Photo-reversible Reaction in Polymer Langmuir-Blodgett Films

Preparation of photoreactive Langmuir-Blodgett (LB) films was carried out using polymers/oligomers prepared from long-chain dialkyl esters of di-and tetra-olefins and having cyclobutane rings in the main chain. These polymers/oligomers formed stable monolayers on a water surface when mixed with arachidic acid. These monolayers could be deposited onto a substrate successfully forming Y-type films. The oligomer LB films were polymerized on irradiation. The polymer LB films showed a photo-reversible process between polymers and oligomers, depending on wavelength of the irradiating light. On the basis of spectral data and molecular weight change, this behaviour was found to be caused by cleavage and formation of cyclobutane rings.     

微波热液法制备光催化TiO2功能材料

采用微波加热法，研究了钛配离子热分解水解反应的规律。结果表明，水解产物在大气气氛和300℃下煅烧2h，所得产物为锐钛型TiO2粉末。在紫外线照射下，乙酸经Ti02光催化反应12h后，残余量小于初始量的20％。     

砂岩储集层微波加热产生微裂缝的机理及意义

微波加热无需介质传热,具有升温速度快、热惯性小、选择性加热、穿透力强、过程易于控制等优点,已被试验性地应用于石油开采中。但有关微波加热对储集层岩石微观结构影响的研究还很缺乏,限制了该项技术在油气开采领域的广泛应用。通过实验手段研究了微波加热前后砂岩岩样微观结构变化、微裂缝产生机理及特征。结果表明,砂岩在微波加热过程中容易产生微裂缝,且不同岩石的微波加热致裂机理不尽相同,主要包括:矿物失水收缩、颗粒粒间开裂和颗粒内部开裂,低渗透致密砂岩刚性颗粒的粒内开裂作用显著。微波加热产生的微裂缝具非定向特征,即使在应力的作用下有一部分裂缝会发生闭合,但仍有大量微裂缝可以起到增加渗透率的作用。井下微波加热的致裂作用有助于改善近井区域渗流能力,提高低渗透油气藏的开采效率。图4参15     

脉冲功率器件直流和动态热特性探测

介绍了针对影响微波脉冲功率器件可靠性的热性能问题，应用红外热分析技术。对比探测微波脉冲功率器件在动态和直流状态下的温度分布，峰值结温，热阻及其变化规律。     

低功率激光对细胞质膜通透性及细胞功能的影响

目的:探索低功率激光对细胞质膜通透性及细胞功能的影响。方法:以波长为632.8nm,功率密度为5.4mW/cm~2的氦氖激光照射人外周血淋巴细胞15、30、60分钟,并采用钙荧光指示剂Fura—2/Am定量测试法检测淋巴细胞内游离钙浓度和质膜Ca~(2+)—Mg~(2+)—ATP酶活性变化。结果:照射后淋巴细胞内游离钙浓度明显低于正常(P<0.05);同时细胞膜Ca~(2+)—Mg~(2+)—ATP酶活性增加(P<0.05);而且照射后细胞内游离钙浓度降低与质膜上Ca~(2+)—Mg~(2+)—ATP酶的激活呈负相关。结论:低功率激光照射激活细胞膜Ca~(2+)—Mg~(2+)—ATP酶活性,使细胞膜对钙通透性发生变化,且影响到细胞内Ca~(2+)贮存,造成细胞膜通透性和细胞功能的改变。     

Effects of Heat Treatment Temperature and Time on Structure and Static Magnetic Property of W-type Ferrite Hollow Mierospheres

Hollow spheres of hexagonal ferrite BaCozFelrO27 were fabricated through a spray pyrolysis technique using co-precipitation ferrite powder precursor as materials, followed by calcinations in an air atmosphere. The phase composition, micro-morphology, and static magnetic property of the particles were measured by XRD, SEM, and VSM. The results indicate that the method for preparation of ferrite hollow microspheres （FHM） results in a broad particles size distribution. The density of FHM decreased from 5.31 g/ cm^3 to 2.31 g/cm^3. When the heating rate was 5℃/min, and temperature was 1 200℃ for 4 hours, pure W-type ferrites were formed. With the heat treatment temperature and time increasing, the crystal structure becomes perfect, the saturation magnetization is increased and the coercive force is decreased.     

微波辐射电镜生物样品制备方法研究

本文报道一种快速微波辐射电镜样品制备方法──水浴法，以及这个方法在动植物样品超薄切片制备中的应用。实验结果表明，水浴法使得样品可以接受相对较长时间的微波辐射而不致造成任何损伤，浸泡液和样品的温度控制简单而且准确，样品处理的结果内外均匀一致，超微结构保存优秀，完全可与常规制样法和Ｌｏｇｉｎ法的结果相媲美，而且在某些方面水浴法要优于常规法和Ｌｏｇｉｎ法。     

从江苏苏南数字微波线路看广播电视专用网发展前景

新建微波干线电路采用高质量的数字微波设备是广电部科技工作会议的精神之一。本文介绍了江苏苏南数字微波线路，并从方案确定、技术实现、设备选型等方面进行分析比较，从而得到一个合理的整体方案。本文还着重阐述了数字传输的关键设备－编码器的现状与发展趋势，提出广播电视专用网多功能应用的设想。     

我国有线电视事业的现状和发展

本文详细系统地介绍了我国有线是视发展历史和现状，及其经营和管理方法。重点介绍了北美的ＣＡＴＶ技术发展动向。最后，指出我国ＣＡＴＶ事业发展中的应用重视的问题。