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Gasification of polyethylene (PE) pellet was studied using atmospheric argon-steam plasma generated by microwave discharge and the feasibility of the process was examined. The experimental results showed that additional steam to argon plasma promoted the weight decrease of PE and enhanced the production of H2, CO, CO2 and CH4. The results confirmed that the treatment of plastics with the steam plasma was effective to obtain synthesis gas. 相似文献
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In polyolefin processes the melt index (MI) is the most important control variable indicating product quality. Because of
the difficulty in the on-line measurement of MI, a lot of MI estimation and correlation methods have been proposed. In this
work a new dynamic MI estimation scheme is developed based on system identification techniques. The empirical MI estimation
equation proposed in the present study is derived from the 1
st
-order dynamic models. Effectiveness of the present estimation scheme was illustrated by numerical simulations based on plant
operation data including grade change operations in high density polyethylene (HDPE) processes. From the comparisons with
other estimation methods it was found that the proposed estimation scheme showed better performance in MI predictions. The
virtual sensor model developed based on the estimation scheme was combined with the virtual on-line analyzer (VOA) to give
a quality control system to be implemented in the actual HDPE plant. From the application of the present control system, significant
reduction of transition time and the amount of off-spec during grade changes was achieved 相似文献
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Liquid viscosity and density of six binary mixtures of HFC-134a with glycols [ethylene glycol, diethylene glycol, triethylene glycol, polyethylene glycol (400), and polypropylene glycol (2000)] have been measured in the temperature range from 273 to 333 K. The viscosity was measured by a rolling-ball viscometer calibrated with standard liquids of viscosities and densities (JS5, JS10, JS20, and JS50). The density was measured with a glass pycnometer. The uncertainties of the measurements were estimated to be less than 3.4 % for viscosity and 0.04 % for density, respectively. An equation is given to represent the obtained viscosity values as a function of weight fraction and temperature. 相似文献
8.
以硫酸、磷钨酸、ZRP-5分子筛为催化剂,研究了二甘醇(DEG)脱水环化的反应规律。结果表明,DEG发生分子内脱水环化反应,生成1,4-二氧六环(DOX),DEG分子间脱水不仅可以生成四甘醇、六甘醇等,同时可生成三甘醇、五甘醇等一系列的多甘醇(PEG)。不仅DEG可以脱水环化生成DOX,在反应中生成的PEG也同样可以进行生成DOX的反应。对于二甘醇(DEG)脱水环化反应,硫酸是性能优良的催化剂,反应可以在较低的温度下进行,馏出产物中DOX选择性大于95%。 相似文献
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Frdric Boschet Catherine Branger Andr Margaillan Thieo E Hogen‐Esch 《Polymer International》2005,54(1):90-95
The synthesis of 2,2,3,3‐tetrahydro‐perfluoroundecanoyl end‐functionalized polystyrene–poly(ethylene oxide) block (PS‐block‐PEO‐RF) copolymers and their matching PS‐block‐PEO diblock copolymers was carried out by sequential anionic polymerization. Viscometry and 19F NMR studies show that the PS‐block‐PEO copolymers, in contrast to their matching PS‐block‐PEO‐RF copolymers, exhibit a micellar rather than the associative behavior seen for the latter. However, the presence of an excess of fluorinated acid, used for end‐functionalization, produces a reduction of the associative behavior above the overlap concentration, with the fluorinated acid acting like a surfactant. A competition may also occur between PS—and RF—mediated micellization. Copyright © 2004 Society of Chemical Industry 相似文献
10.
研究了杂多酸催化无水乙醇和环氧乙烷(EO)制备乙醇乙醚的醚化反应,考察了不同种类的杂多酸以及醚化反应工艺条件对反应活性和选择性的影响.结果表明,PW_(12)催化剂的反应活性高、反应温度低、选择性好,当用PW_(12)作催化剂,乙醇与环氧化乙烷之比为3.0(mol),反应温度45℃,反应时间1h时,转化率和选择性均超过97%. 相似文献