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51.
针对W9Cr3M04V轧制成品材低倍碳化物剥落的形成原因分析,得出一次碳化物颗粒粗大、在1/4D至中心区域聚集是导致低倍热酸浸试验碳化物剥落的主因;由此进行冶炼过程中注速(锭形)、浇注温度选择对比工艺试验,得出在原有冶炼+轧制的工艺基础上选用2.2t锭、降低浇注温度(1489℃)能有效改善一次碳化物颗粒大小和聚集程度,进而有效降低低倍碳化物剥落倾向。 相似文献
52.
In this paper we propose a new method to estimate parameters of a dynamical system from observation data on the basis of a neural network collocation method. We construct an object function consisting of squared residuals of dynamical model equations at collocation points and squared deviations of the observations from their corresponding computed values. The neural network is then trained by optimizing the object function.The proposed method is demonstrated by performing several numerical experiments for the optimal estimates of parameters for two different nonlinear systems. Firstly, we consider the weakly and highly nonlinear cases of the Lorenz model and apply the method to estimate the optimum values of parameters for the two cases under various conditions. Then we apply it to estimate the parameters of one-dimensional oscillator with nonlinear damping and restoring terms representing the nonlinear ship roll motion under various conditions. Satisfactory results have been obtained for both the problems. 相似文献
53.
Synthesis and characterization of acidic properties of Al-SBA-15 materials with varying Si/Al ratios
G. Muthu Kumaran Shelu Garg Kapil Soni Manoj Kumar J.K. Gupta L.D. Sharma K.S. Rama Rao G. Murali Dhar 《Microporous and mesoporous materials》2008,114(1-3):103-109
Al-SBA-15 of varying Si/Al ratios in the range 11.4–78.4 was synthesized using tri-block copolymer P123. The calcined materials were examined by XRD, pore size distribution, surface area, 27Al NMR spectroscopy. The acidity and acid strength distribution were studied using microcalorimetric adsorption of NH3. The acidic properties were also examined by cumene cracking reaction as a function of Si/Al ratios. Systematic variation of acidity and activity was observed as a function of Si/Al ratio. The initial heats of NH3 adsorption correlated well with activity indicate that acid sites with ΔH > 100 kJ/mole is responsible for cumene cracking activity. Linear correlations were obtained with total acidity and cumene cracking activities. The tetrahedral aluminum was found to be responsible for the observed acidities and catalytic activities. 相似文献
54.
Mesoporous GaSBA-15 molecular sieves with different nSi/nGa ratios have been directly synthesized using Pluronic 123 triblock polymer as a structure-directing agent by pH-adjusting method. The mesoporous materials have been characterized using ICP-AES, XRD, N2 adsorption, 71Ga-MAS NMR, SEM and TEM. ICP-AES studies show a high amount of gallium incorporation on the silica pore walls. The structural and textural properties of calcined GaSBA-15 are characterized by XRD and N2 adsorption. 71Ga MAS NMR results demonstrate that a high amount of tetrahedral-gallium could be substituted for Si in the framework of SBA-15. TEM and FE-SEM images show the uniform pore diameter and rope-like hexagonal mesoporous structure of GaSBA-15. These GaSBA-15 materials have been used as catalysts for vapour-phase t-butylation of 1,2-dihydroxybenzene (DHB) for selective synthesis of 4-t-butylcatechol (4-TBC) under different reaction conditions. GaSBA-15(10) gave the highest 93.2% conversion of DHB and 95.7% selectivity of 4-TBC as compared with other GaSBA-15 catalysts. 相似文献
55.
基于试样高温高压釜充氢方法 ,研究了氢对 2 2 5Cr 1Mo压力容器用钢力学性能的影响。对充氢前后的试样进行了拉伸和CVN冲击试验 ,结果表明 ,氢对 2 2 5Cr 1Mo钢的拉伸力学性能和冲击韧性影响不显著。 相似文献
56.
介绍了用CO_2堆焊35CrMo钢钻井泵阀箱密封面磨损修复工作,通过试验表明,采用Φ1.2mm的H08Mn2Si焊丝,以短路过渡CO_2焊法施焊,可以获得致密、耐磨的堆焊金属层。该法已成功地用于生产,取得了良好的经济效益。 相似文献
57.
Human urine - Chemical composition and fertilizer use efficiency 总被引:2,自引:0,他引:2
Stored human urine had pH values of 8.9 and was composed of eight main ionic species (> 0.1 meq L–1), the cations Na, K, NH4, Ca and the anions, Cl, SO4, PO4 and HCO3. Nitrogen was mainly (> 90%) present as ammoniacal N, with ammonium bicarbonate being the dominant compound. Urea and urate decomposed during storage. Heavy metal concentrations in urine samples were low compared with other organic fertilizers, but copper, mercury, nickel and zinc were 10–500 times higher in urine than in precipitation and surface waters. In a pot experiment with15N labelled human urine, higher gaseous losses and lower crop uptake (barley) of urine N than of labelled ammonium nitrate were found. Phosphorus present in urine was utilized at a higher rate than soluble phosphate, showing that urine P is at least as available to crops as soluble P fertilizers. 相似文献
58.
本试验研究了ZrO2与40Cr钢在加入缓冲层前后的钎焊连接,结果表明:插入缓冲层Cu和Ti可以提高接头强度。对每一种缓冲层,存在一最佳厚度,对应的钎焊强度最大。此最佳厚度对Cu为0.4mm左右,对Ti为1mm左右。作者认为这是由缓冲层的力学性能和热膨胀系数对残余应力释放产生的两种相反影响而造成的。钎焊时,缓冲层Cu和Ti向钎料中均有程度不同的溶解,但不影响钎料对ZrO2的浸润和反应结合。ZrO2-40Cr钢连接的所有接头均断在陶瓷的近缝区,其断裂方式有三种。 相似文献
59.
40Cr钢试样经不同热处理后在空气中用CO2连续激光束进行辐照,以穆斯堡尔谱学研究试样在辐照后的组织结构变化。试验结果表明,调质预处理后再进行激光辐照的试样,不仅残作产奥氏体含量较低,而且其中碳的含量最低。 相似文献
60.
F. H. Sam Froes 《Powder Metallurgy and Metal Ceramics》2007,46(5-6):303-310
The approaches to production of titanium powder injection molded parts are reviewed. Historically, oxygen levels have been
too high for structural use (particularly with the Ti-6Al-4V alloy). However, recent advances in starting powders, binders
and sintering facilities now allow oxygen levels in the Ti-6Al-4V alloy to be controlled to about 0.2 wt.% oxygen. This should
result in significant expansion of the titanium PIM market place into aerospace, automobiles, surgical instruments, dentistry,
communication devices (such as computers and cell phones), knives and guns.
__________
Translated from Poroshkovaya Metallurgiya, Vol. 46, No. 5–6 (455), pp. 118–125, 2007. 相似文献