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71.
介绍了用气相色谱分析叔丁醇两步氧化制甲基丙烯酸液相产物的组成,该分析方法能够分析液相产物中的醛类,酮类和酸类化合物共计9个组分,C2-C4有机酸无记忆效应,其色谱峰不拖尾,该分析方法的相对标准偏差≤8.5%,回收率在94.5%-103.7%之间,是一种快速,准确,操作简单的分析方法。 相似文献
72.
73.
We have grown thin carbon films by pulsed laser deposition and have investigated the extent to which the properties of such
films, as well as the processes responsible for these properties, are laser wavelength dependent. Films were grown by ablating
material from a graphite target onto room temperature Si(100) substrates with 1064 and 248 nm laser radiation. The films were
analyzed byin situ electron energy loss spectroscopy and byex situ Raman spectroscopy. The results indicated that films grown with 1064 nm ablation were graphitic, while those grown with 248
nm radiation were diamond-like. We have also examined the mass and kinetic energy distributions of the particles ejected from
graphite by the two laser wavelengths. The results indicated that irradiation of graphite with 1064 nm laser radiation results
in the ejection of a series of carbon cluster ions C
n
+
(1 ≤ n ≤ 30) with mean kinetic energies less than 5 eV. Ablation of graphite with 248 nm radiation results in the ejection
of primarily C
2
+
and C
3
+
with mean kinetic energies of 60 and 18 eV, respectively. These results suggest that large, low energy clusters produce graphitic
films, while small, high energy clusters produce films of diamond-like carbon. 相似文献
74.
D. E. Wetzler P. F. Aramendía M. L. Japas R. Fernández-Prini 《International Journal of Thermophysics》1998,19(1):27-42
Thermal diffusivities of supercritical CO2 and C2H6 were determined over a wide density range with a photothermal technique. The thermal lens, formed by the degradation of the absorbed light energy as heat by the sample, allows the employment of a nonequilibrium method in the critical region. Controlling the refractive-index gradient, i.e., a density gradient, perturbations can be maintained at levels where convection is negligible. An easy-to-operate setup allowed us to measure thermal diffusivities in the density ranges 5 to 20 mol·dm–3 for CO2 at 308 and 313 K and 2 to 12 mol·dm–3 for C2H6 at 308 K with a standard precision of 15%. 相似文献
75.
胜利油田污水储罐腐蚀防护方法评价 总被引:1,自引:0,他引:1
对胜利油田纯粱采油厂A3钢制生产污水(水温约60℃)储罐使用寿命过低的原因进行了实验考察。水质分析数据表明氯离子浓度高(45-48gm)是污水腐蚀性强的主要因素。A3钢在60℃污水中的腐蚀速率,由极化曲线数据计算的值大大高于失重法测定值,敞开系统中失重法测定值又高于密闭系统中测定值,挂片上出现蚀孔,说明储罐中A3钢发生了氧存在下氟离子引起的局部腐蚀(孔蚀)。元素分析结果表明.储罐阴极保护所用的牺牲阳极铝材含铁等元素量超标。牺牲阳极密封不良,在实验污水中7天后电流效率仅为2.92%,失去阴极保护能力。处于实验污水环境中的有涂层保护的A3钢.14天后出现腐蚀极化电流,表明涂层已失去完整性。要提高该采油厂及胜利油田其他采油厂污水储罐的使用寿命,必须改用合格的牺牲阳极和保护涂层材料。图3表2参7。 相似文献
76.
Aggregates of carbon black (CB) in a polymer matrix have a tendency to form a CB network. The dynamic mechanical properties of binary systems of chlorinated polyethylene (CPE) and CB or 3,9‐bis{1,1‐dimethyl‐2[β‐(3‐tert‐butyl‐4‐hydroxy‐5‐methylphenyl)propionyloxy]ethyl}‐2,4,8,10‐tetraoxaspiro[5,5]‐undecane (AO‐80) and their ternary systems were investigated. It was found that the dynamic mechanical properties of those systems depend on the colloidal properties, surface oxides, and surface modification of CB. For binary systems of CPE and CB, oxidized CB gives a high modulus at low strain amplitude and a large Payne effect compared with untreated CB. In contrast, the reverse effect was observed for their ternary systems. Consequently, a good micro‐dispersion is obtainable by surface modification due to physical adsorption of AO‐80 on oxidized CB particles via hydrogen bonds. © 2003 Society of Chemical Industry 相似文献
77.
简要介绍了国内少有的干气催化部分氧化转化制氢工艺,重点讨论了转化水碳比的控制条件,对降低水碳比操作进行了有益地探讨。 相似文献
78.
79.
Works of adhesion at the carbon fiber-liquid interface determined using a modified wetting technique
Works of adhesion WSL between aqueous solutions with pH values in the range from 1 to 14 and carbon fibers from different sources, which were additionally treated in an inert atmosphere or in oxygen, were measured by use of a microbalance. These works of adhesion WSL were found to show distinct stepwise dependencies on the pH value. The works of adhesion WSL are attributed to dispersion interactions WSL1 and various acid-base interactions wslab—in the latter case between the acidic and basic surface groups of carbon and the various basic and acidic aqueous solutions. 相似文献
80.
活性炭单柱提取肌苷新技术研究 总被引:1,自引:0,他引:1
活性炭单柱提取肌苷新技术研究李永泉,张进,姚恕,郑莲英,俞峰(杭州大学生物系杭州310028)(浙江大学化工系杭州310027)关键词:肌苷,提取技术,活性炭单柱1前言目前,国内肌苷发酵后处理工艺落后,在分离提取工序中肌苷损失严重,收率一般只有50%... 相似文献