一种碳－碳复合材料长寿命防氧化涂层的失效机制

用液相法联合ＣＶＤ法和硅化法制备了一种碳－碳复合材料复合梯度涂层，在此基础上对这种涂层在氧化过程中的失效机制进行了研究．结果表明：氧化层与液相层界面反应生成的气相产物是涂层失效的根本原因界面上气泡的不均匀形核、长大和破裂导致涂层表面出现孔洞．孔洞处气泡优先形核、长大和破裂并发展成为缺陷而使涂层失效     

The effect of pre-wetting on dynamic contact angles

A roll-coating experimental system is used to study the effect of pre-wetting on dynamic contact angles, the interfacial displacement depth, and the associated phenomenon of air entrainment. The system consists of a roll, which is horizontally rotating in a liquid pool. The dynamic contact angle is recorded by a macrophotography system. The test liquids are glycerol solutions with viscosities in the range 104 < μ < 748 mPa · s. The value of (μV/ρg)^0.5 is taken as the characteristic length to be used in the dimensionless relationships which correlate experimental measurements. The effect of base layer entry angle into the liquid pool on the dynamic contact angles and other flow parameters is studied. Comparison is made with measurements in dry tape-coating and other pre-wet roll–coating systems.     

n-Al2O3/Ni复合镀层的组织与滑动磨损性能研究

用电刷镀技术制得了镍基n-Al2O3复合镀层，并对镀层的滑动磨损性能进行了试验研究。纳米复合镀层的表面形貌比较细腻，镀层中纳米粒子分布均匀，与基质金属结合紧密。镀层显微硬度达到HV700，比快速镍镀层提高约40％。滑动磨损试验结果表明，随着纳米粒子含量的增大，镀层的耐磨性提高，摩擦系数也呈增大趋势；但当镀层中n-Al2O3粒子的超过2.56%(质量分数）时，镀层的耐磨性显著下降。纳米复合镀层的磨损机制以疲劳磨损为主，而快速镍底层以粘着磨损为主。     

石英晶体监控法镀制高精度光学薄膜

讨论了石英晶体监控法在光学薄膜镀制过程中的应用原理。通过与常规的光学监控法镀制的膜层相比较．证实了石英晶体监控法有助于提高光学薄膜的光学品质。试验表明所镀膜层的光学性能优异，在光通信和激光器等领域具有广阔的应用前景。     

Al2O3基耐磨陶瓷涂层的燃烧合成与应用

介绍了燃烧合成表面涂层技术的基本原理 ,开发了相应的制备工艺 ,并在此基础上研制了内覆陶瓷涂层的复合钢管、弯管及弯头。陶瓷涂层主要由α Al2 O3相、部分FeO·Al2 O3相和 3Al2 O3·2SiO2 相组成 ,采用添加剂可以有效提高熔体的流动性 ,使陶瓷的凝固和结晶过程得到进一步控制 ,有助于减少孔隙 ,提高陶瓷涂层的致密度。现场应用试验表明 ,涂层具有较好的耐磨性能 ,可使设备的使用寿命大为延长     

镁合金表面喷铝防腐蚀层的微观组织分析

在AZ91D镁合金表面热喷铝，用以提高其表面的耐腐蚀性能。采用SEM，EPMA等方法对AZ91D表面喷铝扩散层的组织进行了仔细的观察与分析，发现在防腐蚀层上有大量的Mg17Al12相存在，且呈决状及非连续片状分布。经显微硬度测定，喷铝层硬度较镁合金基体高；腐蚀后这种相凸出于基体，比镁合金基体有较好的耐腐蚀性能。     

The use of natural essential oils as antimicrobial solutions in paper packaging. Part II

We have assessed the antimicrobial, vapor-phase activity of the following natural essential oils (EOs) when used in paraffin-based “active coatings” for paper packaging materials intended to come into contact with foods: clove (Sygzium aromaticum), cinnamon (Cinnamomum zeylanicum), and oregano (Origanum vulgare) EOs, and cinnamaldehyde-enriched cinnamon EO. To our knowledge, this is the first time that such an approach has been presented for consideration by the scientific community.     

Thermal analysis of a ceramic coating diesel engine piston using 3-D finite element method

In this study, firstly, thermal analyses are investigated on a conventional (uncoated) diesel piston, made of aluminum silicon alloy and steel. Secondly, thermal analyses are performed on pistons, coated with MgO-ZrO₂ material by means of using a commercial code, namely ANSYS. Finally, the results of four different pistons are compared with each other. The effects of coatings on the thermal behaviors of the pistons are investigated. It has been shown that the maximum surface temperature of the coated piston with material which has low thermal conductivity is improved approximately 48% for the AlSi alloy and 35% for the steel.     

Corrosion Behavior of a Sputtered K38G Nanocrystalline Coating with a Solid NaCl Deposit in Wet Oxygen at 600 to 700°C

A nanocrystalline coating of K38G alloy was obtained by means of magnetron sputtering. The corrosion behavior of cast K38G alloy and its sputtered nanocrystalline coating with a solid NaCl deposit in dry air or wet oxygen at 600 and 700°C have been studied and compared. The results indicated that the mass gain of the coating is higher than that of the cast alloy at 600 and 700°C. Therefore, nanocrystallization reduced the corrosion resistance at these temperatures. Furthermore, the mass gains of the coating and the cast alloy with a NaCl deposit in wet oxygen were less than that with a NaCl deposit in dry air. The relevant corrosion mechanisms are discussed.     

Oxidation behavior of silicide coating on Ti3SiC2-based ceramic

A silicide coating was prepared on Ti₃SiC₂-based ceramic by pack cementation to improve the oxidation resistance of Ti₃SiC₂, which is a technologically important material for high temperature applications. The microstructure, phase composition and oxidation resistance of the coated sample were investigated. The results demonstrated that the silicide coating was mainly composed of TiSi₂ and SiC. A single layer of a mixture of SiO₂ and TiO₂ was formed on the surface of the coated sample during isothermal oxidation at 1100 °C and 1200 °C for 20h. Compared to Ti₃SiC₂, the parabolic rate constant of silicide coated Ti₃SiC₂ decreased by 2~3 orders of magnitude. Furthermore, the coated sample showed much better cyclic oxidation resistance than Ti₃SiC₂ during the cyclic oxidation at 1100 °C for 400 times. However, during the preparation of the coating, a number of fine cracks formed in the outer layer of the coating. When these cracks penetrated the whole coating during the cyclic oxidation, the oxidation rate was accelerated, which degraded the oxidation resistance. Electronic Publication