Effect of pulse parameters on microstructure of joint in laser beam welding for SiC_p/6063 composite

1　INTRODUCTIONSiC particlesreinforcedcomposites ,thankstotheirlowcostsandhighlevelofstructuralproperties ,areshowingtheirpotentialincivilandmilitaryappli cation .SiC particlesreinforcedaluminummatrixcomposites wideapplicationinaerospaceandautomo tiveareattributedtotheirperformanceofhighspecif icstrength ,highspecificstiffness ,highelasticmodu lusandexcellentwearresistance .Thecoefficientofthermalexpansionandthermalconductivitycanberegulatedbychangingthecontentandsizeofrein forcingparticl…     

地下金属矿山斜坡道浆土路修筑工艺及应用研究

斜坡道是地下金属矿山的主要运输通道,其道路质量直接影响着矿山的安全运输和经济效益。针对斜坡道混凝土浇筑路面存在的筑路成本高、养护时间长、使用寿命短及维护困难等不足,引入浆土路修筑技术,开展了地下金属矿山斜坡道浆土路筑路材料配比试验、黏土搓条和崩解试验、水洗筛分试验,并在云南卡房分公司完成了浆土路试验路段的修筑。结果表明：浆土路筑路技术能够很好地应用于地下矿山道路修筑,具有施工工艺简单、筑路成本低、施工周期短、承载能力强、抑尘防滑和低碳环保等诸多优点,为地下金属矿山道路修筑提供了工程借鉴,对于矿山降本增效、节能减排及安全高效具有重要的意义。     

含稀土硅化铁热电材料的电学性能初探

采用悬浮真空熔炼和800℃,168h真空退火方法制备了含稀土Sm的FeSi2基金属硅化物,并对其晶体结构、See-beck系数、电阻率进行了初步研究。实验发现,名义组成为Fe0.6Sm0.4Si2的试样的热电功率因子从室温时的0.26×10-4W·m-1K-2随温度上升到500℃时的1.6×10-4W·m-1K-2,比不含Sm或含Sm量很少的对比试样高一个数量级左右。其原因被认为是由于Sm的外层4f电子的贡献。     

汽车覆盖件成形过程数值模拟研究

本文介绍汽车覆盖件成形过程有限元模拟两个软件ＩＴＡＳ—３Ｄ和ＤＹＮＡＭＩＣ的最新研究成果，基本原理和有关接触搜索、摩擦和拉伸筋模型等关键技术。并有两个应用实例     

刚塑性有限元模拟中体积变化问题处理方法

分析了在塑性有限元分析金属体积成形问题中引起体积变化的原因 ,指出在采用罚函数方法引入体积不可压缩条件的刚塑性有限元模拟中惩罚因子、增量步长、节点调整、网格密度和重划次数等是引起体积变化的主要原因。针对所分析原因 ,在现有的方法基础上提出基于三维有限元的节点调整和体积补偿新方法 ,并在实际模拟中应用 ,得到较好的效果 ,提高了模拟的精度和可信度。     

碱土金属在萃取剂与树脂间反应平衡常数的测定

研究了碱土金属离子在Ｄ００１树脂与８－羟基喹啉三氯甲烷溶液间的平衡常数Ｏ－ｔＫ的测定。其值依Ｍｇ、Ｃａ、Ｓｒ、Ｂａ次序减小。并得出萃取剂浓度［ＨＡ］。与金属离子在两相分配的关系。     

Physicochemical investigation of the decomposition products of ammonium metal carboxylates: ammonium ferric citrate hydrate

The thermal decomposition up to 400 °C of ammonium ferric citrate hydrate, of unknown structure and formula weight, was studied by thermogravimetry, differential thermal analysis, infrared (IR) spectroscopy and X-ray diffractometry. The possible identities of the formula weight and the intermediate products of calcination are discussed. The results revealed that the parent material is amorphous and contains two moles of water and two moles of ammonia. Decomposition takes place via six weight-loss processes, three endothermic (90–230 °C) and three exothermic (240–298 °C), leading eventually to the formation of Fe₂O₃. The intermediate solid products are mainly unstable amorphous oxycarbonates, as indicated by X-ray and IR spectroscopies. The gas-phase decomposition products identified by IR spectroscopy are NH₃, CO₂, CO, CH₃COCH₃, CH₄ and NH₄OH. Surface area measurement and scanning electron microscopy showed that Fe₂O₃, the final product at 400 °C, hada surface area of 40 m²/g and good crystalline and porous character.     

Preparation,characterization, and adsorption properties for metal ions of a novel chelating resin containing sulfoxide and diethylene glycol

A novel chelating resin containing sulfoxide and diethylene glycol, poly{4‐vinylbenzyl‐[2‐2‐(hydroxyethyl)ethoxyl]sulfoxide} (PVESO) was synthesized using chloromethylated polystyrene (PS‐Cl) as material. Its structure was characterized by elemental analysis, infrared spectra, and scanning electron microscopy (SEM). The adsorption capacities of the resin for Hg²⁺, Ag⁺, Cu²⁺, Zn²⁺, and Pb²⁺ at various pH values were determined. The maximum adsorption capacities for Hg²⁺ and Ag⁺ were 1.56 and 0.75 mmol g^?1 respectively. The resin had high selectivity for Hg²⁺ and Ag⁺ over the pH range 1.0–7.0. The adsorption capacities for Hg²⁺ and Ag⁺ under competitive condition were also determined by batch experiment method. In addition, the adsorption kinetics of the resin towards Hg²⁺ at different temperatures was also investigated. The results showed that the adsorption rate was governed by film diffusion at 20°C and 25°C, by particle diffusion at 30°C and 35°C. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 6054–6059, 2006     

南水北调中线总干渠水质变化趋势及污染源分析

为了解和掌握南水北调中线总干渠水质状况,依据总干渠26个常规水质断面监测数据,分析了总干渠沿程水质变化趋势。结果表明,主要污染指标(CODMn、氨氮、总氮和总磷)呈现出沿程增加趋势。根据影响总干渠水质的潜在影响因素,分析了7类污染源(直接水污染、大气粉尘沉降、桥面雨水污染、底泥污染、周边垃圾场淋溶液污染、雨洪污染、受污染地下水)及其可能对干渠水质产生的影响程度,并针对不同污染源提出了防控对策,供管理部门决策参考。     

低熔点合金填充聚合物材料断口形貌研究

研究了合金元素、加工温度、金属含量、第三组分对低熔点金属填充聚合物材料断口形貌的影响。实验结果表明:不同的合金对体系的影响很大,低分子量、低结晶性聚合物,高的成型加工温度可提高材料的相容性。