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61.
S.K. Lee D.‐H. Hwang B.‐J. Jung N.S. Cho J. Lee J.‐D. Lee H.‐K. Shim 《Advanced functional materials》2005,15(10):1647-1655
By using Ni0‐mediated polymerization, we have systematically synthesized a series of fluorene‐based copolymers composed of blue‐, green‐, and red‐light‐emitting comonomers with a view to producing polymers with white‐light emission. 2,7‐Dibromo‐9,9‐dihexylfluorene, {4‐(2‐[2,5‐dibromo‐4‐{2‐(4‐diphenylamino‐phenyl)‐vinyl}‐phenyl]‐vinyl)‐phenyl}‐diphenylamine (DTPA), and 2‐{2‐(2‐[4‐{bis(4‐bromo‐phenyl)amino}‐phenyl]‐vinyl)‐6‐tert‐butyl‐pyran‐4‐ylidene}‐malononitrile (TPDCM) were used as the blue‐, green‐, and red‐light‐emitting comonomers, respectively. It was found that the emission spectra of the resulting copolymers could easily be tuned by varying their DTPA and TPDCM content. Thus with the appropriate red/green/blue (RGB) unit ratio, we were able to obtain white‐light emission from these copolymers. A white‐light‐emitting diode using the polyfluorene copolymer containing 3 % green‐emitting DTPA and 2 % red‐emitting TPDCM (PG3R2) with a structure of indium tin oxide/poly(3,4‐ethylenedioxythiophene):poly(styrene sulfonic acid)/PG3R2/Ca/Al was found to exhibit a maximum brightness of 820 cd m–2 at 11 V with Commission Internationale de L'Eclairage (CIE) coordinates of (0.33,0.35), which are close to the standard CIE coordinates for white‐light emission (0.33,0.33). 相似文献
62.
63.
采用自行研制的LB自动提膜装置,制备出大面积(10×8cm2)、高质量的PMMA超薄抗蚀剂膜,并将其用于高分辨率铬掩模版的研制。通过电子束曝光,湿法蚀刻,制作了分辨率优于0.5μm,特征线宽0.38μm的4(100mm)铬掩模版。 相似文献
64.
冷库地坪防冻臌机械通风的传热计算 总被引:1,自引:0,他引:1
设计手册中关于使用机械通风防止冷库地坪冻臌的参数(风道直径、间距及长度)仅是推荐值,它忽略了地坪结构、土壤温度和外界空气温度对通风系统节能的影响,因而造成地基土壤的热损失和冷库负荷的增大。从冷库节能和冷库建筑安全使用出发,对采用机械通风防止地坪冻臌进行了传热分析,提出了在传热计算中参数的合理选择和通风系统的设计方法。 相似文献
65.
Atomic layer epitaxy or ALE has proven to be useful for the growth of epitaxial layers of high uniformity, good quality, and
well-controlled thickness. In this study, we have carried out in-situ monitoring during the atmospheric pressure ALE of CdTe on GaAs (100) substrates using spectroscopic ellipsometry (SE). The
susceptor temperature, reactant partial pressures, as well as the flow and flush duration for each precursor are crucial process
variables for ALE growth. Growth was carried out for 20–25 cycles under different sets of these process conditions during
the experiment and in-situ SE was used to verify the presence of layer-by-layer growth, which enabled the quick determination of the process window.
We observed ALE growth of CdTe at 300°C, supporting the explanation that the growth of CdTe occurs via a surface catalyzed
decomposition of the Te precursor di-isopropyltelluride (DIPTe). Investigation of ALE mode growth behavior for different susceptor
temperatures and DIPTe flush times indicated that the growth was limited by competition between desorption and reaction of
the adsorbed DIPTe species on the Cd terminated surface. 相似文献
66.
简介水泥搅拌桩的支护机理,以西涌泵站为例介绍采用格栅式水泥搅拌桩作支护结构的设计及计算方法,指出该技术能较好地解决软湿粘性土地区枢纽深基础开挖问题. 相似文献
67.
Deposition of zinc oxide films from aqueous solutions containing complex Zn2+ ions on soda-lime substrates were studied by two-stage chemical deposition (TSCD) process. It was shown that the film thickness can be controlled by the number of dipping stages. Nano-layers were produced with less than nine times dipping stages. Greater dipping numbers resulted in film thickness exceeding 100 nm. The growth rate obeyed double-stage zeroth order with respect to the concentration and first order with respect to the temperature. This rate was proportional to the difference between the temperature of the hot water and the substrate. Overall activation energy of 17.20 ± 0.42 kJ mol−1 and frequency factor of 2.81 ± 0.07 μm s−1 was determined for ZnO deposition. These values were attributed to two resistances. One resistance corresponded with film heat transfer mechanism. The other was attributed to species attachment to the solid substrate. A modification to the diffuse-interface kinetic model was devised for explanation of the latter. EDAX (electron dispersive elemental analysis), XRD (X-ray diffraction) and SEM (scanning electron microscopy) were used to characterize the layer formed. These methods showed that the product consisted solely of pure elliptical ZnO grains. 相似文献
68.
分层注水管柱有效率低一直是困扰临盘油田开发生产的一大难题。针对这一现状,在分析油藏结构、施工工艺和现场资料的基础上,分析了影响分层注水井管柱有效率的因素,阐述了封隔器、工艺操作、管枉自身及温度等制约分层注水管柱有效率提高的原因,并提出了相应的对策和措施。 相似文献
69.
The evolution of surface defects during shape rolling of high‐speed steel billets is studied using longitudinal surface defects prepared by machining and welding. The reduction of the defects during rolling in a production mill is compared to the total area reduction of the billets. Samples are collected after pass 4, 6, 8, 14, 19 and the final pass, 28, representing the finished 5.5mm wire. By inspecting the cross sections, the rotation of the billets from pass to pass is evaluated. Results from FE simulations on solid billets are compared to the experimental results. Generally, simulations predict less reduction than observed experimentally. In most cases cracks reduce most effectively followed by carbon steel welds and stainless steel welds. 相似文献
70.
The authors of this paper investigated the influence of esters of rapeseed oil fatty acids on the lubricating properties of
mineral lubricants containing chosen AW/EP additives. Methyl esters, ethylene glycol esters, and glycerol esters as well as
some commercial AW/EP packages based on zinc dialkyldithiophosphate, S–P organic compounds, and sulphurized esters of fatty
acids were tested. The tribological tests were carried out with the use of a four-ball machine. Antiwear (AW) properties of
tested compositions were determined using their limiting load of wear (Goz(40)). It appears that the AW action of esters of rapeseed oil fatty acids depends on their structure. The best AW action is shown
by compositions of mineral oil lubricants containing AW/EP additives and methyl esters of rapeseed oil fatty acids. The SEM/EDS
analysis of the scar surface layer indicated that the presence of these esters in lubricants causes a change in the interaction
between AW/EP additives and the metal surface. These observations were confirmed by the XPS surface analysis. 相似文献