宽频介电谱仪热激励去极化电流功能研究

利用宽频介电谱仪拓展热激励去极化电流模块测量介质材料的TSDC操作简单实用,它不仅容易把材料中的各种不同活化能或弛豫时间的荷电粒子区分开,并且能从TSDC谱中直接得出被测材料的介电性能以及相关微观参数,这为研究材料内部机理提供了一条捷径。     

凝析气藏相态参数实验研究

油气藏流体主要有烃类成分组成,在油藏及地面条件下,这种烃类混合物的物理性质取决于其化学成分及给定的温度和压力。对于烃类的相态特征及流体组分研究在油气田开发中具有重要的意义,尤其是凝析气藏田。对海榆和10井的研究,归纳总结其流体PVT性质,为其开发提供科学依据。     

钴钇掺杂（Ba,Sr）TiO_3基介电陶瓷的制备与性能研究

采用二次固相反应法制备Ba0.7Sr0.3TiO3介电陶瓷,研究了掺杂钴、钇离子对钛酸锶钡介电性能的影响。结果表明,陶瓷样品Y3＋、Co3＋的最佳掺杂浓度分别为0.04mol%和0.05mol%,最佳烧结温度为1340℃,样品的相对介电常数为4200,介电损耗（tanδ）为0.005。样品的结构为四方晶系,P4mm空间群。获得了高介电常数、低损耗的Ba0.7Sr0.3TiO3介电陶瓷。     

The influence of oleic acid on the hydration and mechanical properties of portland cement

To investigate the effects of OA on the portland cement using oleic acid （OA） as grinding aid and the effects of OA on the portland cement, we characterized the different perfermances of the cement, discussed the characteristics of properties. The results reveal that the OA can reduce the water requirement of normal consistency. With the content of OA added, setting time was extended. The OA can significantly improve the rheological properties of cement-based materials, while the compressive strength decreases.     

构树果红色素的提取及其理化性质的研究

介绍了用乙醇从构树果中提取红色素的过程,并对其理化性质也进行了试验,实验结果表明,提取方法简单、实用,红色素易溶于水和乙醇,在中性和酸性介质中,对光、热、多数金属离子以及蔗糖、葡萄糖等食品添加剂都是稳定的,具有开发价值。     

Coinage Metals in the Nanometer Length Scale

Cetylpyridinium chloride (CPC)-stabilized gold organosol in toluene has been prepared by using a two-phase (water-toluene) extraction of AuCl₄^- followed by its reduction with sodium borohydride in the presence of the surfactant, CPC. The surfactant-stabilized gold nanoparticles were exploited to examine their optical properties when exposed to various solvent systems by measuring the changes in the localized surface plasmon resonance (LSPR) spectrum.     

Helium gas permeability of montmorillonite/epoxy nanocomposites

Helium gas permeability of silicate clay (montmorillonite) particles/epoxy nanocomposites was examined. The incorporation of increasing amounts of montmorillonite particles reduced the helium gas permeability. Based on Fick’s law, gas permeation behavior of the nanocomposite was evaluated. With the increase of montmorillonite loading, gas diffusivity decreased, while gas solubility increased. Helium diffusion behavior is in agreement to the numerical results based on the Hatta–Taya–Eshelby theory. It has been revealed that dispersion of nanoscale platelets in polymer is effective in improving gas barrier property.     

Micro- and nano-scale deformation behavior of nylon 66-based binary and ternary nanocomposites

The primary aim of this paper is to provide an insight on the effect of the location of organoclay on the micro- and nano-scale deformation processes in melt-compounded nylon 66/organoclay/SEBS-g-MA ternary nanocomposites prepared by different blending sequences. In addition, the deformation processes of the ternary nanocomposites were compared to the binary nanocomposites (nylon 66/organoclay and nylon 66/SEBS-g-MA) and neat nylon 66. The incorporation of SEBS-g-MA particles toughened nylon 66 markedly; but the flexural modulus and strength were both reduced. Conversely, the use of organoclay increased the modulus but decreased the fracture toughness of nylon 66. Nylon 66/SEBS-g-MA/organoclay ternary nanocomposites exhibited balanced elastic stiffness and toughness. Stress-whitening studies of the fracture surfaces in terms of gray level were also performed and an attempt was made to correlate the optical reflectivity characteristics with fracture toughness. It was concluded that the capability of SEBS-g-MA particles to cavitate was decreased by the presence of organoclay in the SEBS-g-MA phase, resulting in reduced toughening efficiency. The best micro-structure for toughness and other mechanical properties is thus to maximize the amount of exfoliated organoclay in the nylon 66 matrix rather than to have it embedded in the finely dispersed SEBS-g-MA particles.     

SHS结合热压制备TiC-Al2O3/Fe-Al复合材料

以天然钛铁矿、铝粉和石墨为主要原料,采用自蔓延高温合成技术、铝热还原法并结合热压烧结技术,制备出TiC—Al2O3／Fe—Al复合材料．研究表明：预热时间少于120s时,预热时间越长,反应燃烧波速度越大,当预热时间继续增大,对反应燃烧波速度的影响不再显著;加入添加剂Y2O3为0．2％时,金属相较均匀地弥散分布在陶瓷颗粒周围．晶粒尺寸约为2～3μm,复合材料的相对密度达到94％,抗弯强度和硬度分别为599．29MPa、83．7HRA．     

Strain rate sensitivity of tensile properties in high Nb containing TiAl alloys

The effect of strain rate on the yield strength of high Nb containing TiAl alloy was studied. The results show that the strain rate sensitivity varies with the test temperature, and the yield strength is not sensitive to the strain rate at room temperature but significantly sensitive to the strain rate at high temperature. An increase of the strain rate or a decrease of the temperature results in an obvious change of fracture mode. It is found that the strain rate sensitivity of this alloy varying with temperature is due to the dislocation climb generated at high temperature.