高强度结构钢的韧性启裂和稳态扩展

研究了具有一定韧度的高强度结构钢裂纹早期扩展阻力与材料的微观组织结构、应力状态、变形历史和应变特性之间的关系。结果表明:裂纹扩展阻力(指J_R阻力曲线中的J_i和dJ/da)主要决定于裂纹尖端的塑性约束程度和应力应变场中消耗的弹性能和塑性功。这与三轴应力状态函数σ_mσ~(1/2)有关。材料的流变曲线描述了形变过程中的变形历史和应变特性,有明显的阶段性,其中第Ⅱ阶段的变形历史和应变特性制约着裂纹的启裂过程,第Ⅲ阶段的变形历史和应变特性制约着裂纹的扩展过程。应变硬化率dσ/dε可以敏感地反映出材料内部的应力分布和微观断裂机制。     

钽钛合金再结晶退火工艺研究

研究了二元钽钛合金丝经拉拔加工中间再结晶退火处理后的组织。结果发现:变形量为12%的!1.5mm的钛钽合金丝经1000℃×1h退火能够发生完全再结晶;变形量由17%增大至70%,再结晶温度下降约40℃,变形量对再结晶温度影响较大;变形量越大,再结晶后的组织晶粒细小。     

MICROSTRUCTURE AND MECHANICAL BEHAVIOUR OF Al-Li-Zr AND Al-Li-Cu-Mg-Zr ALLOYS

The aging response,tensile and impact properties of two kinds of Al-Li based alloys havebeen studied.The microstructure,deformation as well as fracture behaviour in the alloys wereobserved with SEM and TEM.It was found that the mechanisms of deformation and fracturefor different heat-treated alloys with the same chemical composition are quite different.Thecauses leading to the drop of ductility,toughness as well as anisotropy in peak-aged alloyshave been analysed.Finally,possible methods to improve the ductility and toughness of the al-loys have been discussed.     

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 在大量科学试验基础上，提出一种金属表面形成金属陶瓷的新工艺方法。该方法具有放电电压低，陶瓷层结构致密与基体冶金结合，适用于多种金属材料等优点。文中利用光学显微镜和扫描电镜（SEM）观察了陶瓷涂层的显微组织，并通过X射线衍射和机械性能试验对其相结构和室温力学性能进行了探讨。结果表明：金属陶瓷涂层的晶粒细小，分布均匀，具有高的硬度及良好的耐磨性。     

长期高温服役的12%Cr耐热合金钢性能退化与恢复

X2 0CrMoV12 1耐热合金钢广泛应用于热电厂主蒸汽管线等主要部件。经长期高温负荷运行后 ,材料性能明显退化。观察显微组织发现 ,材料性能下降是和晶界碳化物的粗化密切相关的。文章着重研究了损伤材料重新热处理后的性能和组织结构的变化 ,初步探讨了材料长期服役后通过热处理恢复其原始性能的可能性     

MICROSTRUCTURE STUDY OF CONSTITUENT PHASES IN 2024 SERIES Al ALLOYS

X-ray microanalysis,convergent beam electron diffraction(CBD)and selected area electrondiffraction(SAD)studies on the structures and compositions of the constituent phases in2024 series Al alloys have been conducted.Partial substitution of alloying elements is found tooccur in all the constituent phases,which cause small deviations from the stoichiometric com-positions reported in these ternary compounds.The dominant phase is α-Al_(12)(FeMn)_3Si whichhas a body center cubic crystal structure with the Im■ space group and a=1.25 nm.The nextdominant phase is Cu_2FeAl_7 which has a primitive tetragonal crystal structure with theP4/mnc space group and a=0.6336 nm,c=1.487 nm.The minor phase is α'-Al_(12)Fe_3Si hav-ing α primitive cubic crystal structure with the Pm■ space group and α=1.27 nm.     

Effect of pulse parameters on microstructure of joint in laser beam welding for SiC_p/6063 composite

1　INTRODUCTIONSiC particlesreinforcedcomposites ,thankstotheirlowcostsandhighlevelofstructuralproperties ,areshowingtheirpotentialincivilandmilitaryappli cation .SiC particlesreinforcedaluminummatrixcomposites wideapplicationinaerospaceandautomo tiveareattributedtotheirperformanceofhighspecif icstrength ,highspecificstiffness ,highelasticmodu lusandexcellentwearresistance .Thecoefficientofthermalexpansionandthermalconductivitycanberegulatedbychangingthecontentandsizeofrein forcingparticl…     

高深宽比SU-8微结构的简易加工技术

为了提高微驱动器的性能,提出了一种在氧化铟锡(ITO)玻璃上加工高深宽比SU-8微结构的方法.在导电玻璃的ITO层上涂覆一薄层AZ-4620正光胶,用常规的接触式曝光法,将光刻掩模上的二维图形转移到AZ-4620光胶层上,显影后利用ITO玻璃的导电性,在AZ-4620光胶曝光处电沉积镍,原掩膜图形可保真地转移到ITO玻璃表面的镍镀层上,使紫外光透过ITO玻璃基底进行反面曝光,从而保证了光刻掩模与SU-8光胶层间的完全接触,消除了厚光胶层表面不平在曝光时的散射和基片材料的反射影响,成功制备了深宽比为16、侧壁垂直度为89.5°的微结构.本方法使用设备简单,加工成本低.     

Microstructural evolution and interfacial reactions between Ti and ZrO2/CaTiO3 composites

Various proportions of ZrO₂/CaTiO₃ powders were mixed and hot pressed at 1500°C/30 min for Ti casting. The hot-pressed ZrO₂/CaTiO₃ composites were reacted with pure Ti at 1700°C/10 min in Ar. The interfacial reaction between Ti and ZrO₂/CaTiO₃ composites was investigated through X-ray diffraction, scanning electron microscopy, transmission electron microscopy, and energy-dispersive X-ray spectroscopy. The ZrO₂/CaTiO₃ composites with less than 10 vol.%, CaTiO₃, and a minor amount of residual TiO₂ were found. When the content of ZrO₂ was increased to larger than 10 vol.%, two Ca₂Zr₅Ti₂O₁₆ and CaZrTi₂O₇ phases appeared in the composites. The amount of CaTiO₃ and CaZrTi₂O₇ in the composites gradually decreased as the amount of ZrO₂ increased. When Ti came in contact with ZrO₂/CaTiO₃ composites with less than 10 vol.% ZrO₂, the resulting eutectic reaction produced a liquid phase and induced melting. When ZrO₂ was increased to more than 30 vol.% in the composites, Ca₂Zr₅Ti₂O₁₆ and CaZrTi₂O₇ changed completely to CaZrO₃, Ti₂O, CaO, and ZrO₂. With more than 30 vol.% ZrO₂, no other reaction phases occurred in the Ti side after contact with the ZrO₂/CaTiO₃ composites, which is conducive for producing ceramic composites for Ti casting applications.     

Effect of SiC nanowhisker addition on microstructure and mechanical properties of regenerated cemented carbides by low-pressure sintering

The hardness and toughness of regenerated cemented carbides, in general, are contradictory. Therefore, it is critical to explore regenerated cemented carbides with both high hardness and high toughness. In this study, regenerated WC-8-wt% Co cemented carbide with SiC nanowhisker were prepared by low-pressure sintering. The influence of SiCw contents on the microstructure and mechanical properties of regenerated WC-8-wt% Co cemented carbide was investigated. The results indicated that the hardness, density, flexural strength, and fracture toughness of regenerated cemented carbide first increased and then decreased with the addition of SiCw. The Vickers hardness, density, flexural strength, and fracture toughness could reach 1575 HV, 14.6 g/cm³, 2204 MPa, 16.85 MPa·m^1/2, respectively, with SiCw content 0.5 wt%, which were increased by 14.4%, 0.7%, 12.2%, and 17.3%, respectively, when compared with the regenerated cemented carbide without SiCw. The lowest friction coefficient and the best wear resistance could be also reached when 0.5-wt% SiCw was added. The fracture mechanism of the regenerated cemented carbide contained both transgranular and intergranular fracture through the microscopic observation of fracture surface via scanning electron microscope.