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Significant increases in the activity of vanadium(III) amidinate catalysts for ethylene polymerization have been obtained by immobilization on a MgCl2‐based support prepared by reaction of AlEt3 with a MgCl2/ethanol adduct. Catalyst immobilization and activation on this type of support prevents the rapid decay in activity observed under homogeneous polymerization conditions with unsupported catalysts. Stable polymerization activity is also observed with analogous titanium(III) complexes. Polyethylene with narrow molecular weight distribution and spherical particle morphology is obtained without reactor fouling. Copyright © 2005 Society of Chemical Industry 相似文献
34.
A new method of studying the corrosion inhibition mechanism of rare earth metal(REM) on LC4 Al alloy with the spilt cell technique was studied. The principle and experimental method of the spilt cell technique were analyzed. By measuring the change of net-electric current between the two electrodes caused by the change of the amount of oxygen in the solution and the addition of CeCl3, the influence of corrosive performance of CeCl3 on LC4 super-power aluminum alloy in the 0.1 mol·L−1 NaCl solution was investigated. Meanwhile, the conditional changes of pH values, CeCl3 solution, additire and time of performance were also studied. Finally, the features of electrode surface were revealed by using SEM and X-ray energy-dispersive spectrometry (EDS). By combining these with other electric chemical techniques, such as potential-time curve, polarization curve et al. 相似文献
35.
M. Guerioune Y. Amiour W. Bounour O. Guellati A. Benaldjia A. Amara N. E. Chakri M. Ali-Rachedi D. Vrel 《International Journal of Self-Propagating High-Temperature Synthesis》2008,17(1):41-48
Aiming at preparation of shape memory alloys (SMAs), we explored the SHS of Cu1 − x
Zn1 − y
Al1 − z
alloys (0.29 < x < 0.30, 0.74 < y < 0.75, and 0.83 < z < 0.96). The most pronounced shape memory effect was exhibited by the alloys of the following compositions (wt %): (1) Cu(70.6)Zn(25.4)Al(4.0),
(2) Cu(70.1)Zn(25.9)Al(4.0), and (3) Cu(69.9)Zn(26.1)Al(4.0). The effect of process parameters on the synthesis of CuZnAl
alloys was studied by XRD, optical microscopy, and scanning electron microscopy (SEM). The grain size of CuZnAl was found
to depend on the relative amount of the primary CuZn and AlZn phases. Changes in the transformation temperature and heat of
transformation are discussed in terms of ignition intensity and compaction. Mechanism of the process depends on the level
of the temperature attained relative to the melting point of components. At the melting point of AlZn, the process is controlled
by the solid-state diffusion of AlZn into a product layer. The ignition temperature for this system depends on the temperature
of the austenite-martensite transformation in CuZnAl alloys. The composition and structure of the products was found to markedly
depend on process parameters. The SHS technique has been successfully used to prepare a variety of SMAs.
相似文献
36.
高镁边缘磷矿制取阻燃剂氢氧化镁的工艺 总被引:1,自引:0,他引:1
为解决大量的高镁低磷边缘磷矿废渣堆存对环境的影响,开发了以其为原料制取阻燃剂氢氧化镁工艺.该工艺主要包括酸解磷矿和镁沉淀过程,重点讨论了沉淀氢氧化镁过程中时间、温度、氨镁摩尔比n(NH3/MgO)等多种因素的影响,得到的最佳工艺条件是:反应温度65℃,反应时间80min,n(NH3/MgO)为5∶ 1,镁的沉淀效率为80%. 相似文献
37.
Vibration cavitation erosion tests were carried out on Ni-Mn-Ga alloys of three different crystal structures: (1) the cubic austenite, (2) the non-modulated tetragonal martensite (T) and (3) the five-layered martensite (5M). All Ni-Mn-Ga alloys exhibited cavitation behaviour characterized by a step-wise curve of mass loss versus test time. This behaviour is correlated to the microstructural nature of the alloys as well as the surface conditions of the pre-test samples. The type and concentration of the defects at the surfaces were critical to the cavitation resistance of the alloys. The best cavitation resistant alloy was of a cubic austenitic structure, followed with the alloy of a tetragonal T-martensite. The largest material loss was found in the alloy with a 5M martensite. All the studied Ni-Mn-Ga alloys had an excellent cavitation resistance compared to that of the reference stainless steel, and they even excelled some NiTi alloys found in literature. This may be due to the superelasticity of the cubic austenite and the twinning of the martensitic phases. 相似文献
38.
镍氢电池负极用低成本储氢合金的研究 总被引:1,自引:0,他引:1
研究了ABS型储氢合金在低Co含量条件下,随B组元替代元素Co,Al,Si等含量的变化对合金电化学性能的影响规律,同时研究了A组元中不同La/Ce比对合金电化学性能的影响情况。结果表明,随合金中Co含量的降低,合金的活化性能和放电容量得以改善,但合金的循环寿命下降也比较明显;在试验范围内,随Al元素的加入,合金的循环寿命得以改善,但材料的放电容量和活化性能均有所下降;随合金La/Ce比的降低,合金的放电容量略有下降,但其循环寿命和放电电压平台有较大提高。 相似文献
39.
40.
Ferdinando Auricchio Lorenza Petrini 《International journal for numerical methods in engineering》2004,61(6):807-836
An always increasing knowledge on material properties as well as a progressively more sophisticated production technology make shape memory alloys (SMA) extremely interesting for the industrial world. At the same time, SMA devices are typically characterized by complex multi‐axial stress states as well as non‐homogeneous and non‐isothermal conditions both in space and time. This aspect suggests the finite element method as a useful tool to help and improve application design and realization. With this aim, we focus on a three‐dimensional macroscopic thermo‐mechanical model able to reproduce the most significant SMA features (Int. J. Numer. Methods Eng. 2002; 55 : 1255–1264), proposing a simple modification of such a model. However, the suggested modification allows the development of a time‐discrete solution algorithm, which is more effective and robust than the one previously discussed in the literature. We verify the computational tool ability to simulate realistic mechanical boundary value problems with prescribed temperature dependence, studying three SMA applications: a spring actuator, a self‐expanding stent, a coupling device for vacuum tightness. The effectiveness of the model to solve thermo‐mechanical coupled problems will be discussed in a forthcoming work. Copyright © 2004 John Wiley & Sons, Ltd. 相似文献