化学沉积法制备的Ni(P)、Ni(B)纳米薄膜的结构与磁性

用化学沉积法制备了系列Ni(P),Ni(B)合金薄膜样品，用X射线衍射结构分析方法证明样品由尺寸为纳米量级的颗粒组成，样品在磁性上表现出超顺磁性，对热磁处理前后的磁学参数进行了比较研究。     

液相添加剂对PTCR陶瓷电性能的影响

液相添加剂ＡＳＴ（Ａｌ２Ｏ３＋ＳｉＯ２＋ＴｉＯ２）对ＢａＴｉＯ３陶瓷材料电性能的影响很大，随着Ａｌ２Ｏ３含量的增加，材料的电性能降低；ＳｉＯ２、ＴｉＯ２的物理特性对材料电性能影响较大；过量ＴｉＯ２对材料ＰＴＣ效应有重要影响，适当过量ＴｉＯ２含量，可得到性能优良的ＰＴＣＲ陶瓷。     

哈尔滨炼油厂MTBE装置试生产

介绍了哈尔滨炼油厂ＭＴＢＥ装置的工艺路线、新技术的应用及特点；催化剂的装填及应用情况；总结了生产过程中遇到的一系列问题及解决办法；探索了平稳生产的新徐径，以保证装置安全、平稳、长周期运行；同时对反应器操作温度、催化蒸馏塔操作压力、原料中醇烯比等因素对异丁烯转化率及ＭＴＢＥ产品的影响做了简单的总结。     

材料研究中系列试样的单标样法 X 射线定量分析

本文提出了用一个标样进行系列试样 X 射线定量相分析的方法.它克服了一般 X 射线定量方法需要混合研磨和手续烦复的缺点以及无标样 X 射线定量方法存在病态方程不易解决的问题.该方法对常规 X 射线定量分析具有普遍的实用性.     

自旋为j的粒子在旋转磁砀中的几何相位

用相干态的方法得到旋转磁场中自旋为j的粒子的态矢量的严格表达式，由此可计算相干态和叠加相干态的Abaronov－Anandan相位（AA相让）．并具有清楚的物理图象．     

Effect of Bi and Sr concentrations on the formation of the 2223 phase in Bi-Pb-Sb-Sr-Ca-Cu-O materials, obtained under different conditions of thermal treatment

The superconducting properties and the phase and chemical composition of Bi _x Pb_0.3Sb_0.1Sr _y Ca₂Cu₃O_z (x=1.5, 1.6, and 1.7;y=1.9, 2.0, and 2.1) materials synthesized by one-step and multistep thermal treatments have been investigated. The multistep annealing between 825–875°C promotes the 2223 phase. The change of Bi concentration has little effect on the 2223 phase formation, regardless of the kind of thermal treatment used, but increasing the Sr concentration (y> 2) strongly inhibits this phase. It has also been established that the loss of Pb after synthesis depends on the initial Bi concentration. The loss of Pb decreases when the initial Bi content is lower.     

相转移催化合成芳基烷基醚

报道了以四丁基溴化铵为相转移催化剂，简便地合成了１０个芳基烷基醚，反应几乎是定量地快速进行。     

Immobilization of inert TRISO-coated fuel in glass for geological disposal

Vitrification of TRISO-coated gas reactor fuel particles was achieved via two methods: glass melting and sintering. Inert TRISO-coated fuel particles and a borosilicate glass were used. With glass melting at 1200-1300 °C floatation and decomposition of carbon and silicon carbide occurred. Thermal pre-treatment of the particles for oxidation of pyrocarbon did not improve the coating properties of the glass. During cooling most of the particles floated and sorbed on the crucible or mold walls. The sintered glass at 700 °C showed better coating properties of the TRISO-coated fuel particles despite higher porosity compared to glass made by melting. Aqueous leaching properties of glass with particles are similar regardless the mode of fabrication, indicating the good chemical durability of the sintered glass. Sintered glasses may constitute a good technique for TRISO-coated fuel particles immobilization for an eventual deep geological disposal.     

Corrosion protection of iron by polypyrrole coatings electrosynthesised from a surfactant solution

This work is a study of the electropolymerisation of pyrrole onto iron electrodes in the presence of sodium bis(2-ethylhexyl) sulfosuccinate in a wide pH interval. The characterisation of the films was done using electrochemical techniques, SEM/EDX and IR spectroscopy. We show that it is possible to synthesise homogeneous, adherent and very compact films in the pH range between 7 and 12 under potentiodynamic, galvanostatic and potentiostatic conditions without substrate dissolution. The effects of various parameters on electrodeposition were investigated. The new procedure for the electrochemical synthesis of polypyrrole results in improved anticorrosion properties. The inhibition is proposed to be due to the sum of a repulsion of chloride ions because AOT remains entrapped in the polymer matrix and the presence of the iron oxide. Advantages of the use of surfactants in the electropolymerisation solution are discussed.