铸铁热分析用试样新型激冷剂的实验研究

从冷却曲线上相变段倾角最小原则出发，研究了新型激冷剂的配比与热分析法检测铸铁成分精度的关系，实验结果表明，能使相变段倾角最小的成分配比，也能提高对铸铁成分的热分析和检测精度。     

Preparation of polyimide-epoxy composites

The formation of a three dimensional network of crosslinked epoxy leads all unmodified epoxies to have inherent brittleness and relatively low degradation temperatures. Polyimides, on the other hand, are widely used for applications that require high degrees of flexibility and thermal resistance. Here, we have focused on the preparation of epoxy systems cured with polyamic acids instead of traditional amino-group-containing hardening agents. The cure behavior and potential reaction mechanisms of EPON 828 resin and polyamic acid mixtures were evaluated by DSC and TGA. Thermal analysis showed a complex reaction sequence taking place in the mixture and also determined the extent of reaction of the polyamic acid with itself and the competitive reaction of the polyamic acid with the epoxy. The compositions of the mixtures were varied to see the dependence of the cure behavior on component concentrations. Solutions of the two components did not phase separate and also phase separation was not apparent either optically or microscopically in the cured samples. This phase behavior was attributed to a unique in situ reaction. A novel solvent system for the polyamic acid precursor was also used.     

聚氨酯泡沫夹克管生产材料的代用

介绍一种用于生产聚氨酯泡沫夹克管保温层的新材料聚酯聚醚，报道选用这种材料生产泡沫夹克管的工艺及工要工艺参数和产品达到的技术指标及现场应用情况。     

水泥膨胀珍珠岩砂浆的保温试验研究与应用

荆江分洪北闸加固工程２号护坦（斜面）混凝土的保温层采用了水泥膨胀珍珠岩砂浆，并对这种材料的保温效果进行了试验研究。试验表明：水泥膨胀珍珠岩砂浆降低最高温差，减小内表温差，缩小表温变幅和防止混凝土表面裂缝效果显著。在北闸２号护坦混凝土表面铺设１万平方米保温层，获得良好效果。     

固体火箭发动机喷管用烧蚀隔热材料研究进展

介绍了固体火箭发动机喷管用烧蚀隔热材料的研究进展，喷管受热分析，指出了先进复合材料的发展趋势，提出碳／酚醛复合材料在制造低成本的发动机喷管中仍有重大使用价值。     

节理岩体参数对围岩破损区影响的敏感性分析

本文针对黄河拉西瓦地下水电站工程，对节理岩体诸参数对围岩破损区范围的影响进行了敏感性分析。指出了主要敏感参数，对这些参数影响围岩破损区的趋势和可能程度进行了讨论，并对勘察和施工提出了一些意见。     

超薄SiO2层的热生长

隧道小孔中超薄ＳｉＯ２的生长是ＥＥＰＲＯＭ电路制造的关键工艺之一。采用ＳＵＰＲＥＭ－Ⅲ工艺模拟程序对超薄ＳｉＯ２的热生长进行了工艺模拟，经过大量的工艺实验及优化，确定了超薄ＳｉＯ２的最佳生长条件，生长出的ＳｉＯ２性能良好，完全可满足ＥＥＰＲＯＭ研制的要求。     

Characterization and modification of fillers for paints and coatings

This paper highlights the possibility of inverse gas chromatography for the surface characterization of common fillers (CaCO₃, talc, SiO₂,) for paints and coatings. Divided solids are described, on the one hand, by the dispersive component of their surface energy and, on the other, by a specific parameter indicating their acid-base interaction potential. The role of the surface morphology at a molecular level is also examined. It is demonstrated that steric effects play an important role in the adsorption of probes on lamellar solids like talc. The consequences of surface treatments as well as examples of practical applications are also reported.     

Improvement of the optical properties of electrodeposited CuInSe2 thin films by thermal and chemical treatments

Cu, In and Se have been codeposited in thin films by potentiostatic one-step electrodeposition. The as-deposited material has shown direct optical transitions attributable to the CuInSe₂ semiconductor, but also additional absorption corresponding to another semimetallic phase. The secondary phases are selenium and copper selenide compounds which have been determined by composition measurements. In order to eliminate the semimetallic phases and to improve the semiconductor behaviour of the electrodeposited material, thermal and chemical treatments have been performed. After heat-treatment of the samples at 400°C in flowing argon, elemental selenium loss has been detected together with an enhancement of the allowed direct optical transition. The subsequent chemical etching of the layers in a KCN solution has showed to be successful in eliminating the copper selenide phases which were responsible of the remaining sub-bandgap absorption.     

搅拌工艺对半固态Y112铝合金组织及性能的影响

采用自行研制的机械搅拌装置,研究了不同工艺参数对半固态Y112铝合金组织及性能的影响.研究表明,搅拌温度越高,搅拌速度越大,固相颗粒越细小、均匀和圆整,其抗拉强度与伸长率越高;但温度太高,固相颗粒会熔化,抗拉强度及伸长率也降低;随搅拌时间的延长,固相颗粒先变得细小、均匀和圆整,然后长大,抗拉强度、伸长率先升高后降低.