一种制备磁性粉末的新技术--均匀颗粒成型法

采用均匀颗粒成型法（Uniform Dropler Spray-UDS）制备Fe基合金粉末，该方法制备的颗粒粒度分布均匀，性能一致，大大优于传统的粉末制备方法（如破碎法、气雾化），具有广阔的应用前景。本文分析了粉末制备过程中颗粒尺寸的影响因素，结果表明：颗粒的大小主要取决于坩埚底部小孔、坩埚内外气体压强差以及振荡频率三个独立变量。     

SSRF储存环预研制铝合金真空室的机械加工

上海同步辐射装置（SSRF）储存环铝合金超高真空室已研制成功，该机加真空室的尺寸大、尺寸精度、形位公差及粗糙度要求极高，不同于常规的大型超高真空室。在预研件加工中，成功地解决了一系列问题，如光洁度提高困难，加工成型后变形大；加工尺寸和精度受环境温度影响较大等。本文详细阐述了储存环真空室材料和热处理状态的选择依据，为了保证尺寸精度和形位公差所采取的工艺措施，分析了粗糙度的形成机理和影响因素，从刀具材料、几何角度、切削参数、冷却液选型等多方面提出了解决办法。     

高强铝合金断裂韧性的研究现状及展望

通过对三种裂纹模式的概述，引出了铝合金断裂韧性的概念及断裂判据，重点评述了影响高强铝合金断裂韧性的内在与外在因素，以及断裂韧性与其它力学性能间的关系，最后提出了几个在今后的研究及应用中需要重点解决的问题。     

Isothermal Gas Forming of Mg Alloy AZ31 Sheet

There have been reports on sheet forming of Mg alloy in industry via the punch and die method;this paper is probably the first formal one for studying the sheet formability of AZ31 employing pressurized gas to press the sheet into a female die cavity at various elevated temperatures.The results indicate it is feasible to form a rectangular box via pressurized gas from extruded sheets of 0.5 and 1.7 mm thick.The formed box has 1:2 depth over width ratio,which should be large enough when dealing with realistic industrial sheet forming parts.Presently,forming a sheet of 0.5 mm thick is considered a technical challenge by industry,and it is conquered as demonstrated in this paper.Gas forming technique applied to Mg alloy is unprecedented and shows potential for industrial utilization.     

Influence of Ti Powder Characteristics on Combustion Synthesis of Porous NiTi Alloy

Porous NiTi shape memory alloy (SMA) is a novel biomedical material used for human hard tissue implant .The influence of elemental titanium powder characteristics such as powder morphology, particle size and specific surface area( SSA) on the minimal ignition temperature ,combustion temperature and final product of porous Ni-Ti SMA fabricated by combustion synthesis method was investigated in this paper by scanning electron microscopy (SEM) and laser diffraction.The preliminary data indicated that the titanium powder characteristics had a strong effect on combustion synthesis of porous NiTi SMA.     

宽带激光熔覆WCP/Ni基合金梯度复合涂层组织与摩擦磨损特性

研究了铸造WC_P/Ni基合金梯度复合涂层组织与摩擦磨损特性。结果表明,梯度复合涂层与基材实现了良好的冶金结合,涂层内有γ-Ni枝晶组织,γ-Ni＋M₂₃C 6共晶组织以及凝固结晶析出的M₆C、M₂₃C₆、M₇C₃等块状或条状组织;随着铸造WC_P体积分数的增加,复合涂层摩擦系数减小,耐磨性增加。19-4试样的耐磨性最高值为4.61,是基材的3倍以上。梯度涂层的磨损机理为磨粒磨损与粘着磨损的复合作用。     

Assessment of different techniques for quantification of α-Al(FeMn)Si and β-AlFeSi intermetallics in AA 6xxx alloys

During homogenisation of AA 6xxx aluminium alloys, the platelike β-AlFeSi intermetallic phase will transform to a less Si-rich and more spheroidised α-Al(FeMn)Si phase which is more favourable for extrusion. In this study, several quantitative methods, which determine the relative volume fraction of α-Al(FeMn)Si and β-AlFeSi, are compared and an assessment of each method is made. The methods used are optical microscopy, scanning electron microscopy (SEM) in combination with electron dispersive X-ray (EDX) using polished samples, and X-ray diffraction (XRD) on intermetallics, extracted through selective dissolution of the Al matrix. The highest accuracy is obtained by using SEM/EDX analysis and applying two criteria.     

单晶钛酸铋纳米片的XPS和Raman特性

以Bi（NO3）3·5H2O和Ti（OC4H9）4为原料，NaOH为矿化剂，采用水热法制备了形貌规则的单晶Bi4Ti3O12纳米片。X射线衍射（XRD）结果表明，所合成的产物为正交相层状钙钛矿结构的Bi4Ti3O12。场发射扫描电子显微镜（FESEM）研究显示：样品是由大量边缘尺寸接近200nm，厚度约为15nm的片状结构组成。利用X射线光电子能谱（XPS）研究产物的化学组分和价态分布。室温拉曼光谱研究表明，Bi4Ti3O12纳米片的声子寿命和热稳定性低于相应的块体材料。     

Surface Hardening of High-Strength Low Alloy Steels (HSLA) Dual-Phase Steels by Ball Burnishing Using Factorial Design

Burnishing is used increasingly as a finishing operation which gives additional advantages such as increased hardness, fatigue strength, and wear resistance. Experimental work based on 3⁴ factorial design was carried out to establish the effects of ball burnishing parameters on the surface hardness of high-strength low alloy steels (HSLA) dual-phase (DP) steel specimens. Statistical analysis of the results shows that the speed, feed, lubricant and ball diameter have significant effect on surface hardness.     

开发稀土铝合金镀层油管的设想

叙述了热浸镀铝钢的镀层组织、耐蚀性能及研究进展，介绍了稀土对铝合金耐蚀性的影响作用，在此基础上提出了开发稀土铝合金镀层油管的设想。