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81.
低翘曲玻纤增强PET复合材料的制备和性能研究 总被引:4,自引:0,他引:4
依据降低翘曲的机理,选用不同降低翘曲的方法,制备了系列翘曲玻纤增强PET复合材料,结果表明,具有较高形状对称性的填料,如滑石粉,云母粉和玻璃微珠都能不同程度地降低玻纤增强PET体系的翘曲,非晶聚合物也能有效改进该体系的翘曲性能。 相似文献
82.
The evolution of the amorphous structure of starch was characterized during the drying process by real‐time X‐ray wide‐angle scattering. The X‐ray diffractograms of injection‐molded starch show two superposed, rather broad, scattering maxima indicative of noncrystalline structures. The location of the two peaks has been associated to disordered starch single helices. A third maximum that arises upon drying the material in vacuum is associated to the scattering emerging from regions containing double helices. A model for the starch network is proposed, assuming a primary and a secondary component. The wider, temperature stable component appearing first, is correlated to the entanglement network of the melt. The narrower network component, which is created later, at lower temperature (secondary network), is explained by the formation of double helix regions that densify the wider primary network. The secondary network is increased strongly by the drying process. X‐ray experiments performed during the penetration of water, provoking a higher molecular mobility, reveal a better‐packed helical structure that becomes the precursor of a double helix crystalline formation. When temperature increases, the secondary network is dissolved and water molecules arrange themselves in better‐organized crystals as strongly bound crystal water. © 2005 Wiley Periodicals, Inc. J Appl Polym Sci 99: 1880–1886, 2006 相似文献
83.
Dielectric characterization of the α-relaxation in polyarylate (PAr) has been carried out by means of a dielectric spectroscopy technique in a frequency range of 10–30 kHz. Complementary thermally stimulated depolarization currents (TSDC) and differential scanning calorimetry d.s.c.) measurements have also been performed. The results are interpreted in terms of the standard Cole-Cole plot and Havriliak-Negami distribution for the dielectric relaxation times. Information about the temperature and frequency dependence of a.c. conductivity is also obtained from the experimental curves. However, the behaviour of the main dielectric relaxation time is deduced from the experimental data in a wide range of temperature around the glass transition. This behaviour results in close agreement with the theoretical predictions of a free-volume approach for the dielectric α-relaxation recently proposed by the authors. 相似文献
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金属铝诱导法低温制备多晶硅薄膜 总被引:4,自引:0,他引:4
以氢气稀释的硅烷(SiH4)和硼烷(B2H6)为气源,利用等离子体增强化学气相沉积法(PECVD)制备出p型a-Si薄膜.采用铝诱导晶化技术对不同厚度的铝膜对a-Si薄膜晶化的影响进行了研究.实验中发现,铝膜溅射为10 s的非晶硅薄膜样品在450℃下退火10 min后,p型a-Si结构仍为非晶态,铝膜溅射为20 s的非晶硅薄膜在450℃下退火20 min后,p型a-Si薄膜开始晶化为polySi薄膜,并且铝膜厚度越厚,则a-Si薄膜晶化程度越强. 相似文献
88.
T. S. Wilson J. P. Bearinger J. L. Herberg J. E. Marion III W. J. Wright C. L. Evans D. J. Maitland 《应用聚合物科学杂志》2007,106(1):540-551
Aliphatic urethane polymers have been synthesized and characterized, using monomers with high molecular symmetry, to form amorphous networks with very uniform supermolecular structures, which can be used as photo‐thermally actuable shape memory polymers (SMPs). The monomers used include hexamethylene diisocyanate (HDI), trimethylhexamethylenediamine (TMHDI), N,N,N′,N′‐tetrakis(hydroxypropyl)ethylenediamine (HPED), triethanolamine (TEA), and 1,3‐butanediol (BD). The new polymers were characterized by solvent extraction, NMR, XPS, UV/VIS, DSC, DMTA, and tensile testing. The resulting polymers were found to be single phase amorphous networks with very high gel fraction, excellent optical clarity, and extremely sharp single glass transitions in the range of 34–153°C. Thermomechanical testing of these materials confirms their excellent shape memory behavior, high recovery force, and low mechanical hysteresis (especially on multiple cycles), effectively behaving as ideal elastomers above Tg. We believe these materials represent a new and potentially important class of SMPs, and should be especially useful in applications such as biomedical microdevices. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci, 2007 相似文献
89.
粘结型Nd—Fe-B永磁体具有组织疏松、孔隙率高、强度低、耐热性差等特点。试验了孔隙封闭、除毛刺、边角滚光及活化除去基体氧化膜等前处理技术。研究化学镀Ni—P工艺,选择一次性化学镀Ni—P合金工艺,成功地解决了Nd—Fe-B永磁体的防腐技术问题。既简化了工艺流程,缩短了施镀时间,又降低了成本。本工艺亦适合烧结型Nd—Fe-B永磁体的防腐。 相似文献
90.
混合碱法是以熔融的无水混合碱(氢氧化钠和氢氧化钾)做为溶剂,以成本低廉的氧化物和金属无机盐作为反应物,在常压,200℃左右合成陶瓷粉体的方法.混合碱法合成微米甚至纳米结构的粉体具有成本低,温度低,粉体结构的生长可以得到有效的控制的优点,因此混合碱法是一种快速制备粉体的比较理想方法. 相似文献