Preparation and characterization of GaN films grown on Ga-diffused Si （111） substrates

Hexagonal GaN films were prepared by nitriding Ga2O3 films with flowing ammonia. Ga2O3 films were deposited on Ga-diffused Si (111) substrates by radio frequency (r.f.) magnetron sputtering. This paper have investigated the change of structural properties of GaN films nitrided in NH3 atmosphere at the temperatures of 850, 900, and 950℃ for 15 min and nitrided at the temperature of 900℃ for 10, 15, and 20 rain, respectively. X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray photoelectron spectroscopy (XPS) were used to analyze the structure, surface morphology and composition of synthesized samples. The results reveal that the as-grown films are polycrystalline GaN with hexagonal wurtzite structure and GaN films with the highest crystal quality can be obtained when nitrided at 900℃ for 15 min.     

铝合金液态与半固态压铸件的组织性能研究

对A356铝合金液态与半固态压铸成形件在压铸态和T6热处理态下的力学性能与微观组织进行了研究。试验得出，与液态压铸成形件相比，半固态压铸成形件可以获得更佳的综合力学性能；经同样T6热处理后，两者抗拉强度都得到提高，伸长率下降，但半固态压铸成形件抗拉强度提高的幅度更大，伸长率降低得更少。从微观角度解释了两种不同成形方法产生这一性能差异的内在原因。     

反应溅射制备AlN薄膜中沉积速率的研究

通过对浅射过程中辉光放电现象及薄膜沉积速率的研究，发现随着氮浓度的增大，靶面上形成一层不稳定的AlN层，由于AlN的溅射速率远小于Al，从而使薄膜的沉积速率显著下降。同时还研究了其它溅射参数对薄膜沉积速率的影响。结果表明：随靶基距的增大靶功率的减小，不同程度引起沉积速率的下降；随着溅射气压的增大，最初沉积速率不断增大，当溅射气压增大到一定程度时，沉积速率达到最大值，之后随溅射气 压的增大，又不断减小。     

铝锅蒸屉零件冲孔成形模设计与制造

该零件原采用先成形后冲孔两道加工工序,经对零件进行工艺分析后,改为冲孔成形一道加工工序.改进后的模具结构合理、效率高、产品零件稳定性可靠.     

Bio-mimetic surface structuring of coating for tribological applications

A novel multilayered coating was developed for applications associated with friction reduction and wear resistance improvement. The nano-engineered coating integrates a soft lubricating layer, consisting of MoS₂-PTFE, onto hard load-supporting layers, with controlled surface morphology (roughness and patterning) of cBN-TiN. The coating was synthesized by sequential procedures including electrostatic spray deposition of cBN particles with different average particle sizes, chemical vapor deposition of TiN, deposition of nano- and micro-sized MoS₂ dispersed in PTFE, and curing. The effect of cBN particle size (with different combinations of particle size) and deposition parameters (specifically electrical voltage) on the cBN-TiN surface morphology were studied experimentally and optimized. SEM characterization of the as-synthesized cBN-TiN coating shows surface features similar to that of colocasia esculenta, with alternating nano- and micro-sized domes and “pockets”; the MoS₂-PTFE top layer has MoS₂ particles retained in the pockets by a basket structure formed during PTFE curing. Tribological and scratch tests were carried out for the as-prepared cBN-TiN and cBN-TiN/MoS₂-PTFE multilayered coatings. Sliding test results demonstrate significantly lower friction coefficient for the multilayered coating, showing that the unique integration of soft lubricating layer and biomimetically structured hard layer can effectively improve tribological performance. It is suggested that lubrication at the frictional contacts was realized by continuous release of the lubricants, MoS₂ and PTFE, from the pockets.     

离子渗氮对2Cr13钢疲劳性能的影响

对2Cr13不锈钢离子渗氮后的疲劳性能进行试验研究，结果表明，离子渗氮后，材料的表面性能得到改善并能造成沿氮化层有利的应力分布是其疲劳强度显著提高的主要原因。     

1Cr20Co6Ni2WMoV钢热变形行为研究

文章采用Gleeble-2000热模拟试验机对1Cr20Co6Ni2WMoV热强钢的热变形行为进行研究。变形温度为950℃,1000℃,1050℃,1100℃,1160℃,变形速率为0．01s~(-1),0．1s~(-1),1s~(-1),10s~(-1)。结果表明．1Cr20Co6Ni2WMoV钢在低应变速率热压缩变形过程中发生明显的动态再结晶;当应变速率大于10s~(-1)时,只发生动态回复。动态再结晶晶粒随变形温度降低,应变速率升高而减小。随应变速率的提高,峰值应力和峰值应变均升高。     

铸态QT800-2铸件的生产

介绍了用覆砂铁型工艺生产轮廓尺寸为Ф30×260mm的铸态QT800—2通机曲轴铸件的生产控制方法。选择炉料：废钢为厚度≥3mum的Q235冲压边料，生铁为Q10，球化剂为QRMg8RE3，孕育剂用FeSi75A；球化处理温度在1400-1450℃，加入量1．0％．1．2％，盖包法处理，并控制w（Mg残）／w（RER）〉1；采用二次孕育处理方法，加入量0．8％-1．0％，稳定生产出抗拉强度800．930MPa，伸长率2％．5％的铸态QT800—2铸件。     

高速电弧喷涂FeAlCr/Ni包Cr3C2涂层高温性能

用高速电弧喷涂技术制备了FeAlCr/Ni包Cr3C2涂层,并对涂层的耐高温冲蚀性能、高温腐蚀性能和高温磨损性能进行了研究.结果表明,与基体比较涂层具有良好的耐高温冲蚀性能,并随温度的升高和冲击角度增大,耐冲蚀性能提高;良好的高温抗腐蚀性能,随温度升高,腐蚀率略有上升;优异的常温耐磨损性能,超过550℃的耐磨损性能高.     

ANALYSIS OF DEPOSITED PRODUCTS AND REANODIZED POROUS LUBRICATING FILM ON A1 AFTER(NH_4)_2MoS_4 SOLUTION TREATMENT

Observation was carried out of the structure of sulphuric,oxalic or phosphoricfilm on Al after treatment of reanodizing and electrolytic depositing lubricant in(NH_4)_2MoS_4 solution,as well as of the deposited products by means of EMPA,TEMand energy spectro-scopic analysis.The deposited products are mixture of compounds ofS and Mo rather than single MoS_2 and most of them dcposited near the surface layerof the film.Some regular long pores without barrier layer occurred in the film,but theregular fine channels without relation to the structural element parameters of originalanodized film were found in the thickened barrier layer of phosphoric film.Sulphur maybe remained as Mo sulphide in the film during heating under Ar protective environment.