LaCrMnNiO系热敏陶瓷的微观结构控制

通过对不同配方、工艺下的ＬａＣｒＭｎＮｉＯ系热敏陶瓷的微观结构研究，指出材料的相组成对其宏观电性能的影响，并提出了通过复合工艺利用“过渡相”的形成，对材料的“最终相”加以控制的方法。文中列出了使用ＸＲＤ及ＸＰＳ手段对材料微观结构的分析结果及有关电性能的测试数据。     

Effect of Bi and Sr concentrations on the formation of the 2223 phase in Bi-Pb-Sb-Sr-Ca-Cu-O materials, obtained under different conditions of thermal treatment

The superconducting properties and the phase and chemical composition of Bi _x Pb_0.3Sb_0.1Sr _y Ca₂Cu₃O_z (x=1.5, 1.6, and 1.7;y=1.9, 2.0, and 2.1) materials synthesized by one-step and multistep thermal treatments have been investigated. The multistep annealing between 825–875°C promotes the 2223 phase. The change of Bi concentration has little effect on the 2223 phase formation, regardless of the kind of thermal treatment used, but increasing the Sr concentration (y> 2) strongly inhibits this phase. It has also been established that the loss of Pb after synthesis depends on the initial Bi concentration. The loss of Pb decreases when the initial Bi content is lower.     

红外隐身技术的现状与发展

综述了红外隐身技术的现状，指明了存在的问题以及发展的方向。     

Recrystallization/precipitation behaviour in microalloyed steels

Microalloyed high-strength low-alloy (HSLA) steels contain additions of Nb, V, Ti, or in combination, in amounts of 0.01 to 0.1 weight percent to improve mechanical properties, which are strongly dependent on the thermomechanical interaction taking place in the course of rolling mill processes. The recrystallizatian of hat-twisted austenite has been investigated in a cylindrical specimen (f 6×50 mm) machined from hat rolled plates of 0,052 wt % Niobium microalloyed steel. Continuous and interrupted torsion test were carried out in the temperature range 1123 K to 1173 K after a solution treatment of 1.5 minutes at 1423 K and torque-twist data were analysed. The various methods were discussed for obtaining results from torsion tests. The effect of precipitation kinetics was appreciated by way of connection t_p/t_p(red), where t_p is the experimental measured time for the peak stress and t_p(red) is the newly defined reduced time. The softening ratio X and time t_0.05R for start of static recrystallization were established.

The correlation between precipitation and recrystallization is presented as a graphs for chosen requirements (temperature of austenitization, carbon and niobium content and strain rate). If temperature goes below 850°C, the restoration processes are hardly suppressed, both are limited by diffusion and Nb(CN) precipitation, which are extended dynamically in the range of strains rates 10⁻² to 1 s⁻¹.

In the present paper, an attempt is made to derive the PRTT diagram and to define all mathematical equations for describing recrystallization times t_0.05R, t_0.5R, t_0.95R and t_0.05P for the start of precipitation. In real metal forming processes such as the hot rolling of plates or strips the knowledge of these parameters and results is extremely important for the the correct microstructure and sheet quality to be obtained.     

相转移催化合成芳基烷基醚

报道了以四丁基溴化铵为相转移催化剂，简便地合成了１０个芳基烷基醚，反应几乎是定量地快速进行。     

微量Ag对CP276合金性能和组织的影响

研究添加不同含量的Ａｇ对ＣＰ２７６合金的拉伸性能和时效组织的影响。对拉伸强度、延伸率测试及透射电镜观察表明：０．１１ｗｔ％加入可促进Ｔ１相析出，使合金强度值升高；０．３５ｗｔ％Ａｇ的加入可在时效前期生成富Ａｇ、Ｍｇ的稳定的ＧＰ区，从而降低合金中Ｃｕ的固溶度，阻碍Ｔ１相析出，时效后期，ＧＰ区分解，生成大量Ｔ１相，使合金强度值显著升高。     

Prediction of liquid–liquid phase diagrams of aqueous salt+PEG systems using a thermodynamic model

In this study a thermodynamic model for the phase behavior of aqueous salt+polymer solutions is developed. The model is based on the solution theory of Hill, which included scaling laws for the polymer molecular mass dependence and Pitzer–Debye–Hückel theory. This model was tested for systems composed of two different molecular mass of polyethylene glycols (PEG) and five different inorganic salts. All the model parameters were determined from independent measurements. The agreement between the experimental and predicted phase diagrams by this model is good.     

Microstructure and Mechanical Properties of Heat-treated GeSb_2Te_4 Thin Films

The effect of annealing on microstructure,adhesive and frictional properties of GeSb 2 Te 4 films were experimentally studied.The GeSb 2 Te 4 films were prepared by radio frequency(RF)magnetron sputtering,and annealed at 200℃and 340℃under vacuum circumstance,respectively.The adhesion and friction experiments were mainly conducted with a lateral force microscope(LFM)for the GeSb 2 Te 4 thin films before and after annealing.Their morphology and phase structure were analyzed by using atomic force microscopy(AFM)and X-ray Diffraction(XRD)techniques,and the nanoindention was employed to evaluate their hardness values.Moreover,an electric force microscope(EFM)was used to measure the surface potential. It is found that the deposited GeSb 2 Te 4 thin film undergoes an amorphous-to-fcc and fcc-to-hex structure transition;the adhesion has a weaker dependence on the surface roughness,but a certain correlation with the surface potential of GeSb 2 Te 4 thin films.And the friction behavior of GeSb 2 Te 4 thin films follows their adhesion behavior under a lower applied load.However,such a relation is replaced by the mechanical behavior when the load is relatively higher.Moreover,the GeSb 2 Te 4 thin film annealed at 340℃presents a lubricative property.     

热力学相图计算技术在闪速燃烧合成氮化硅铁中的应用

将热力学相图计算技术应用于Si-Fe-O-N体系,以评估由FeSi75粉闪速燃烧合成氮化硅铁的条件和目标产物。结果表明:将闪速燃烧温度控制在1200～1500℃之间较为适宜,此时平衡态产物中除主要含有Si3N4以外,还有一定量的Fe与Si间化合物和少量稳定的SiO2存在。此计算结果与实际试验结果吻合良好。     

新型微波-毫米波幅相测试系统及扩展应用

介绍了一种新型微波 毫米波幅相测试系统及其在相关测试领域中的典型应用。与传统微波幅相测试系统相比 ,该系统具有原理新颖、结构简单、扩展频段容易和使用方便等优点。本系统目前广泛应用于紧缩场电气性能检测、天线测量和RCS测量等领域中 ,频率范围为 1～ 110GHz。本测试系统已经申请国家专利 ,并通过相关部门鉴定。