炭材料的高温粘结剂(Ⅰ)

随着炭材料在高温领域应用的增长 ,对炭材料部件的生产和连接性能的要求越来越高。传统的机械连接技术在接头处有明显的应力集中现象 ,因此需要新的连接技术以用于制造和连接复杂或大尺寸的材料、部件。由于粘接技术的突出优势 ,对炭材料高温粘结剂的研究越来越活跃。就高温粘结剂的定义、分类等进行了介绍 ,并着重就应用于炭材料的无机型和冷固化型高温粘结剂及其性能进行了讨论。     

Experimental analysis on mechanical interlocking of metal–polymer direct joining

Injection molded direct joining (IMDJ) is a method for direct joining of metals and polymers. In this work, we identified the most influential parameter for IMDJ and explained the reasons for successful joining by considering mechanical interlocking. We prepared hybrid joints of 30% glass-fiber-reinforced polybutylene terephthalate and aluminum alloy (A5052) plates with laser-treated surface dimples via IMDJ under various injection parameters. We studied the effects of the packing and holding pressures and the polymer temperatures on the joining strength. We discussed the reasons for the observed effects by considering mechanical interlocking, including the infiltration depth and the contact between the metal and the polymer. We found the packing pressure to be the most influential parameter. Moreover, the interaction between the packing pressure and the polymer temperature also influenced the joining strength considerably. The increased joining strength under various combinations of injection parameters was a result of deeper infiltration depth and better contact. We anticipate that the findings of this study will aid better selection of injection parameters for IMDJ.     

Al/Ti反应多层膜中反应区传播速度的理论计算

Al/Ti反应多层膜中反应区的传播速度是表征其特性的特征参数之一.通过定义初始单层厚度比为δ:(2b-1)δ,将Mann模型扩展为可计算任意厚度比的多层膜中反应区的传播速度.采用扩展模型计算了1A1/1Ti和3A1/1Ti反应多层膜中反应区的传播速度,计算结果与文献中的实验结果吻合.此外,讨论了预混厚度对反应传播速度的影响,得到了预混厚度与临界厚度的关系式.     

小口径耐磨复合钢管的研制

采用SHS铝热 -重力分离法制备陶瓷内衬复合钢管 ,研究了影响制备陶瓷内衬复合钢管的因素。结果表明 ,选择壁厚均匀的母管 ,采取适当的预热温度、适量的添加剂均有利于制备陶瓷内衬复合钢管。     

浅谈输变电线路施工中导、地线压接施工技术

文章分析了输变电线路施工中导、地线连接方式三种施工方法的适用性、施工流程和注意事项,并分析了连接后不同损伤情况下的修补和处理方法,以输电线路导、地线施工的爆破压接方法为例,介绍了具体的使用过程.     

在MDCAD中利用AutoCAD进行图幅自动接边

介绍了在MDCAD地图数字化系统中，利用AutoCAD进行图幅自动接边的各个工序：预处理、计算机抄边、自动接边的实现方法，并提出了特殊情况下接边的处理方法。     

静态顶空-气质联用法检测葡萄酒中香气成分条件的优化

采用静态顶空（SHS）与气-质联用技术（GC-MS）测定葡萄酒中挥发性香气成分。通过单因素试验分别考察平衡温度、平衡时间、样品量和NaCl添加量对干红葡萄酒香气成分有效峰个数的影响。以有效峰个数（匹配度＞85%）为评价指标,采用正交试验优化了香气成分的检测条件。结果表明,静态顶空-气质联用检测干红葡萄酒中香气成分的最佳条件为：平衡温度55 ℃,平衡时间35 min,样品量8 mL,NaCl添加量2.4 g。在此条件下,共鉴定出干红葡萄酒中的香气成分18种,其中醇类8种、酯类9种和1种酸。     

防水透湿服装及其加工工艺探讨

防水透湿服装由于其面料集防水、透湿、防风、保暖于一体,其加工工艺与普通服装缝制工艺有很大不同.文中分析探讨了防水透湿服装所采用的面料的分类与发展趋势、独特的加工工艺及其与传统缝制工艺的比较优势.     

Efficient gene targeting in Kluyveromyces lactis

Integration of a DNA fragment in a host genome requires the action of a double-strand break (DSB) repair mechanism. Homologous recombination (HR) is initiated by binding of Rad52p to DNA ends and results in targeted integration. Binding of the Ku heterodimer (Ku70p/Ku80p) results in random integration via non-homologous end joining (NHEJ). In contrast to Saccharomyces cerevisiae, the budding yeast Kluyveromyces lactis shows variable, but in general low, gene targeting efficiency. To study and to improve gene targeting efficiency, K. lactis has been used as a model. The KlRAD51, KlRAD52 and KlKU80 genes have been isolated and deletion mutants for these genes have been constructed. Efficiency of gene targeting was determined at the KlADE2 locus using targeting constructs with different lengths of homologous flanking sequences. In wild-type K. lactis, the gene targeting efficiency ranged from 0% with 50 to 88% with 600 bp flanks. The Klku80 mutant, however, showed >97% gene targeting efficiency independently of the size of the homologous flanks. These results demonstrate that deletion of the NHEJ mechanism results in a higher gene targeting efficiency. Furthermore, increased gene targeting efficiency was achieved by the transformation of wild-type K. lactis with the KlADE2 deletion construct in the presence of excess small DNA fragments. Using this method, PCR-generated deletion constructs containing only 50 bp of homologous flanking sequences resulted in efficient targeted gene replacement.     

SHS-GC-MS分析黄酒中的挥发性风味物质

采用自动静态顶空进样技术,结合气质联用对黄酒中的挥发性风味物质进行分析.通过单因素水平实验得到优化的顶空条件:在10mL顶空瓶中加入样品5mL,NaC1 2.0g,60℃萃取30min.通过GC-MS分析,初步确定了26种风味成分,其中大部分为酯类和醇类.