Effects of a Nd—Fe—B magnetic filler on the crystallization of poly(phenylene sulfide)

The crystallization of poly(phenylene sulfide) (PPS) in a polymer–magnetic Nd—Fe—B powder suspension was studied. Isothermal crystallization behavior was analyzed by way of differential scanning calorimetry, and the kinetics were described via the Avrami equation. The Avrami parameters and the crystallization times were strongly affected by both the particle size and the presence of a coupling agent coated on the filler particles. The small Nd—Fe—B particles exhibited long induction and half‐times, whereas the large particles tended to have short crystallization times. Particles ranging from 38 to 150 μ appeared to have similar crystallization times and to have no significant change in the value of Avrami index with melt crystallization temperature. As a result of these analyses, the dynamic mechanical properties were determined to correlate the fundamental polymer crystallization characteristics and the physical properties of the PPS binder. The enhancement of the wetting of the filler to the binder was promoted through the coupling agent, as confirmed by dynamic mechanical testing performed on the samples. The storage modulus typically decreased because of the presence of the uncoated small particles. Conversely, the loss modulus was enhanced because of the presence of the coated small particles in the PPS binder. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 1091–1102, 2002     

ON THE MODELLING OF PARTICLE-BODY INTERACTIONS IN STOKES FLOWS INVOLVING A SPHERE AND CIRCULAR DISC OR A TORUS AND CIRCULAR CYLINDER USING POINT SINGULARITIES

Few exact solutions of the Stokes equations are known, even for steady or quasi-steady flows, involving finite sized bodies, and numerical techniques generally have to be resorted to for finding solutions. However, quite effective modelling of flows involving complicated boundary geometries is possible using the three-dimensional Stokeslet and rotlet point singularities. Two problems are studied in detail. In the first example, exact solutions for the three-dimensional Stokeslet and rotlet placed axisymmetrically along the axis of a circular disc are found and combined with Brenner's first order interaction formulae to determine the effect of the presence of the disc on the force and torque acting on a particle whose dimensions are small compared with its distance from the disc. The results are compared with those of a full numerical integration of the Stokes equations for a sphere translating towards a disc. In the second example, Brenner's first order wall correction theory is applied to the motion of a particle in a circular cylinder using the exact solutions for a torus translating or rotating in isolation. The theoretical predictions for the drag on a torus settling symmetrically in a circular cylinder are compared with those determined experimentally.     

蝶阀加工及装配工艺的研究

传统工艺加工阀体、活门时，对机床的性能要求较高，一般为数控镗床。介绍了一种采用普通镗床加工阀体、活门的工艺方法及蝶阀在厂内装配的工艺方法。     

光声耦合与光子Cooper对

文中研究了光声耦合所导致的光子Cooper对的形成机制，计算了光子Cooper对的能隙（0.01eV）和尺度（10^-5m)以及内禀角动量（奇数），并简要讨论了几十开低温下介质中光的超流效应的可能性。由于在低温下， 光子Cooper对不容易受到热运动的激发，因此有可能存在光的超流现象。     

改进的第三代相干算法及应用

在讨论相干技术发展及三代相干算法优缺点的基础上，介绍了改进的第三代相干算法。应用自行开发的相干软件对多个油气勘探和开发区块的三维地震资料进行处理、分析，对相干时窗长度、相关道数等参数对算法效果的影响及相干体对断层、异常地质体的识别，以及解释方法进行了探讨。应用实例证明，改进的第三代相干算法抗干扰能力强，横向分辨率高，不仅适用于倾斜地层，而且对断层尤其对小断层、异常地质体具有较高的检测能力，是油气勘探和开发的一项有效和实用的技术。     

A study on UV-curable coatings for HD-DVD: Primer and top coats

This study relates to the development of coatings for optical discs in high-density digital versatile disc systems (HD-DVD or blue lay disk) that use a high numerical aperture of 0.85 at 405 nm wavelength and have a protective top layer over a primer layer for protection against damage and dust. Ultraviolet-curable raw materials of two acrylic monofunctional monomers ( isobornylacrylate, IBA and tetrahydrofurfurylacrylate, THFA) and two kinds of urethaneacrylate oligomers (OUMD and OUME) have been easily mixed with photoinitiators. Curing rate of these materials was characterized by FT-IR. In case of top coats, VTES (vinyltriethoxysilane) and acrylic acid were added to enhance the abrasion resistance. These two kinds of UV-curable resinous materials having no solvent were synthesized and investigated as means for making a blue ray disk having good optical and mechanical properties. In addition, dynamic characteristics including reflectivity, fluctuation of RF signal and noise level were also investigated.     

江汉平原印支期以来的盆山耦合关系及下古生界油气响应

利用构造地质学和油气系统理论，以盆地构造-沉积分析技术为手段，研究了印支期以来江汉平原与周缘造山带的耦合关系，探讨了江汉平原的构造演化及其对油气成藏的控制作用。印支期以来江汉平原及周缘经历了挤压、拉张、挤压3次大的构造应力场的转换，使古生代海相碳酸盐岩沉积为主的盆地具有改造盆地的特点；一方面强烈的抬升、剥蚀使早期聚集的油气经历改造和再分配、再聚集过程，另一方面燕山期构造活动使逆冲推覆构造成为该区重要勘探领域。综合分析表明，位于台、盆转换带的宜昌-珂理-簰州区带是目前江汉平原及周缘下古生界油气勘探的有利地区。     

Hybrid of multi-signal processing methods for detection of small objects in containers filled with beverages using ultrasound

Ultrasound backscattered signals for object detection could be too weak to be perceived when superposed to strong reflection signals, and could also be complicated either in time or frequency domain. These peculiarities raise a challenge for signal processing methods. In this paper four signal processing methods were studied to detect objects in containers. Root mean squares (RMS) method was better in object detection but needed to combine other methods to increase detection success rate. Variance, center frequency pressure ratio (CFPR) and backscattered amplitude integral (BAI) methods have similar overall detection ratings. The optimal signal size, to increase the detection ability, corresponded approximately to the length of reverberation signals before it was dissipated.     

宣钢1260 m3高炉扩容大修改造设计

宣钢l260m^3高炉大修改造时将炉容扩大到l350m^3，对高炉本体系统设备及冷却系统、自动控制及检测系统进行了全面的改造更新，在炉腹、炉腰及炉身下部高热负荷区域采用铜冷却壁，取消炉身中上部铸铁冷却壁凸台，并采用薄内衬等先进、适用、可靠、成熟的技术。     

一种协调的科技文献分类方法

科技文献之间的相互引证关系反映了一种科学交流活动,显示了科学文献之间(甚至是学科之间)的内在联系,而通过追溯文献之间的这种关系,可以改善和提高传统的基于内容的科技文献的分类的方法。论文利用有相互引证关系,有同引关系,以及有耦合关系的两篇文献一般是属于同一类的这一特点,提出了文献之间的引用相似度,同引相似度,耦合相似度这三个概念,再利用这三个概念生成了文献之间的“结构相似度”,并将它用于K-NN分类法中得出一种基于结构的分类法。最后,论文将这种基于结构的分类法和基于内容的NaveBayes分类法结合起来提出了一种新的协调分类法。