小截面送料双频电磁成形的试验研究

研究了金属熔体的小截面送料双频电磁成形过程。结果表明：屏蔽罩能够调节成形感应圈内的磁场分布，使成形感应圈内的熔体处于合理状态；两感应圈间必须保持一定距离，使预热感应圈的磁场不影响成形感应圈的磁场分布，利于成形稳定；在其他条件一定的情况下，有一适合的抽拉速度和电源功率匹配；并获得了表面质量良好的耐热不锈钢样件。     

Flakes of natural carbyne in a diamond mine

Flakes of natural carbyne were found in Liao-Ning diamond mine, China, and examined by HRTEM, XRD and EDX. Lattice fringes and clear SAD patterns were obtained. The interlayer spacings obtained with SAD were in good agreement with those determined on the powders found in Ries crater meteorite by X-ray diffraction. However, they are different in color and shape, the one found in China being black and flaky, but the one in Ries crater meteorite being silver-white and particulate. It was assumed that carbyne might be stabilized by the intercalation of either Si or Fe in nature.     

多声路超声波流量计在引水明渠中的流量测量分析

介绍了多声路超声波流量计在明渠中的流量测量原理,并通过多声路时差式超声波流量计在引水明渠上的实例应用对影响流量测量的误差源进行了具体的分析。     

煤化工专用黑水阀阀座流通性能研究

介绍了一种煤化工专用黑水阀的结构构成,并提出进行该型号阀门流通性能研究的重要性。建立流道三维模型,应用CFD有限元分析软件,模拟黑水阀内部流场分布情况,分析可视化结果,确定阀座/阀芯易损位置。分别对不同阀座渐扩角时模型进行仿真模拟,得到阀门进、出口压力值,并依此计算Cv值大小,拟合流量系数曲线,提出阀门在实现最大介质流通时阀座渐扩角范围,为阀门设计提供重要的理论参考。     

Enabling customers engagement and collaboration for small and medium-sized enterprises in ubiquitous multi-channel ecosystems

Over the last few years, we have encountered an exponential growth in online communication opportunities. Organizations have more and more ways to connect and engage with their current or future customers. The existence of more opportunities in connecting to people can be both an enabler and a burden. Being present at a multitude of different channels requires the effective management of a very large number of adapted contents, formats, and interaction patterns fulfilling the communication and cooperation needs of distributed target groups. In this respect, we integrate existing fragmented communication and monitoring approaches into a full-fledged communication model as a basis for an adequate engagement approach. We describe applications of our approach in both the eTourism and manufacturing domain. In this paper, we introduce an approach that will enable communication, collaboration and value exchange of users through a multitude of online interaction possibilities based on the use of semantic technology. Finally, we also compare our approach with existing solutions with respect to the identified challenges in this subject.     

Gel-size dependence of temperature-induced microphase separation in weakly-charged polymer gels

The gel-size dependence of microphase separation in weakly-charged gels of N-isopropylacrylamide (NIPA) and 1-vinylimidazole (VI) copolymers has been investigated using swelling measurement, small-angle neutron scattering (SANS), and dynamic and static light scattering (DLS/SLS). It is known that weakly-charged polymer gels undergo microphase separation in a poor solvent as a result of competing interactions involving hydrophobic attraction versus electrostatic repulsion. The microphase separation is characterized by a scattering maximum in SANS intensity functions of which Bragg spacing, Λ, is around 20-30 nm. However, when gel size was reduced to the order of Λ, no microphase separation was observed. Instead, a typical scattering of isolated spherical particles was clearly observed. On the basis of the experimental evidence, we conclude that microphase separation has its own wavelength independent of gel size, and nanometer-order gels, i.e., nanogels, do not undergo microphase separation.     

Morphology, structure and properties of a poly(1-butene)/montmorillonite nanocomposite

A specifically formulated nanocomposite based on isotactic poly(1-butene) (PB) and montmorillonite was studied, by wide angle X-ray diffraction (WAXD), small angle X-ray scattering (SAXS), transmission electron microscopy (TEM) and polarized light optical microscopy, investigating the polymorphism of the polymer, and examining the interaction between PB and the silicate. Montmorillonite was found to disrupt the ordered morphology of the polymer, determining a dramatic increase in the rate of the II→I phase transition. Interaction between polymer and clay was studied by TEM and SAXS also under a quantitative point of view. A significant enhancement of physical-mechanical properties was observed, even though exfoliation did not occur, but just a slight intercalation and a reduction in the size of tactoids.     

新疆加甫沙尔苏地区中酸性小岩体型矿化蚀变遥感异常提取与找矿

中酸性小岩体的内部及附近的围岩中常形成与岩浆岩体有关的大型、超大型矿床,已成为找矿工作的一个重点方向。由于地质工作程度的限制,中酸性小岩体易被遗漏,严重制约了该类型矿化的发现。在新疆西准噶尔达尔布特断裂带下盘加甫沙尔苏地区找矿工作中,通过综合分析,提出了以遥感手段为主导的中酸性小岩体型矿化找矿模型:利用ASTER数据,通过图像增强处理、图像解译识别中酸性小岩体并提取蚀变遥感异常,结合地质、化探信息综合分析后确定重点检查区域。野外检查发现了加甫沙尔苏斑岩型钼矿化点,证实了该方法的有效性。该方法可以为西部地区中酸性小岩体型矿产资源勘查提供借鉴。     

毛细管SDS无胶筛分电泳测定小分子多肽相对分子质量

目的建立快速毛细管SDS无胶筛分电泳法(SDS-NGS),测定小分子多肽相对分子质量。方法涂层毛细管(管长30cm,内径100μm);分离电压为9kV(300V/cm),分离温度为20℃;检测波长为214nm,检测时间为18min;所用SDS-多肽相对分子质量标准范围为2 512~16 949;以橙G(OG)为内标参照物。结果在相对分子质量2512~16949范围内,多肽相对分子质量的对数与其相对迁移率具有良好的线性关系(r=0.996);应用该方法测定了重组人奈西立肽、重组人表皮生长因子、虎纹镇痛肽、重组人心钠肽4种重组小分子多肽的相对分子质量,所测结果变异系数CV均小于3%。结论毛细管SDS无胶筛分电泳方便快速,灵敏度高,重现性好,结果准确,可作为小分子多肽相对分子质量的检测方法。     

Quantitative analysis of small angle neutron scattering data from montmorillonite dispersions

A new model is presented which can describe quantitatively the small angle neutron scattering from montmorillonite-type clay dispersions and polymer-clay nanocomposites. The model is shown to be able to describe well the data from a series of dilute montmorillonite in water dispersions in which the deuterium content of the water phase is varied. The fits combined with information from other techniques suggest strongly that H-D exchange occurs in the montmorillonite-water dispersions. Deviations from Q⁻² behaviour often observed experimentally for clay dispersions are convincingly explained by the presence of a small proportion of tactoids.