基于光纤像面全息的金属构件微位移测量

针对激光全息技术能处理常规方法难以解决的问题以及光纤具有环境适应性的特点,设计了一种基于光纤像面全息干涉计量对金属材料构件微小位移测量的方法.通过对不同芯径传像光纤束情况下的成像结果分析,得出了与材料力学相符合的结论.实验结果表明,提出的方案适用于对金属材料特性的高精度测量,可以解决阻碍激光全息技术推广应用和发展的环境要求.     

电热爆炸喷涂法制备TiC涂层的特性分析

采用电热爆炸定向喷涂工艺在镍合金基体上制备TiC涂层,借助光学显微镜、显微硬度计分别对涂层显微组织、涂层硬度进行了测试。利用图像分析软件对涂层的晶粒尺寸进行了测量。结果表明,电热爆炸定向喷涂制备的涂层组织晶粒明显细化,涂层组织为典型的快速凝固组织。涂层组织比原始喷涂材料镍合金组织细小、均匀;TiC涂层中大晶粒所占涂层面积为93.6%,小晶粒所占面积为6.4%;大晶粒的弦长平均值为500 nm左右,小晶粒的弦长平均值为81 nm左右;表层有些孔隙;涂层硬度均明显高于基体材料镍合金的硬度,其最高硬度达到了582.5 HV。     

关于基体曲率的热障涂层残余应力分析

采用空心和实心四相同心圆模型,导出了轴对称温度应力状态下的位移公式,分析了基体曲率对热障涂层残余应力的影响。结果表明:热障涂层结构中各层内既有环向应力,又有径向应力,应力大小与温降成线性关系;当陶瓷层在外层时,在氧化层/陶瓷层和粘结层/氧化层界面上产生垂直界面的拉应力,且实心模型的拉应力远大于空心模型的拉应力;当陶瓷层在里层时,空心模型中相应界面上的应力为压应力。     

一维光子晶体光开关的研究

由掺杂非线性介质的一维光子晶体形成光开关,并利用传输矩阵法对其特性进行了分析。研究发现,该结构可以很好地完成光开关的功能。     

基于容量的相对最小影响资源分配算法

在对现有的波长资源分配算法进行了研究和分析的基础上,提出了一种基于容量的相对最小影响波长资源分配算法.该算法通过定义基于容量的影响因子,分析受当前波长分配影响之后各路径在各波长上的可用信道数,更为精确地描述了当前分配波长对于受影响路径的路径容量产生的影响.仿真结果表明,新的算法降低了网络阻塞率,提高了网络资源利用率.     

儿茶素在离子交换纤维上的扩散机理研究

研究了静态下儿茶素在自制的聚丙烯基阴离子交换纤维上的扩散机理。结果表明，离子交换纤维对儿茶素的吸附主要以扩散而不是以交换为主控步骤．在反应的初期．以液膜扩散为主，反应3min后．以孔隙扩散控制为主。     

陶瓷电容器的制备工艺概述

简介了新型陶瓷电容器的优点、功能、类型和发展现状及表面层陶瓷电容器、表面层型陶瓷电容器和晶界型陶瓷电容器的产生机理和区别，和影响陶瓷电容器性能的诸多因素，如显微结构、掺杂元素和包覆改性等；回顾了国内外陶瓷电容器的烧成工艺发展历史，如高温一次烧成、低温一次烧成、独石法和激光辐射法等；展望了陶瓷电容器在21世纪的研究和应用前景。     

两步干法腈纶工艺聚合反应配方的特点

对恒定反应条件下 ,两步干法腈纶工艺不同聚合产率配方中各物料的用量进行了分析 ,提出了物料用量的选择依据与合理范围。从反应机理上探讨了中和剂与终止剂的作用本质 ;HSO3- /SO4 -·比例可以作为催化剂用量选择范围的代用指标 ;受亚磺酸稳定性的影响 ,第三单体用量随反应产率的提高而显著下降。     

我国涂料市场的发展现状及趋势

从我国需求旺盛的涂料市场、涂料产品的结构等方面,阐述了我国涂料市场发展的商机;指出环保型防腐涂料的发展方向。     

Study on volume ratio and plasticizer screening of free coating membranes composed of ethyl cellulose and chitosan

The aim of this study was to optimize the formula of free blended coating membrane of ethyl cellulose (EC) and chitosan (CS), including their suitable ratio range and the best plasticizer used. The dry films were produced by a casting/solvent evaporation method, with different volume ratio of EC and CS solution plasticized by various plasticizers, respectively. The wet films were prepared by immersing dry films in pH 6.8 phosphate buffer saline (PBS) for 24 h. The promising ratio range of EC/CS was below 20/5 or 20/6 with various plasticizer, which was determined by comparing the viscosity of the blended solutions and the morphology of the blended films. The efficiency of plasticization was evaluated by measuring glass transition temperature (T_g). All the testing plasticizers have good compatibility with EC or CS and dibutyl phthalate (DBP) have the strongest efficiency inducing the lowest T_g (39.9°C) of the film. Mechanical properties were evaluated by the ratio of tensile strength (T) to elastic modulus (E). In the wet state, the films with DBP had the highest T/E value (1.2). The results of leaching of plasticizers also verified that DBP was the most stable plasticizer in the films. The release rates of tetramethylpyrazine phosphate (TMPP) through the pellets coated with the blended films of EC/CS (20 : 6 v/v) plasticized by various plasticizers showed that the more water‐soluble the plasticizer was, the more quickly TMPP dissolved from the coated pellets, which further indicated that the water‐insoluble plasticizers (such as DBP) could be more applicable to keep the sustained or controlled release property of the blended films in wet state. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 1932–1939, 2006