Vapor absorption by LiBr aqueous solution in vertical smooth tubes

Heat and mass transfer in a falling film vertical in-tube absorber was studied experimentally with LiBr aqueous solution. The presented results include the effect of solution flow rate, solution subcooling and cooling water temperature on the absorption in a smooth copper tube 16.05 mm I.D. and 400 mm long. The experimental data in the previous report for a 1200-mm-long tube was also re-examined and compared. It was demonstrated by the observation of the flow in the tube that the break down of the liquid film into rivulets leads to deterioration of heat and mass transfer at lower film Reynolds number or in longer tubes. An attempt to evaluate physically acceptable heat and mass transfer coefficients that are defined with estimated temperature and concentration at the vapor–liquid interface was also presented.     

Determining the Instantaneous Effective Energy of x-Ray Tube Bremsstrahlung

A method is described for determining the instantaneous effective energy of x-ray tube brehmsstrahlung by means of two semiconductor detectors employing epitaxial GaAs structures and a measurement circuit, which together determine the effective energy with an error of 5% in the range 20–80 keV in the presence of nonlinearity in the detector response.     

WC/Cu复合材料制备及其高温性能

用机械合金化法结合冷变形，制备了WC／Cu复合材料，研究了冷变形后复合材料的组织特征和高温退火时韵性能变化。结果表明：烧结后的材料经冷变形，组织呈显著纤维状，WC颗粒弥散分布，密度明显提高，达到理论密度的99．2％；复合材料经600～900℃高温退火，强度和硬度略有下降，塑性则有大幅提高；900℃退火时未发生明显的再结晶，界面结合良好；所制备的WC／Cu复合材料有优良的综合性能。     

魏氏组织对20#碳钢H2S应力腐蚀开裂性能的影响

文章对H₂S-CO₂-H₂O腐蚀环境下发生H₂S应力腐蚀的20^＃碳钢弯管（无缝钢管）进行了成分、组织、拉伸、硬度和应力腐蚀开裂等性能的试验研究，并与同材质、同时投产、腐蚀环境基本相似而未发生应力腐蚀开裂的在役弯管及未使用的新弯管作对比，结果表明魏氏组织是引起20^＃钢发生应力腐蚀开裂的主要原因；正火能消除魏氏组织，降低钢的应力腐蚀开裂敏感性。     

Atomic layer chemical vapour deposition of copper

Copper films with (1 1 1) texture are of crucial importance in integrated circuit interconnects. We have deposited strongly (1 1 1)-textured thin films of copper by atomic layer deposition (ALD) using [2,2,6,6-tetramethyl-3,5-heptadionato] Cu(II), Cu(thd)₂, as the precursor. The dependence of the microstructure of the films on ALD conditions, such as the number of ALD cycles and the deposition temperature was studied by X-ray diffraction, scanning electron microscopy (SEM), and transmission electron microscopy. Analysis of (1 1 1)-textured films shows the presence of twin planes in the copper grains throughout the films. SEM shows a labyrinthine structure of highly connected, large grains developing as film thickness increases. This leads to low resistivity and suggests high resistance to electromigration.     

薄壁圆筒试样的扭转断裂曲线

通过比较多种材料的光滑薄圆筒和切口薄壁圆筒试样的扭断裂曲线，测向两种试验的断裂韧性ＫＩＩＣ相同，从而间接证实了利用光滑薄壁筒测定延性金属断裂韧性ＫＣ方法的正确性。     

水力喷射径向水平井生产管的工艺评定与检验

在URRS系统施工过程中 ,生产管处于多种变化复杂的应力和变形状态下 ,若出现失稳、渗漏、刺穿和断裂等事故 ,将造成巨大经济损失。为此 ,开展了水力喷射径向水平井用生产管的焊接方法、焊接设备、焊接工艺过程和焊接接头力学性能评定方法的试验研究。通过研究和试验 ,管材基本上实现了国产化 ,与之相匹配的焊接材料、焊接工艺以及质量检测技术已基本配套和规范化 ,形成了一套稳定的、可靠性较高且能完全满足现场工况的施工体系和质量保证体系     

纱管跳管及应对措施

通过在长期使用纱管中发现的纱管跳管的成因，提出了防止跳管的有效措施。     

The microstructure of Cu films deposited by the self-ion assisted technique

The microstructures of Cu films deposited by the self-ion assisted, partially ionized beam (PIB) deposition technique under two different accelerating potentials, 0 KeV and 6 KeV, are compared. The 6 KeV film shows a bimodal (111) fiber and (100) fiber texture with an abundance of twin boundaries and a relatively large average grain size with a typical lognormal distribution. The 0 KeV film consists of small, mostly (111) oriented grains with islands of abnormally large (100) grains. The controlling factors for the abnormal growth of the (100) grains are discussed in relation to the observed microstructures, showing that all factors necessary for abnormal (100) growth are present in the films.     

φ1m氨合成塔20钢异径管失效分析

分析了氨合成塔底部副线20钢异径管爆破的原因。结果表明：异径管长期处于200℃以上工作，管内H2与管材中的碳或Fe3发生化学反应，生成CH4致使管内脱碳并产生裂纹，异径管强度降低脆性增加，导致爆破。