提升检测机构水平、保持体系有效的运行

探讨了检测机构提高管理水平和技术能力的途径,提出了保持管理体系的持续有效运行方法。     

乳胶涂料中填料粒径测定与分散剂的选择

介绍了重力沉降法和容量沉降法两种测定乳胶涂料中填料粒径的方法。通过比较粉体粒径结果显示：沉降法比激光法更形象直观，更能代表体系粒径真实情况。以滑石粉、重钙、轻钙粉体为基准，采用不同用量、不同类型的分散剂的容量沉降法进行比较得出：用容量沉降法能定量地对分散剂性能做出评价。     

Probabilistic and interval reliability design of the composite pressure vessel

Considering the randomness or interval character of physical parameters and applied loads of composite pressure vessels (COPV), the COPV reliability-analyzing model is built. And then the computational expressions for the mean value, standard deviation and deviation of fiber stress are deduced by the random factor method. The probabilistic and interval reliability designs on COPV are implemented by utilizing the probabilistic method and interval method combined with the improved particle swarm optimization (PSO) algorithm, respectively. The influence of fluctuation of structure uncertain parameters on COPV design thickness is inspected. Finally, examples are given to demonstrate that both probabilistic and interval reliability methods can satisfy the safety requirement and both are of higher rationality than the traditional safety factor method. And probabilistic method has a lower relative error but a higher computational complexity contrasted with the interval method.     

超细Al（OH）3的粒度控制研究

采用铝酸钠种子分解法制备超细Al（OH）3.用X射线衍射仪（XRD）表征了样品的晶相组成,用扫描电子显微镜（SEM）观察了样品的形貌,用激光粒度分析仪测定样品的粒度分布.研究了NaOH浓度、NaOH/Al（OH）3摩尔比,分解温度,分解时间、晶种率和搅拌速率等因素对Al（OH）3的粒度的影响.结果表明：NaOH浓度越高,分解温度越低,NaOH/Al（OH）3摩尔比越小,得到的Al（OH）3颗粒的粒度越小.试验条件为：NaOH浓度180 g/L,NaOH/Al（OH）3摩尔比1.15,分解温度40℃,分解时间26 h,晶种率8％,搅拌速率200 rpm时,氢氧化铝颗粒的平均粒度为2.89 μm.     

Recent progress of CERN RD50 Collaboration

The objective of the CERN RD50 Collaboration is to develop radiation hard semiconductor detectors for very high luminosity colliders, in particular, for the upgrade of the large hadron collider （LHC） which itself is scheduled to be operational in 2007. The approach of the RD50 has two major research lines, material engineering and device engineering. These are further subdivided into projects covering defect characterization and engineering, new detector materials, detector characterization, new detector structures and full detector systems. Presently, 264 members from 53 institutes are actively participating in the RD50 Collaboration. Detectors made of defect engineered substrates, e.g. high resistivity magnetic Czochralski （MCz-Si）, epitaxial silicon （Epi-Si） on Czochralski silicon （Cz-Si） substrate, intentionally thermal donor （TD） compensated p-type MCz-Si and oxygen enriched （DOFZ） silicon, have been demonstrated by the RD50 Collaboration. An overview and highlights of the results of these defect engineering techniques were given in this report.     

A computational fluid dynamic analysis of gas and particle flow in flame spraying

The flame spraying process, which is a common industrial thermal spraying application, has been analyzed by means of three-dimensional computational fluid dynamics (CFD) simulations. The process used at the Volvo Aero Corporation for the coating of fan and compressor housings has been modeled. The process uses the Metco 6P torch (Metco, Westbury, NY), which ejects a mixture of acetylene and oxygen at high speed through a ring of 16 orifices to form the flame. A stream of argon gas flowing through an orifice in the center of the ring carries a powder of nickel-covered bentonite through the flame to the spray substrate. The torch is cooled by a flow of air through an outer ring of 9 orifices. The simulation emulated reality closely by including the individual inlets for fuel, cooling air, and injected particles. The gas combustion was simulated as a turbulent, multicomponent chemically reacting flow. The standard, two-equation k-ε turbulence model was used. The chemical reaction rates appeared as source terms in the species transport equations. They were computed from the contributions of the Arrhenius rate expressions and the Magnussen and Hjertager eddy dissipation model. The first simulations included several intermediate chemical substances whose predicted concentration agreed favorably with measurements. Later, more simplified simulations incorporated only the global chemical reaction involving the initial and the final products, with corrections to the thermal properties being made to account for the missing intermediaries. The gas velocity and temperature fields predicted by the later simulations compared satisfactorily to those predicted by the earlier, more elaborate, ones. Therefore, the final simulations, which incorporated injected particles, were conducted employing the simplified model with only the global reaction. An in-house finite difference code was developed to calculate particle properties. Allowance was made for elliptical shapes, phase changes, and internal heat transfer with regard to the composite material. The particle velocities and temperatures predicted by the final simulations compared fairly well with experimental results obtained with the optical DPV2000 system.     

Temperature Dependence of the Magnetocrystalline Anisotropy in Nd_2Co_(14)B Compound

Easy and hard magnetization curves of Nd_2Co_(14)B compound have been measured withextracting-sample-magnetometer(μ_0H_(max)=6T)at 10～300 K.Magnetic anisotropy constants K_1 and K_2have been determined by fitting the hard magnetization curves,in which only K_1 ,K_2 and misalignment anglehave been taken as fitting parameters.The values of K_1 and K_2 at 4.2 K were derived by extrapolation.Anisotropy coefficients,x_2~° and x_4~°were derived from the anisotropy constants.The anisotropy constant K_2increases rapidly with increasing temperature when TT_(sr).The temperature depen-dence of the magnetic anisotropy coefficient x_2~° was fitted with the formula.The anisotropy coefficients x_2~°can be well described by the tenth-power law from 4.2 K to T_(sr)and by the sixth-power law from T_(sr_ to 300 K.     

AGING BEHAVIOUR OF PARTICULATE REINFORCED ALUMINUM ALLOY MATRIX COMPOSITES

The process of aging precipitation in SiC_p/6061 and Al_2O_3/6061 composites were investigated. Hardness testing, differential scanning calorimetry(DSC) and transmission electron microscopy were employed. Results showed that the precipitation phase form directly along dislocation lines in the composites because the particles produce high densities of dislocations which makes vacancy densities in the composites decrease, and the main precipitation phase at peak hardness was β′ phase.     

泡沫塑料表面的磁控溅射镀膜技术研究

对硬质聚氨酯泡沫塑料进行适当的前处理(涂刮不饱和聚酯腻子和喷涂双组份聚氨酯清漆),再采用磁控溅射镀膜技术对其进行紫铜T2镀膜,能够有效地降低泡沫塑料的吸水率,提高尺寸稳定性.     

液态铝合金表面张力快速检测新方法与装置

表面张力是液态合金的重要物性参数之一,铝合金表面张力与其变质处理效果及充型能力等质量参数密切相关,研究铸造铝合金表面张力快速检测方法及装置,对于开发铝合金熔炼质量炉前实时评价系统具有非常重要的实际意义.介绍了一种液态铝合金表面张力快速测试的新方法和新装置,新方法以固定时间内吹入被测液体的气泡个数以及气泡在生长过程中内部压差变化为信息参数,通过回归公式求解表面张力.基于该方法研制的表面张力新型测试装置由单片机测控单元、探头及其锁紧和升降机构、供气单元等部分构成.采用新装置可在5 s内测得铝合金表面张力,且具有较高的测试精度.