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951.
Gérald Guérin 《Polymer》2003,44(24):7477-7484
The bonding of polystyrene (PS) surfaces below Tg was investigated by two different fracture tests: the lap-shear joint method and the cantilever beam method. Adhesion energy values obtained by the two methods are in agreement and develop with (time)1/2, at temperatures as low as Tg−16 °C. Even if the double cantilever method is the most common test found in the literature for adhesions above Tg, for low adhesion values, below Tg, the lap-shear joint geometry is more appropriate. Moreover, when the glass transition temperature is used as a reference temperature, polydisperse and monodisperse PS adhesion energy curves are superposable, suggesting that the auto-adhesion is not significantly favored by the presence of numerous chain ends at the surface (due to the low molecular weight chains provided by the polydisperse PS). 相似文献
952.
953.
The application of a low temperature ashing method for estimating total residual organic matter (toluene insolubles) in oil sands is described. A linear correlation exists between organic carbon content and loss on ignition at 400 ± 10 °C of solvent extracted oil sands. The ratio between total organic carbon and the weight loss on ignition (CT/LOl) owing to the removal of residual organic matter is much lower than that obtained for toluene soluble bitumen fractions, indicating very different chemical composition for the residual organic matter. The measured carbon content of the residual organic matter in oil sands suggests that this material could be a mixture of various fractions contained in resins, asphaltenes, asphaltic acids and humic acids. 相似文献
954.
研究试验温度和停放时间对胶料加工性能的影响。结果表明,试验温度对胶料的门尼粘度、门尼焦烧时间和硫化特性均有一定影响。门尼粘度测定的试验温度选择100℃;门尼焦烧时间测定的试验温度一般选120℃,SBR胶料可提高至130℃左右,以缩短试验时间;硫化特性测定的试验温度一般选185℃。试验前模腔达到规定温度后再保持15min,以使转子与模腔温度一致。胶料停放时间应控制在2h左右。 相似文献
955.
Nianxue Song Colin Rhodes David W. Johnson Graham J. Hutchings 《Catalysis Letters》2005,102(3-4):271-279
Temperature programmed reduction (TPR) and oxidation (TPO) are used extensively in catalyst characterisation. In this paper, we examine the use of TPR/TPO cycles for the characterisation of a range of molybdates and single oxides. In particular we observe that the first cycle differs from that of subsequent analyses, even when the maximum temperature is limited to that used in the catalytic reaction. The effect is independent of heating rates and cooling atmospheres and has been demonstrated using different bed configurations. This observation has significance when these oxides are used in periodic flow reactors that involve many cyclical reduction/oxidation. 相似文献
956.
957.
研制了以熔融合金惰性气体雾化法制备的含有大量硅化物的镍铁合金粉末为烧结粘结相的硅化物-镍铁合金/碳化钛金属陶瓷。用SEM,EDS,XRD和热重天平等测试分析了金属陶瓷的组织结构与性能。结果表明:这种硅化物-镍铁合金/碳化钛金属陶瓷具有核/环形边缘结构,硅化物-镍铁合金对碳化钛粒子有较好的润湿烧结作用。研制的金属陶瓷的抗弯强度在1000~1200MPa,硬度HRA为80~90。由于合金中含有较高的对氧有较强亲和力的元素硅,在氧化过程中形成SiO2以及一系列复合氧化物构成的致密氧化膜,使合金具有高的抗高温氧化性能。 相似文献
958.
中原化肥厂合成氨装置由于修复过渡段保温材料,在过渡段降温及一段炉升温方法上采取了特殊措施,特别是一段炉升温采取了先点火的升温方法。 相似文献
959.
以硝酸锌和氢氧化钠为原料,分别以水和醇作为溶剂,采用液相直接沉淀法合成纳米氧化锌。在以水为反应溶剂条件下,研究了反应时间、反应温度、反应物浓度和反应物配比对纳米氧化锌中位径和形貌的影响,得到制备较小中位径及合适长径比纳米氧化锌的最优反应条件,即:反应时间为3 h、反应温度为70 ℃、锌离子浓度为0.5 mol/L、锌离子与氢氧根浓度比为1:2。在上述最优反应条件下,研究了不同醇溶剂对纳米氧化锌中位径、形貌及其光催化性能的影响。研究发现,随着溶剂碳链长度的增长,纳米氧化锌中位径呈现上下波动,无明显变化规律,形貌由球状向柱状发展,光催化性能总体不断减弱。 相似文献
960.
Semih Eser Robert G. Jenkins Guangquan Wei Harold H. Schobert Joseph T. Joseph 《Fuel》1991,70(12):1445-1455
High pressure microdilatometer experiments were performed on a subbituminous (Wyodak) and a bituminous (Illinois no. 6) coal in helium and hydrogen atmospheres with and without added tetralin. Wyodak coal samples showed no swelling but contractions ranging between 24 and 40 vol% upon heating at 20 and 100 °C min− 1 under helium or hydrogen pressures between 150 and 1000 psig (˜1.0–6.9 MPa). Under the same conditions, Illinois no. 6 coals displayed contractions (25–60 vol%) prior to swelling up to 117 vol%. Upon tetralin addition (at 35–190 wt% of the coal), Wyodak coal samples did not swell but showed an increasing contraction with increasing helium or hydrogen pressure due to a slight softening and fusion of the coal particles. In contrast, addition of tetralin at much lower concentrations (5–35 wt%) had a marked effect on the contraction and swelling behaviour of Illinois no. 6. A maximum swelling of 200 vol% was obtained at a tetralin addition of 30 wt%. The increased swelling results from more extensive softening and fusion of coal particles in the presence of tetralin. Both coals showed a decreasing char yield with increasing tetralin concentration. The substantially lower extent of interaction observed between Wyodak coal samples and tetralin compared to Illinois no. 6 coal can be attributed to the differences in pore structure and/or chemical constitution of the two coal samples. Examination of the resultant solids by optical microscopy revealed the microstructural changes produced by thermal treatment in dilatometer experiments. 相似文献