Boundary trend of α1/(α1 +α2) phase region at lower Cu side in Al-Zn-Cu system

The range of miscibility gap above 300 ℃ at low Cu side in Al-Cu-Zn ternary system was obtained by EPMA of the designed alloys and diffusion-couples treated for equilibrium. The results about the boundary trend of the α1 / (α1 α2 ) phase region was obtained. The α1 / (α1 α2 ) boundary moves towards the lower Zn side with the increase of Cu content. The results are opposite to traditional phase diagrams obtained by experiments, but consistent with recent thermodynamic calculations.     

TP347H不诱钢与12Cr2MoWVTiB（G102）耐热钢异种钢焊口试验分析

文章对运行55 221．64h的TP347H不镑钢与12Cr2MoWVTiB(G102)耐热钢异种钢焊接接头进行了试验研究，结果表明，G102侧热影响区为整个焊接接头的薄弱环节，鉴于该类焊接接头G102侧热影畸区冲击值很低，建议尽早更换。     

碳纤维表面处理对铝电解用硼化钛阴极涂层性能的影响

硼化钛阴极涂层是铝电解用可润湿性阴极材料中的一种，具有优良的抗钠渗透性和对铝液润湿性，可以有效地延长铝电解槽寿命。碳纤维是硼化钛涂层材料的增强剂之一．对硼化钛阴极涂层的性能影响很大。本文研究了不同工艺的液相碳纤维表面氧化处理法对硼化钛阴极涂层抗拉强度和粘接强度的影响。采用PTIR检测碳纤维处理后表面含氧基团的变化，寻找影响硼化钛阴极涂层性能的原因，从而达到最有效地提高TiB2阴极涂层抗拉强度和粘接强度的目的。结果表明，采用工艺(1)(10％HNO3，80℃、恒温5min．超声波、5min)对碳纤维进行表面处理最合理，处理后碳纤维表面含氧基团的含量最高．用其制备硼化钛阴极涂层的抗拉强度、粘接强度最大。     

固体超强酸SO2-4/Fe2O3-TiO2催化合成癸二酸二乙酯的研究

研究了用固体超强酸SO4^2-/Fe2O3-TiO2为催化剂，由癸二酸和乙醇反应合成癸二酸二乙酯的最佳工艺条件。结果表明，当n(醇）：n(酸）＝4．0：1，催化剂用量为酸质量的5％，反应时间为3．5h，酯的产率可达96％。该工艺产率高，反应时间短，无腐蚀无污染，催化剂可回收、活化、重复使用10次。     

Chemical States of Lanthanum in Carbonized La2O3-Mo Thermionic Cathode Materials

The chemical reaction between lanthanum oxide and molybdenum carbide was studied by thermodynamic calcu-lation, thermal analysis and in-situ X-ray Photoelectron Spectroscopy. The theoretical results show that at the environment allowing for the evaporation of lanthanum, such as in high vacuum, La2O3 in the La2O3-Mo materials can be reduced to metallic lanthanum by molybdenum carbide (Mo2C). To confirm the conclusion, many analysis methods such as XRD, SPS, and TG-DTA were taken. The experimental results show that the chemical state of lanthanum changes during heat-ing. It was proved, for the first time, that reacted metallic lanthanum appears at the surface of this kind of material at high temperature.     

(U,Gd)O2芯块试验与工业生产

文章介绍在宜宾核燃料元件厂(YFP)生产线上进行(U,Gd)O2芯块工业规模的生产试验及产品合格性鉴定,对试验结果进行讨论和评价.结果表明YFP的(U,Gd)O2芯块生产线完全具备工业生产能力,并实现(U,Gd)O2芯块制造的国产化.     

基于B／S的国贸商务信息管理系统开发研究

阐述了B/S模式的基本原理及特点,实现了基于B/S模式的国贸商务信息系统,并对实现中采用的技术作了简要的讨论。此系统是一个跨区域、跨平台的商务信息管理系统,能够实现国贸公司内部信息,如外销、采购、库存等信息的实时交互,使信息得到及时的传递。     

准连续Ti~(3+):Al_2O_3可调谐激光的研究

本文给出了Ti~(3+):Al_2O_3的准连续可调谐激光的实验结果。采用Nd:YAG内腔倍频532nm的准连续输出作为泵浦源,得到Ti~(3+):Al_2O_3的连续可调谐输出。波长覆盖范围为685nm到821nm。最大输出功率为293mW,斜率效率为20％,在805nm处的窄谱输出功率达240mW,总体转换效举为26％。     

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