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21.
The selenisation of the thin film precursors indium, Cu-In and Cu-In-Ga has been studied by in-situ X-ray diffraction. The influence of sodium doping on the kinetics of the solid-state reactions observed agrees with the predictions derived from a phenomenological model presented earlier. In this model a layer of sodium polyselenide is assumed to form at the surface of the precursor, or around each crystal grain. This layer might be responsible for impeded ion exchange in certain solid-state reactions. 相似文献
22.
Shaobing Zhou Qiuxiang Su Xiaohong Li Jie Weng 《Materials Science and Engineering: A》2006,430(1-2):341-345
In the paper, we found a novel method to synthesize dicalcium phosphate dehydrate (DCPD) nanocrystals by in situ reaction in biodegradable PDLLA matrix. Calcium hydrid was selected as calcium source of DCPD, which is different from general methods. The method is not only simple and effective to synthesize Ca–P particles, but also can avoid the aggregation of inorganic nanoparticles in the course of their being dispersed into polymer matrix. 相似文献
23.
SHIHongju SHIYongji 《半导体光子学与技术》1998,4(4):197-208,234
The liquid crystal televison spatia light modulator(LCTVSLM)characterized is usable in optical processing applications.e.g.,optical pattern recognition,associative memory,optical computing,correlation detection and optical data processing systems.The array performance and real-time optical correlation applications are reviewed. 相似文献
24.
25.
文中简述了卤化银(主要是溴化银)单晶片的某些特性,氯化银单晶片与此大致相似。作为低温晶体探测器,对~(241)Am-α放射源,分辨率为17%。卤化银晶片是固体电解质,只有Ag离子对输出电信号有贡献,有显著的极化现象。在液氮槽内溴化银晶片的电导率在几个数量级内成为可控的,由在室温下外加偏置电压大小所引起的分解状态下的初始电流决定。 相似文献
26.
本文介绍了强脉冲辐射场非平衡硬X辐射谱测量方法。文中对测量原理、关键定标技术进行了叙述。 相似文献
27.
We investigate the thermodynamics, kinetics, and capacity of the hydrogen storage reaction: Li2Mg(NH)2 + 2H2 Mg(NH2)2 + 2LiH. Starting with LiNH2 and MgH2, two distinct procedures have been previously proposed for activating samples to induce the reversible storage reaction. We clarify here the impact of these two activation procedures on the resulting capacity for the Li–Mg–N–H reaction. Additionally, we measure the temperature-dependent kinetic absorption data for this hydrogen storage system. Finally, our experiments confirm the previously reported formation enthalpy (ΔH), hydrogen capacity, and pressure–composition–isotherm (PCI) data, and suggest that this system represents a kinetically (but not thermodynamically) limited system for vehicular on-board storage applications. 相似文献
28.
The crystal structures and electrochemical properties of a V3TiNi0.56Co0.14Nb0.047Ta0.047 alloy prepared by the melt-spinning method were studied. The rapidly solidified alloy consists of a major Vanadium-based solid solution phase and a secondary Ti2Ni-based phase. The secondary phase exists between the dendritic arms of the major phase, showing a typical eutectic characteristic. With increasing cooling rate, the amount of the secondary phase decreases but the lattice parameters of both the major phase and the secondary phase show no obvious change. Because the disappearance of the catalytic effect of the secondary phase, the rapidly solidified alloy shows bad electrochemical properties except cycle stability. 相似文献
29.
The phase diagram of the Ti–In system was determined using DTA, XRD and EDX analyses. The existence of the phases Ti2In5 [Mn2Hg5 type structure, space group P4/mbm, a=0.99995(3), c=0.29960(2) nm] and Ti3In [Ni3Sn type structure, space group P63/mmc, a=0.5978(1), c=0.4812(1) nm] was confirmed. The phase previously labeled Ti3In2 was found to exist in a narrow homogeneity region near Ti56In44. Rietveld refinement of the XRD powder pattern yielded solutions compatible with a Cu3Au-type or a BiIn-type crystal structure, but not with a CuAu-type crystal structure. Furthermore, at 38.5 at.% In, a new phase was observed having a γ-brass related crystal structure [Ti8In5, space group
, a=0.99578(6) nm]. The intermetallic phases were formed by a cascade of peritectic reactions ending in a eutectic at >99 at.% indium between Ti2In5 and (In) at 0.4 K below the melting temperature of pure indium. 相似文献
30.
We present a comprehensive computational analysis of the deformation of ultrafine crystalline pure Cu with nanoscale growth twins. This physically motivated model benefits from our experimental studies of the effects of the density of coherent nanotwins on the plastic deformation characteristics of Cu, and from post-deformation transmission electron microscopy investigations of dislocation structures in the twinned metal. The analysis accounts for high plastic anisotropy and rate sensitivity anisotropy by treating the twin boundary as an internal interface and allowing special slip geometry arrangements that involve soft and hard modes of deformation. This model correctly predicts the experimentally observed trends of the effects of twin density on flow strength, rate sensitivity of plastic flow and ductility, in addition to matching many of the quantitative details of plastic deformation reasonably well. The computational simulations also provide critical mechanistic insights into why the metal with nanoscale twins can provide the same level of yield strength, hardness and strain rate sensitivity as a nanostructured counterpart without twins (but of grain size comparable to the twin spacing of the twinned Cu). The analysis also offers some useful understanding of why the nanotwinned Cu with high strength does not lead to diminished ductility with structural refinement involving twins, whereas nanostructured Cu normally causes the ductility to be compromised at the expense of strength upon grain refinement. 相似文献