow--rapiddieforgingtechniquewassuccessfullyusedinTCg,TCll,andTi679Ti--Alalloydieforging,andsolvedalltheseproblems.1THEPRINCIPLESOFSHORT~HOLLOWRAPIDDIEFORGING1.1ThePrincipleofShortDiesAccordingtotherelationsbetweentheforgingpressureandthepress--downshortages(seeFig.1),whenthepress--downshortagesarelessthan…     

Effect of AlP master alloy on grain refinement of primary silicon in eutectic Al-Si alloys

To obtain the finer primary silicon crystals, the proprietary Al-P master alloy was adopted to modify the eutectic Al-Si alloys and the most suitable modification process was made in the experiments. The SEM (Scanning Electron Microscope) and DSC (Differential Scanning Calorimeter) analysis indicate that the Al-P modifier has more advantages over Cu-P and Fe-P modifier in easily addition, no elemental alteration and less undercooling of primary silicon′s solidification, which suggests the Al-P master alloy is an effective modifier of eutectic Al-Si alloys.