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31.
In this work we investigated the mechanism of the electrochemical intercalation reactions in rf sputtered nickel oxide thin films electrodes by two techniques: mechanical stress change measurements by means of an optical technique and mass changes using an electrochemical quartz microbalance (EQCM). The experiments were performed in alkaline electrolytes containing cations of the first column of the periodic table. Reversible mass and volume changes were observed. In order to explain these experimental results, an exchange reaction is proposed, in which the oxidation process is accompanied by the deinteractional of a relative large number of “light” cations, simultaneously with the intercalation of a smaller number of heaviest cations. 相似文献
32.
The magnetic properties of polyethersulfone-matrix composites with 3-19 vol.% polycrystalline nickel filaments (0.4 (im diam)
were investigated. These filaments were found to exhibit hysteresis energy loss 10800 J/m3 of nickel and coercive force 16.9 kA/m, compared to corresponding values of 4930 J/m3 and 4.7 kA/m for 2 μ.m diam polycrystalline nickel fibers, 1020 J/m3 and 0.5 kA/m for 20 μm diam polycrystalline nickel fibers, and 1280 J/m3 and 2.3 kA/m for solid polycrystalline nickel. 相似文献
33.
34.
T. D. M. Weijers H. Timmers R. G. Elliman 《Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms》2002,190(1-4):397-401
The impact of the pulse height deficit effect in gas ionization detectors on the accurate extraction of depth information from heavy ion elastic recoil detection spectra has been investigated. Thin GaN films and GexSi1−x/Si heterostructures have been analyzed with a 200 MeV 197Au beam. Employing an empirical parameterisation of the pulse height deficit, a global energy calibration of the detector can be achieved. Energy spectra have been compared, calibrated with either a constant or a full energy-dependent compensation for the deficit. A constant compensation results in significant distortion of the extracted depth profile for heavier ions, whereas an energy-dependent compensation yields true concentration–depth profiles. 相似文献
35.
水性聚氨酯电导率与聚沉值的研究 总被引:4,自引:0,他引:4
研究了软(硬)段含羧基的水性阴离子纳米聚氨酯体系的n(NCO)/n(OH)比值,COOH的质量分类,反离子各类,合成方法与电导率关系及产生的原因;探讨了该体系的n(NCO)/n(OH)值,COOH的质量分数,合成方法与临界聚沉值(Cc.c)的关系和规律。并分析,比较了软(硬)段含羧基的水性阴离子聚氨酯体系电导率与Cc.c二者关系,得出了随COOH的质量分数升高,二者变化相同,随n(NCO)/n(OH)比值升高,二者变化相反的结论。 相似文献
36.
化学镀镍合金在电子工业中的应用 总被引:5,自引:0,他引:5
对化学镀镍合金铁工艺和性能特性及其在电子工业中的应有委展现状作了评述。化学镀镍合金具有镀层均匀,适用基材广,结合力高,硬度高,优良的耐磨、耐蚀性,可焊性好和特殊的电磁性能等特性,在电子工业中获得了广泛的应用。文中着重介绍了化学镀镍合金在磁盘、电磁屏蔽、微电路、半导体、连接器及薄膜电阻上的应用情况。这些案例说明,合理应用化学镀镍合金技术,有利于提高电子元器件的质量,降低成本,促进技术进步。 相似文献
37.
钛合金的银脆,镉脆敏感性及其控制 总被引:4,自引:0,他引:4
利用慢应变速率拉伸技术(SSRT),并结合恒载实验,较全面地研究了Ti-6Al-4V合金的银脆行为、固态与液态镉脆行为,确定了应变速率、接触条件、热处理制度、试样取向、温度等因素对Ti-6Al-4V合金银脆与镉脆敏感性的影响,探讨了Ni阻挡层对控制Ti-6Al-4V合金和TC11合金银脆开裂的作用。 相似文献
38.
K-S. Park S-H. Park Y-K. Sun K-S. Nahm Y-S. Lee M. Yoshio 《Journal of Applied Electrochemistry》2002,32(11):1229-1233
The structural and electrochemical properties of LiNiO2 powders were investigated as a function of the oxygen flow rate employed in the preparation of lithium nickel oxide. It was found that oxygen played an important role in the synthesis of highly crystallized LiNiO2(R3¯m). In the crystallization process of LiNiO2, a deficiency of oxygen in the calcination reactor induced the formation of impurities and cubic rock-salt structure (Fm3m) in LiNiO2 powders. For LiNiO2 prepared at higher oxygen flow rates, the electrode delivered high discharge capacities with relatively good retention rates. But very low electrode capacity was obtained from LiNiO2 prepared at lower oxygen flow rates. 相似文献
39.
对云母粒子化学镀镍及以LDPE为基材,镀镍云母粒子为填料制备的导电复合材料进行研究。认为此种导电复合材料只有质量轻、强度大及良好的导电等性能。 相似文献
40.
Takashi Kato Tadahiro Kurosawa Takashi Nakamura 《Nuclear instruments & methods in physics research. Section A, Accelerators, spectrometers, detectors and associated equipment》2002,480(2-3):571-590
A simple phenomenological analysis using the moving source model has been performed on the neutron energy spectra produced by bombarding thick targets with high energy heavy ions which have been systematically measured at the Heavy-Ion Medical Accelerator (HIMAC) facility (located in Chiba, Japan) of the National Institute of Radiological Sciences (NIRS). For the bombardment of both heavy ions and protons in the energy region of 100–500 MeV per nucleon, the moving source model incorporating the knock-on process could be generally successful in reproducing the measured neutron spectra within a factor of two margin of accuracy. This phenomenological analytical equation is expressed having several parameters as functions of atomic number Zp, mass number Ap, energy per nucleon Ep for projectile, and atomic number ZT, mass number AT for target. By inputting these basic data for projectile and target into this equation we can easily estimate the secondary neutron energy spectra at an emission angle of 0–90° for bombardment with heavy ions and protons in the aforementioned energy region. This method will be quite useful to estimate the neutron source term in the neutron shielding design of high energy proton and heavy ion accelerators. 相似文献