单晶高温合金定向凝固过程中初生碳化物的上浮现象SCIEI

本文在一种抗热腐蚀单晶镍基高温合金平面及胞状液-固界面定向凝固条件下,发现了初生碳化物(TiC)的上浮现象并分析了其形成原因。     

Microstructure and mechanical properties of high strength as—cast Ti—15—3 alloy

The effects of heat treatment and solidification cooling rate on the microstructure and mechanical properties of as-cast Ti-15-3 alloy prepared by induction skull melting method were investigated.Results show that the microstructure of as-cast Ti-15-3 alloy changes from the features of simplified and larger size of beta grains to finer grain size with increasing solidification cooling rate.After solution treatment and different ageing treatment,alpha phase precipitates in grains interior as well as in grain boundaries.Due to the modification of the precipitate phase,the tensile stength and elongation of the alloy are improved simultaneously.A good combination of the values of 1.406GPa of σb and 4.5% of δ was obtained,which will be satisfied the use of this kind of alloy in critical areas.     

电、磁场对金属凝固组织的影响及应用

利用外加物理场凝固细晶技术是目前材料加工领域的研究热点。综述了各种电、磁场对金属凝固组织的影响，并对其主要的机理进行了探讨；并对电、磁场在金属凝固成形中的应用和进一步研究进行了展望。     

磷对Ni3Al凝固组织的影响

磷(P)在Ni3Al中的溶解度很低，凝固过程中向剩余液体中偏聚，最终在晶界上析出富P相，凝固后期。P在剩余液体中的偏聚程度升高，降低形核率，抑制试样心部等轴晶的形成，促使试样外缘晶粒向心部延伸生长，增加柱状晶长度。P降低合金终凝温度，增如糊状区长度，阻碍液相补缩，增加形成疏松的倾向。P产生上述作用的根本原因是其降低固、液两相体积自由能差和原子跃迁穿过液／固界面的激活能。     

快速凝固铝硅合金粉末加热过程中硅颗粒的粗化行为

利用差示扫描量热仪(DSC)、电子显微镜等设备对Al-12.8%Si合金粉末的原始状态及热处理后的状态进行了分析。发现其显微组织有两个连续的变化过程:在156℃时,固溶在基体Al中的过饱和Si开始析出,并在340℃发生粗化,随着加热温度的升高,粗化现象仍然存在。另外,对Si颗粒的粗化机理进行了研究,发现其粗化符合经典的LSW理论。     

MICROSTRUCTURE OF RAPIDLY SOLIDIFIED TiAl ALLOY POWDER

The rapidly solidified powder of Ti-34Al-2Mn alloy was obtained by means of ultrasonicgas atomisation (USGA) technique.The tupical size of the powder is 27 μm.X-ray diffractionresults show that the powder consists of major α_2-phase and minor γ-phase.Under opticalmicroscope both equiaxed and dendritical microstructure features were observed on RS pow-der sections.After annealing at 900 ℃/for 2 h in vacuum,most of α_2-phase transforms intoγ-phase,resulting in refinement of structure.     

CREEP CRACK PROPAGATION IN CONVENTIONAL CAST AND DIRECTIONALLY SOLIDIFIED SUPERALLOY RENE 80

The creep crack propagation in superalloy René80 of two different microstructures,i.e.,equiaxed grain structure by conventional casting and columnar grain by directionalsolidification,was investigated under static load at 1123 K.The creep crack growth rate,da/dt,seems to be correlated with the stress intensity factor,K.The creep crack growth ratein the directionally solidified alloy is lower than that in the conventional cast alloy,owing tothe elimination of transverse grain boundaries.The effect of microstructure on creep crackpropagation has also been discussed.     

凝固过程中的颗粒推斥

颗粒推斥是材料在固液相变过程中的基础问题之一，界面自由能的传统理论难以解释在金属基复合材料制备过程中的颗粒推斥现象，作者提出了固液界面前沿的流体流动是颗粒推斥的主要原因之一，并给出颗粒滚动及颗粒速度两种作用机制，推导出颗粒推斥条件判据，并以实验验证流体流动的作用机制及颗粒推斥理论判据。     

ELECTRON MICROANALYSIS FOR LASER MELTED ZONE IN 45 STEEL WITH Fe-Ni-Cr COATING

The Fe-Ni-Cr coating laver has been alloyed with 45 steel base metal by transverse.flow typeCO_2 gas laser of maximum output 5kW.The characteristics of the melted zone and the es-sence of the“bright band”has been investigated using the electron microscopy.The resultsshow that the“bright band”belongs to the melted zone and is a vertical section of the planecrystal,The width of the“bright band”equals the height of the plane crystal,which decreaseswith the increase of laser beam scanning rate and the decrease of laser power.This has beenexplained in terms of constitutional supercooling G/R.