A disposable single-use electrochemical sensor for the detection of uric acid in human whole blood

We report here a non-enzymatic detecting electrode strip for fast monitoring of uric acid in human whole blood. A single-use amperometric uric acid sensor strip, incorporating a three-electrode configuration, has been fabricated on a polypropylene substrate using low cost screen-printing (thick-film) technology. Both the working and counter electrodes were prepared by screen-printing commercial carbon ink. The integration on the same support of pseudo-reference electrode was obtained by screen-printing a commercial silver ink and subsequent electrochemical pretreatment. Simply by placing a 20 μl human whole blood drop on the strip is enough for uric acid analysis by square-wave voltammetry. Real human whole blood samples were analyzed by this method and compared to the phosphotungstic acid clinical test procedure with satisfactory results.     

M－Z型铌酸锂高速调制器

报道了采用行波电极结构的偏振型和与偏振无关型Ｔｉ：ＬｉＮｂＯ３高速强度调制器，其中与偏振无关的高速强度调制器是首次研制成功。     

硒化铅光导型红外探测器的电极选择

本文主要介绍硒化铅光导型多元红外探测器的电极材料选择和电极的制备工艺。     

Evaluation of rapeseed meals in broiler chicks: Effect of iodine supply and glucosinolate degradation by myrosinase or copper

In rapeseed meals (RSM) of a conventional (c) or a newly bred (n) variety 117 or 44 mmol glucosinolates and glucosinolate degradation products per kg dry matter were detected. Soaking meals in aqueous myrosinase or copper sulphate solution and subsequent drying reduced the content of antinutrients by more than 90%. Broiler chickens were fed (i) a glucosinolate-free diet, or this diet in which half the soybean meal was replaced by RSM of various origins and treatment; (ii) untreated cRSM; (iii) cRSM treated with myrosinase: (iv) cRSM treated with Cu (v) untreated nRSM; or (vi) nRSM treated with myrosinase. These diets were administered with or without supplementary iodine. Chickens receiving the iodine-deficient diets with myrosinase-treated RSM showed growth depression, incomplete feathering, leg injuries and severe goitre. In the serum T⁴ could not be detected. Giving myrosinase-treated RSM plus iodine, or giving other RSM diets irrespective of iodine administration, no growth depression was observed. RSM diets without iodine dosage markedly increased thyroid weight: there were no differences between the RSM variants. In contrast to the treatment with myrosinase, in the sera of the chickens fed on untreated RSM or RSM treated with copper T⁴ could be detected, suggesting that in iodine-deficient conditions differences in serum T⁴ concentration between RSM groups indicate a differing anti-thyroid activity. With iodine supplementation the RSM had a significant effect on thyroid weight. The largest thyroids (five-fold heavier) were in the animals with myrosinase-treated cRSM. The untreated cRSM and the nRSM trebled or doubled the thyroid weight, and the myrosinase-treated nRSM trebled it. The thyroid weight of chicks fed cRSM treated with copper did not differ significantly from the glucosinolate-free control. There was evidence that heating the myrosinase-treated RMS produced anti-thyroid compounds; these should be identified in further investigations.     

利用扫描电镜研究三维电极主电极表面腐蚀状况

借助扫描电镜（SEM）对不同实验条件下的三维电极主电极表面腐蚀状况进行研究。结果表明，三维电极主极阳极的内侧腐蚀程度远大于其外侧，水样性质、电极材料性质对电极的腐蚀程度有很大的影响，不锈钢做三维电极主电极优于铝、铁电极。为三维电极主电极的选材提供了一定的理论依据。     

Pore‐free mold‐pattern‐transfer method for barrier ribs of HD PDPs

Abstract— Among various barrier‐rib manufacturing processes, the mold‐pattern‐transfer method has potential to reduce processing cost as well as the manufacture of high‐resolution pixels. In this study, the effects of major processing variables of the mold‐pattern‐transfer process on the formation of air‐trapped pores within barrier ribs were examined. The results indicated that with an optimum combination of the processing variables, barrier ribs without trapped defects can be produced, demonstrating the possibility of reducing the number of processing steps and costs of barrier ribs.     

铜冶炼系统节能降耗与余热利用前景分析

大规模铜冶炼系统的技术改造,可在短期内改变铜厂的面貌,快速提升产品产量,大幅降低铜冶炼的能耗,如何能更深层次地利用好余热资源,是我们研究和发展的方向。     

印制板蚀刻、微蚀刻废液的再生和铜回收的技术及设备

传统的印制板蚀刻废液处理方法存在着工艺落后、操作不便、二次污染、效益不高等问题,本工艺采用特殊的萃取电解、吸附电解技术,使蚀刻废液得以再生循环利用,铜得以100%回收,低含铜废水铜得到98%回收,整个系统不产生二次污染,获得的铜为高纯度铜板,在实现污染控制的同时,废液废水得到了资源化利用。     

微波高压提取快速测定饲料含氟量的探讨

采用微波高压制样技术,快速提取饲料中的氟元素,结合氟离子选择性电极标准添加和电位极差测试方法,能够快速、准确地测试饲料中的含氟量     

草酸二甲酯加氢合成乙二醇反应的研究

在微型管式反应器中,采用Cu/SiO2催化剂,在温度190～210℃、压力1～3MPa、草酸二甲酯(DMO)与氢气的摩尔比(氢酯比)40～120、DMO空速6.0～25.0mmol/(g.h)的条件下,对DMO加氢制乙二醇的反应进行了研究。实验结果表明,高温、高压、高氢酯比和低DMO空速都能提高DMO的转化率和乙二醇的收率,但同时也增加了副产物的选择性。较适合的反应条件为:压力2MPa,温度205～210℃,氢酯比80～100,DMO空速10.0mmol/(g.h)。动力学研究表明,DMO加氢反应符合Langmuir-Hinshelwood吸附反应动力学模型,表面反应为速率控制步骤,氢气不解离吸附,由此得到了相应的动力学方程及参数。统计检验结果表明,该模型对DMO加氢反应高度适定。