EMD与KOH溶液的相互影响

利用滴定分析、热失重分析以及XRD方法研究了EMD和KOH溶液混合后的变化。结果表明:碱与MnO2可以相互作用并导致体系温度的升高,碱浓度的下降,EMD中形成Mn3O4以及MnO2中结合水的损失。相互作用的结果与所加KOH溶液的浓度、EMD中的水含量、二者用量的比例关系以及体系的温度有关。     

Transient Green’s Tensor for a Layered Solid Half-Space With Different Interface Conditions

Pulsed ultrasonic techniques can be and have been used to examine the interface conditions of a bonded structure. To provide a theoretical basis for such testing techniques we model the structure as a layer on top of a half-space, both of different elastic properties, with various interface bonding conditions. The exact dynamic Green’s tensor for such a structure is explicitly derived from the three-dimensional equations of motion. The final solution is a series. Each term of the series corresponds to a successive arrival of a “generalized ray” and each is a definite line integral along a fixed path which can be easily computed numerically. Willis’ method is used in the derivation. A new scheme of automatic generation of the arrivals and ray paths using combinatorial analysis, along with the summation of the corresponding products of reflection coefficients is presented. A FORTRAN code is developed for computation of the Green’s tensor when both the source and the detector are located on the top surface. The Green’s tensor is then used to simulate displacements due to pulsed ultrasonic point sources of known time waveform. Results show that the interface bonding conditions have a great influence on the transient displacements. For example, when the interface bonding conditions vary, some of the first few head waves and regular reflected rays change polarities and amplitudes. This phenomenon can be used to infer the quality of the interface bond of materials in ultrasonic nondestructive evaluation. In addition the results are useful in the study of acoustic microscopy probes, coatings, and geo-exploration.     

Stability of Standard Electrolytic Conductivity Solutions in Glass Containers

The stability of solutions having an electrolytic conductivity, κ, of 5 μS/cm to 100 000 μS/cm packaged in glass screw-cap bottles, glass serum bottles, and glass ampoules was monitored for 1 year to 2 years. The conductivity was determined by measuring the ac resistance of the solution. Mass loss was also monitored for solutions packaged in bottles. The solutions were prepared using KCl in water (κ ≥100 μS/cm) or KCl in 30 % (by mass) n-propanol 70 % (by mass) water (κ ≤ 15 μS/cm). The conductivity changes were compared by packaging type and by nominal κ. The main causes of the κ changes are evaporation (screw-cap bottles) and leaching (screw-cap bottles, serum bottles, and ampoules). Evaporation is determined from mass loss data; leaching occurs from the glass container with no change in mass. The choice of optimal packaging, which depends on the conductivity level, is the packaging in which κ changes the least with time. Ampoules are the most suitable packaging for standards having nominal κ values of 500 μS/cm to 100 000 μS/cm. Screw-cap bottles are most suitable for standards having a nominal κ of 5 μS/cm to 100 μS/cm.     

带有集中质量的分布质量弹性转动横振精确解

求得了带有集中质量的分布质量弹性转轴系统横向自由振动的频率方程和振型函数的精确解析表达式，及其与不转动轴系统自由振动的频率方程和振型函数及转动角速度之间的精确解析关系     

氨荒酸盐抑制铜在NaCl溶液中腐蚀的电化学研究

通过电化学极化曲线和失重实验,研究了氨荒酸盐对铜在氯化钠溶液中的缓蚀性能,并与相应胺的缓蚀性能进行了对比。结果表明:氨荒酸盐对铜具有较好的缓蚀性能。     

TRT入口方管道爆裂原因剖析

介绍了鞍钢7#高炉TRT装置入口方管道爆裂事故经过,进行了原因分析,并提出了解决措施。     

Bridging process and structure through criteria

Scholars in design face two central challenges in design methods inquiry: firstly, to integrate process and solution, and secondly, to examine developmental junctures leading to innovation. With these goals in mind, we maintain that design criteria deserve greater attention and illustrate this position with a study of noted designers' use of criteria. The primary finding was that five criteria functions were considered during the design process. The study also explored potential relationships between designer variables (i.e., professional expertise and personality type) and criteria use.     

非均匀有耗媒质部分参数的重建

在高频部分，通过用Ｗｅｎｔｚｅｌ—Ｋｒａｍｅｒｓ—Ｂｒｉｌｌｏｕｉｎ—Ｊｅｆｆｅｒｙｓ（ＷＫＢＪ）解作为内场近似，本文证明了有耗非均匀媒质的反射系数在复平面上的轨迹是个圆。根据不同入射角度、不同极化的高频反射系数圆的圆心与半径，可以重建出有耗媒质的部分关键参数。本文方法同时适用于已知复反射系数谱和仅知反射系数振幅情况。文中给出具体重建实例。     

初级金属固溶体的固相线

本文提出二元合金A_(1-x)B_x的初级金属固溶体的固相线的计算公式为:T_m(x)=T_(mA)F(x),其中T_(mA)是A金属的熔点,F(x)是以X为变量、包含A和B的原子密度N、价数Z、熔化体积增率(△V/V)和熔化熵△S的解析函数.对于以Cu、Ag、Au为基的、包含一价到四价的简单金属的24种初级金属固溶体的固相线作了理论计算.与实验结果符合较好.对于三元合金也作了相应的推广.     

LabWare树立全球LIMS的典范

本文站在技术和应用的角度，简要介绍美国LabWare公司LIMS产品的功能，对其特点进行分析，其中，该系统的先进性和可组态性，实施的准时、概算的可控制，以及成功的业绩，对中国的用户将具有很大的吸引力。