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41.
Yuk Ming X. Hung Hung Mariano H. Talou María A. Camerucci 《International Journal of Applied Ceramic Technology》2021,18(5):1466-1477
Alumina ceramic porous structures were shaped by the fused deposition of alumina/polyamide 612 composite granules using an FDM 3D printer with a modified extruder to process granulated powder instead of a filament. The composite granules were prepared via thermally induced phase separation (TIPS). Firstly, in order to determine the proportion of polymer/solvent to be used in the TIPS process, different volume fractions of PA612 in dimethyl sulfoxide (DMSO) were studied (0.01 to 0.20), and the granules obtained were characterized by SEM, DSC, and Raman spectroscopy. Secondly, the addition of different ceramic loadings to the PA612/DMSO solution was studied with the aim of determining the amount to be used for preparing the composite granules by TIPS. In particular, the effect of the alumina content on the morphology and size of the obtained composite granules was studied. In addition, rheological properties (oscillatory and rotational tests) of the feed materials were studied. Finally, the printing conditions, including the nozzle temperature and nozzle diameter, and the extrusion process, were optimized in order to obtain porous structures with good quality. Alumina porous structures were successfully printed, debinded, and sintered. Adequate bonding between layers was achieved, and no defects at interfaces were detected. 相似文献
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以6061Al作为基质材料,利用液体冶金的搅拌铸造技术及挤压法制备Al2O3颗粒增强的金属基复合材料,选取6061Al添加3种质量分数为5%、10%和15%的Al2O3为研究对象,以改善6061Al/Al2O3复合材料的力学性能。通过SEM分析表明,Al2O3颗粒在6061Al金属基体中的分布相当均匀;由X射线衍射试验结果显示,复合材料中只有6061Al和Al2O3,且不会影响结晶性及6061Al的组织结构型态。试验结果表明,随着Al2O3添加量增加至15%,6061Al/Al2O3复合材料的硬度和抗拉强度均有较大提高,但伸长率略有下降,由于材料孔隙率的提升,致密度下降,从而引起材料的硬度略微下降;分析磨损量与Al2O3添加量及磨损率与滑动距离的关系,结果显示商用6061Al的磨损率最大,而6061Al/Al2O3(15%)复合材料的磨损量最小,并且磨损率最低,这是由于在6061Al中加入Al2O3颗粒,Al2O3颗粒的存在可以减少磨粒对基体的犁削作用,有效提高基体的耐磨性。深入探讨Al2O3颗粒增强的金属基复合材料,发现颗粒增强体以很细的粉末(一般在20 μm以下)加入到金属基中起到提高硬度、强度和耐磨性的作用;然而,Al2O3添加量越来越大时,其对6061Al系列材料的硬度、强度和耐磨耗性等性能将起到负面作用。 相似文献
45.
Hiroyuki?Y.?SuzukiEmail author Hidenori?Kuroki 《Metals and Materials International》2004,10(2):185-191
A new compacting method for powder materials is presented. High-Speed Centrifugal Compaction Process (HCP) utilizes centrifugal
force of about 10,000 g for the compaction. HCP is suitable for net shape compaction of fine sub-micron and nano-powders.
HCP possesses a unique compacting mechanism that is different from other colloidal processes including Pressure Casting (PC),
and has a number of useful characteristics. HCP has a higher compacting speed than PC, wide applicability for net shape formation,
as well as a defect removing function. Because of homogeneous and flawless green microstructure, HCP alumina shows superior
sinterability and higher strength and hardness than most of other aluminas.
This article is based on a presentation made in the symposium “The 3rd KIM-JIM Joint Symposium on Advanced Powder Materials“,
held at Korea University, Seoul, Korea, October 26–27, 2001 under auspices of The Korean Institute of Metals and Materials
and The Japan Institute of Metals. 相似文献
46.
1 INTRODUCTIONAlumina(Al2 O3)ceramicsareoftenconsideredforstructuralapplications,duetotheirpropertiesofhighhardness ,chemicalandwearresistanceandgoodmechanicalpropertiesatroomandhightemperature .Thewellknownlimitationfortheseceramics ,how ever ,istheverylowtoughness .Recentstudieshaveshownsignificantimprovementsinmechanicalprop erties ,includingtoughness ,byaddingductilesecondphaseparticles ,suchasNi,Al,MoandCu[14 ] .Anincreaseof 80 % 333%inthefracturetoughnesshasbeenreportedforAl2 O3… 相似文献
47.
The residual stresses in -Al2O3 scales formed on high-purity FeCrAl and FeCrAlY during oxidation at 1200°C and subsequent cooling and reheating were studied using photostimulated luminescence spectroscopy. Systematic measurements of the stress in the oxide were made as a function of both alloy thickness and cooling rate and the development of stresses in the oxide scale during thermal cycling was investigated as a function of the temperature. Depending on the ratio of the alloy and oxide-scale thicknesses, substantial stress relaxation was observed to occur during cooling at a rate of 8 K/min. Compressive growth stresses of 1 GPa were determined by comparing the residual-stress measurements at room temperature with those calculated based on thermal-expansion mismatch. No significant differences in the growth stresses, the total residual stresses, or the stress relaxation during thermal cycling were observed between the oxides formed on the Y-doped and undoped FeCrAl samples. Stress relaxation is also shown to lead to the development of tensile stresses in the oxide scale under certain conditions, in particular, those associated with slow cooling followed by rapid heating. 相似文献
48.
Molds made of gray cast iron for casting pig iron ingots are subjected to severe temperature fluctuations. The main life-
limiting factor for mold damage is the formation of surface cracks arising from thermal fa-tigue. Various flame and plasma
sprayed coatings were investigated to extend the life of these molds. Coating materials studied include plasma sprayed ceramic
coatings with bond coats as well as flame sprayed oxidation- resistant alloy powders. The results of cyclic furnace tests
from room temperature to 1100 °C in air, simulating the thermal cycle in casting, indicated that failure occurred along the
interface between the bond coat and the gray iron substrate because of iron oxidation, and not at the interface between the
ceramic top coat-ing and the bond coating for a superalloy substrate. The field test results indicated that plasma sprayed
alumina coatings with 200 μm top coating thickness are the most promising materials for pig iron casting. 相似文献
49.
The relative reactivities of the lower alkanes in hydrogenolysis on a Pt/Al2O3 catalyst depend on the H2 pressure used, as do those of a Ru/Al2O3 catalyst, pretreated in various ways, for propane hydrogenolysis. Apparent activation energies also vary with H2 pressure. No single rate measurement adequately represents catalytic activity, which is properly defined as the rateconstant for the slow step. 相似文献
50.
Yury G. Gogotsi Franz Porz Viktor P. Yaroshenko 《Journal of the American Ceramic Society》1992,75(8):2251-2259
The study examines the effect which the composition of hot-pressed electroconductive ceramics has on their structure, mechanical properties, and oxidation behavior, for ceramics of the type AIN–Al2 O3 –42 wt% TiN, differing in the AIN/Al2 O3 ratio. The results are physico-mechanical property data, including density, hardness, strength, fracture toughness, and wear resistance. A correlation was found between the wear resistance and fracture toughness. The analysis of oxidation products revealed the formation of α-Al2 O3 and rutile in the temperature range from 600° to 1100°C and aluminum titanate above 1200°C. The spallation of the oxide layer caused low oxidation resistance of Al2 O3 -rich composites above 1250°C. The oxidation of composites was compared with the oxidation of pure TiN. The relationship is discussed between material properties, composition, phases, and processing parameters. 相似文献