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101.
Guo-jun Wang ) Bai-qing Xiong) Yong-an Zhang) Zhi-hui Li) Pei-yue Li) ) State Key Laboratory for Fabrication Processing of Nonferrous Metals General Research Institute for Nonferrous Metals Beijing China ) Northeast Light Alloy Co. Ltd. Harbin China 《北京科技大学学报(英文版)》2009,16(4):427-431
The microstructure of the as-cast 2D70 aluminum alloy and its evolution during homogenization were investigated by means of optical microscopy (OM), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X-ray diffraction (XRD), and differential scanning calorimetry (DSC) analysis. The results indicate that the microstructure of the as-cast 2D70 aluminum alloy mainly consists of the dendritic network of aluminum solid solution and intermetallic compounds (Al2CuMg, Al2Cu, Al9FeNi, Cu2FeAl7... 相似文献
102.
103.
《Ceramics International》2022,48(21):31203-31210
Ti–Si–Fe alloys extracted from high-titanium blast furnace slag were utilized to replace part of the silicon powders, and then nitride/oxynitride bonded SiC ceramics were prepared by reactive sintering in graphite bed. Ti–Si–Fe alloys could react with CO/N2 at a low temperature (1200 °C), and the addition of Ti–Si–Fe alloys could reduce the nitriding temperature of Si. Density functional theory calculations suggested that Ti–Si–Fe alloys enhanced reaction activity via weakening the strength of CO and NN bonds. The regional equilibrium phase diagrams of Si–C–N–O and Ti–Si–C–N–O under CO/N2 atmosphere were calculated by thermodynamics. The change of whiskers morphology was observed by scanning electron microscope. Furthermore, the bulk density, the cold modulus of rupture, and the cold compressive strength improved with Ti–Si–Fe alloys content. The results showed that the addition of Ti–Si–Fe alloys not only significantly promoted nitriding of Si and formation of Si3N4 whiskers, but also improved the mechanical properties of the samples. 相似文献
104.
105.
M. M. Kamel 《Journal of Applied Electrochemistry》2007,37(4):483-489
Thin films of cobalt–nickel alloys were galvanostatically deposited onto steel substrates from gluconate baths. Cathodic polarization
curves were determined for the parent metals and Co–Ni alloy. The effects of bath composition, current density and temperature
on cathodic current efficiency (CCE) and alloy composition were studied. The deposition of Co–Ni alloy is of anomalous type,
in which the less noble metal (Co) is preferentially deposited. The CCE of codeposition is high and increases with increase
in temperature and current density, but it decreases as the [Co2+]/[Ni2+] ratio in the bath increases. The percentage of Co in the deposit increases with increasing cathodic current density, temperature
and increasing Co2+ ion concentration. The structure and surface morphology of the deposit were studied by XRD, ALSV and SEM. The results showed
that the alloys consisted of a single solid solution phase with a hexagonal close packed structure. 相似文献
106.
A novel polymerization procedure, the concentrated‐emulsion graft polymerization of styrene monomer with poly(butyl acrylate) seed, was proposed for the production of a self‐compatibility macromolecule alloy. The effects of the butyl acrylate content, sodium dodecyl sulfate concentration, and polymerization temperature on the graft ratio were investigated. Scanning electron microscopy, transmission electron microscopy, and impact strength were used to characterize the microstructure and mechanical performance of the self‐compatibility macromolecule alloy. The results showed that increasing the butyl acrylate content, reducing the sodium dodecyl sulfate concentration, and improving the polymerization temperature all favored an increased graft ratio, which resulted in increased impact strength of the self‐compatibility macromolecule alloy. Therefore, the concentrated‐emulsion polymerization method is particularly suitable for seed‐graft polymerization. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 2915–2920, 2002; DOI 10.1002/app.10288 相似文献
107.
The oxidation behavior is very different for an aluminide with a wide homogeneity range such as -NiAl than for a line compound such as NbAl
3.Oxidation of -NiAl at temperatures 1273 K leads to a slow-growing -alumina layer. The metal phase beneath the scale remains as -NiAl; however, cavity formation is observed. The cavity formation may be favored by sulphur surface segregation. Oxidation of NbAl
3
at temperatures 1273 K initially leads to -Al
2O3,but the Al depletion causes the formation of Nb
2
Al beneath the oxide layer. Cracking of the Al
2O3
layer opens Nb
2
Al to the atmosphere, which oxidizes rapidly to Nb
2O5 and NbAlO4.After consumption of the Nb
2
Al, a layer of Al
2O3
formed again on the NbAl
3
phase, but failure of the alumina and the fast growth of the other oxides occur as a repeated process. Thus, NbAl
3
exhibited rapid linear oxidation kinetics. Multiphase alloys in the system Nb-Ni-Al generally behave better than NbAl
3,and the low oxidation rates of -NiAl can be approached. In the temperature range below 1273 K, with a maximum at 1000 K, both NiAl and NbAl
3
show the pest phenomenon, an intergranular disintegration. Preceding the disintegration, oxygen diffuses into the grain boundaries of the material and Al
2O3
is formed at the grain boundaries, beginning from the surface region. NiAl is susceptible only in a very limited range of oxygen pressures and temperatures, whereas NbAl
3
is much more susceptible. 相似文献
108.
The effects of insoluble eutectic Si particles on the growth of anodic oxide films on ZL114A aluminum alloy substrates were in-vestigated by optical microscopy (OM) and scanning electron microscopy (SE... 相似文献
109.
采用扫描电镜(SEM)、X射线衍射仪(XRD)、电子能谱(EDS)分析Cu-Te-Cr合金时效析出相的形貌与组成,研究合金元素对Cu-Te-Cr合金时效组织与性能的影响。结果表明,时效过程中Te、Cr以多元化合物或细小的单质Cr析出,合金的硬度明显升高,随时效温度的升高,Cr粒子长大,共格度降低;同时基体晶粒内,部分析出相重溶,使合金硬度下降;由于Cr和Te两种元素互不相溶,其交互作用生成CrxTey化合物,随着Te含量的增加,铸造过程中生成这种化合物越多,减少Cr元素在铜基体的固溶度,从而合金硬度下降,而导电率有所提高。 相似文献
110.
在H厂生产硝酸的2套机组4台氨氧化常压炉中用Pt-Rh或Pt-Pd-Rh针织催化网作实验,并将稀土强化Pt-Pd-Rh针织催化网与该2种催化网进行了应用比较.用化学分析、光谱定量、光电子能谱、扫描电镜等方法分析了样品的组成及状态.结果表明,优化配套的稀土强化Pt-Pd-Rh针织催化网转化效率高、吨酸铂耗低、使用寿命长,合金中Pt高温氧化轻微,Rh的表面氧化及富集减弱,催化效果明显.提出了氨氧化常压炉用铂合金针织催化网的配套措施. 相似文献