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61.
H. Ji D. Chopp J. E. Dolbow 《International journal for numerical methods in engineering》2002,54(8):1209-1233
A hybrid numerical method for modelling the evolution of sharp phase interfaces on fixed grids is presented. We focus attention on two‐dimensional solidification problems, where the temperature field evolves according to classical heat conduction in two subdomains separated by a moving freezing front. The enrichment strategies of the eXtended Finite Element Method (X‐FEM) are employed to represent the jump in the temperature gradient that governs the velocity of the phase boundary. A new approach with the X‐FEM is suggested for this class of problems whereby the partition of unity is constructed with C1(Ω) polynomials and enriched with a C0(Ω) function. This approach leads to jumps in temperature gradient occurring only at the phase boundary, and is shown to significantly improve estimates for the front velocity. Temporal derivatives of the temperature field in the vicinity of the phase front are obtained with a projection that employs discontinuous enrichment. In conjunction with a finer finite difference grid, the Level Set method is used to represent the evolution of the phase interface. An iterative procedure is adopted to satisfy the constraints on the temperature field on the phase boundary. The robustness and utility of the method is demonstrated with several benchmark problems of phase transformation. Copyright © 2002 John Wiley & Sons, Ltd. 相似文献
62.
We have used x-ray phase analysis to study the composition of the products of reaction between oxygen and nanocrystalline
powders with particle sizes 15, 40, 55, and 80 nm, and also specimens pressed (and sintered) from them. The powders were oxidized
in air at 100°C (400 h) to 500°C (5 min), while the sintered specimens were oxidized at 600–900°C for 15, 120, and 240 min.
In all cases, in the initial oxidation step the oxynitride Ti(OxNy) is formed, which over time is oxidized to TiO, Ti2O3, Ti3O5, TiO2 (anatase) and TiO2 (rutile). In the range 600–800°C, formation of a continuous oxide layer and conversion of anatase to rutile slows down diffusion
of oxygen in the scale. We have established that at 900°C, the growth rate of the scale thickness increases and so the reflections
from the oxynitride are barely noticeable on the diffraction patterns taken from the surface of the oxidized specimen. In
these diffraction patterns, along with strong reflections from the rutile, we also observed weak reflections from lower oxides
and anatase, which may be due to reaction between oxygen and the titanium ions diffused to the scale surface. We have concluded
that at T > 850°C, the mechanism for oxidation of TiN changes. This is due to superposition of counterdiffusion of titanium
ions on the diffusion of oxygen.
__________
Translated from Poroshkovaya Metallurgiya, Nos. 3–4(448), pp. 72–78, March–April, 2006. 相似文献
63.
《Ferroelectrics Letters Section》2007,34(3):95-107
Dielectric, ferroelectric and piezoelectric properties of xPb(Mg1/3Nb2/3)O3-(1-x)(Pb0.988 La0.012)(Zr0.535Ti0.465)O3 ceramic system synthesized through columbite precursor method are investigated. X-ray diffraction patterns of ceramics indicated pseudocubic phase formation with pyrochlore phase. Grain growth (4.47 μ m) and apparent density (7.68 gm/cm3) enhanced remarkably in 0.8PMN-0.2PLZT composition, respectively. Increasing PMN content remarkably increased both room temperature dielectric permittivity (εRT = 2316) and dielectric maximum (εTc = 24747) in 0.6PMN-0.4PLZT composition, respectively. PMN substitution in PLZT system enhanced the ferroelectric remanent (Pr = 28.4 μ C/cm2) and spontaneous (Ps = 31.2 μ C/cm2) polarization while coercive field (Ec) continuously decreased in xPMN-(1-x)PLZT system. PMN modification in PLZT system influenced piezoelectric properties (d33, kp and kt) throughout the PMN-PLZT system. 相似文献
64.
V. G. Khoruzhaya K. E. Kornienko P. S. Martsenyuk T. Ya. Velikanova 《Powder Metallurgy and Metal Ceramics》2006,45(5-6):251-258
Methods of differential thermal analysis, x-ray diffraction, microstructural analysis and electron probe microanalysis are
used to study alloys of the Al-Rh system over the whole concentration range. It is established that the phase of equiatomic
composition AlRh melts congruently at 2060°C and it has an extended range of homogeneity (45.1–54.2 at.% Rh). The solubility
of aluminum in rhodium reaches 9 at.%, decreasing to 6 at.% at 850°C. Coordinates are determined for the eutectic point l
⇆ AlRh + 〈Rh〉 as 70 at.% Rh and 1715°C. The existence of intermediate phases, their crystal structure, and also the method
of forming phases in the field of composition rich in aluminum given in publications are confirmed.
__________
Translated from Poroshkovaya Metallurgiya, Nos. 5–6(449), pp. 48–56, May–June, 2006. 相似文献
65.
研究了(Ba1-xSrx)(Zn1/3Nb2/3)O3微波介质陶瓷温度系数的非线性变化以及异常的原因。根据CM公式,随着系统中Sr(Zn1/3Nb2/3)O3的增多,τc的异常是由于氧八面体的畸变导致的相转变(对称性降低)所造成的(晶体结构由无序立方相向有序赝立方相的连续变化)。相转变的发生相应影响了极化以及极化模式,这是造成τc异常的根本原因。 相似文献
66.
微型构造表征技术在八面河油田的应用 总被引:1,自引:1,他引:0
通过对八面河油田井网密集区及井网稀疏的欠开发区的微构造研究,探讨了微构造表征技术。首先在储层多层次逐级对比的基础上,建立主力油层对比关系;密集井网条件下,则利用钻井资料编制油层顶底微型构造图;对于欠开发地区,通过人机联作自动追踪成图技术,输出2m等值线间隔构造图,建立微构造模型。以微构造模型为基础进行潜力评价,部署关键井寻找优质储量或进行开发动态调整。应用该项技术在八面河油田滚动发现了角15块等断鼻翼部局部高点,增加石油地质储量488×10~4t。 相似文献
67.
The exact magnetization pattern of magnetic films close to a spin-reorientation transition is difficult to analyze due to the intrinsically three-dimensional (3d) variation of the orientation of the local magnetization. We present a technique how this can be performed, based on the analysis of high quality 2d polarization maps from a single scanning electron microscope with polarization analysis (SEMPA) measurement with tilted sample. The key tool is the statistical distribution of all occurring polarization doublets, visualized in a 2d histogram plot. From the shape of the distribution the type of transition—canted-phase, or coexisting phases—can be inferred. For the canted-phase state, the canting angle can be accurately determined from geometrical considerations. With help of the histogram the image data can be analyzed and the three components of the magnetization can be calculated for most points of the image. For a Co/Pt multilayer film we found a cone state. The magnetization forms a complex pattern consisting of out-of-plane domains while the in-plane magnetization shows a maze pattern. 相似文献
68.
基于高抗热震性能的陶瓷刀具材料的微观结构设计 总被引:1,自引:0,他引:1
本文以现有的抗热震断裂和抗热震损伤的评价理论为基础,通过对材料中微裂纹的长度进行预测,从而实现了对陶瓷刀具材料的抗热震性能的微观结构设计。根据此理论对现有材料的抗热震性能的进行预测,预测结果与实际的测量结果相符,验证了该理论的正确性。 相似文献
69.
Sintered Nd-Fe-B magnet was manufactured by advanced equipment via a SC (Strip casting) technology.It has integrative performance. 相似文献
70.
David M. Scott Debendra K. Das Vijayagandeeban Subbaihaannadurai 《Petroleum Science and Technology》2006,24(8):895-909
A finite element scheme is presented to model the dissociation of gas hydrates in porous media by hot water injection. We show a complete derivation of the finite element formulation, including the associated mass and energy conservation equations capable of performing transient analysis of both conductive and convective heat transfer for gas and liquid flow in porous media. The scheme also includes the latent heat effect to accommodate the change of phase due to melting of hydrate. In the companion paper, Part II, this method is successfully applied to hydrate reservoirs. 相似文献