全文获取类型
收费全文 | 13957篇 |
免费 | 1690篇 |
国内免费 | 982篇 |
专业分类
电工技术 | 637篇 |
综合类 | 772篇 |
化学工业 | 2863篇 |
金属工艺 | 3173篇 |
机械仪表 | 598篇 |
建筑科学 | 72篇 |
矿业工程 | 145篇 |
能源动力 | 360篇 |
轻工业 | 1291篇 |
水利工程 | 7篇 |
石油天然气 | 153篇 |
武器工业 | 145篇 |
无线电 | 1375篇 |
一般工业技术 | 2307篇 |
冶金工业 | 1166篇 |
原子能技术 | 1363篇 |
自动化技术 | 202篇 |
出版年
2024年 | 60篇 |
2023年 | 329篇 |
2022年 | 607篇 |
2021年 | 666篇 |
2020年 | 625篇 |
2019年 | 606篇 |
2018年 | 595篇 |
2017年 | 624篇 |
2016年 | 546篇 |
2015年 | 514篇 |
2014年 | 696篇 |
2013年 | 930篇 |
2012年 | 829篇 |
2011年 | 947篇 |
2010年 | 657篇 |
2009年 | 742篇 |
2008年 | 689篇 |
2007年 | 948篇 |
2006年 | 806篇 |
2005年 | 670篇 |
2004年 | 653篇 |
2003年 | 505篇 |
2002年 | 368篇 |
2001年 | 325篇 |
2000年 | 284篇 |
1999年 | 245篇 |
1998年 | 188篇 |
1997年 | 185篇 |
1996年 | 162篇 |
1995年 | 104篇 |
1994年 | 93篇 |
1993年 | 96篇 |
1992年 | 75篇 |
1991年 | 57篇 |
1990年 | 37篇 |
1989年 | 37篇 |
1988年 | 22篇 |
1987年 | 9篇 |
1986年 | 8篇 |
1985年 | 12篇 |
1984年 | 6篇 |
1983年 | 4篇 |
1982年 | 31篇 |
1981年 | 20篇 |
1979年 | 4篇 |
1978年 | 4篇 |
1977年 | 2篇 |
1976年 | 2篇 |
1959年 | 1篇 |
1951年 | 4篇 |
排序方式: 共有10000条查询结果,搜索用时 15 毫秒
31.
Electric and mechanical performances of Bi0.5Sb1.5Te3 prepared by spark plasma sintering 总被引:1,自引:0,他引:1
Thermoelectric (TE) materials are a kind of functional materials which can be used to convert directly heat energy to electricity or reversely.The thermoelectric effects hold great potential for application in power generation and refrigeration.Bi2Te3 and its alloys are well known as best TE materials currently available near room temperature.This paper studies respectively the effects of spark plasma sintering (SPS) on electric performance of Bi0.5Sb1.5Te3 thermoelectric materials that are prepared through vacuum melting and ball milling.Through X-ray Diffraction and cold field emission scanning electric microscope s4800, the phase constituent and microstructure of the TE materials samples were analyzed.Electric conductivity and power factor can be improved with the rise of Spark Plasma Sintering temperature (from 300 to 500 ℃) and pressure(from 30 to 60 MPa), and the density and mechanical strength of Bi0.5Sb1.5Te3 thermoelectric material increase, too. 相似文献
32.
Quantification of trace amounts of impurities in high purity cobalt by high resolution inductively coupled plasma mass spectrometry 总被引:2,自引:0,他引:2
XIE Hualin HUANG Kelong NIE Xidu TANG Yougen 《稀有金属(英文版)》2007,26(3):286-291
An analytical method using high resolution inductively coupled plasma mass spectrometry (HR-ICP-MS) for rapid simultaneous determination of 24 elements (Be, Mg, Al, Ti, V, Cr, Mn, Fe, Ni, Cu, Zn, Ga, Ge, As, Se, Mo, Ag, Cd, Sn, Sb, Ba, Pt, Au, and Pb) in high purity cobalt was described. Sample digestions were performed in closed microwave vessels using HNO3 and HCl. The matrix effects because of the presence of excess HCl and Co were evaluated. The usefulness of high mass resolution for overcoming some spectral interference was demonstrated. The optimum conditions for the deter- mination were tested and discussed. The standard addition method was employed for quantitative analysis. The detection limits were 0.016-1.50 μg?g?1, the recovery ratios were 92.2%-111.2%, and the RSD was less than 3.6%. The method was accurate, quick, and convenient. It was applied to the determination of trace impurities in high purity cobalt with satisfactory results. 相似文献
33.
用普通反应热压方法(RHP)和反应放电等离子体方法(R-SPS)原位反应制备了ZrB2-SiC,ZrB2-SiC—ZrC,ZrB2-SiC-ZrN,以及ZrB2-SiC-AIN4种复合材料。从密度,物相以及显微结构等方面比较了两种烧结方式之间的差别,对于升温速度较慢的普通热压方法,反应分步进行,显微结构不均匀;对于升温速度快的放电等离子体烧结,原料间的自蔓延反应被点着,反应速度快,显微结构均匀。同时以红外灯的热量为点火源,引发了Zr,Si及B4C间在空气气氛下的自蔓延反应,制备了较纯及粒径约为1μm的活性粉体。 相似文献
34.
CHENFei ZHAHGYue-fei LiuYu TANGBin PANJun-de 《材料热处理学报》2004,25(5):401-404
This paper introduces a new titanium alloys surface strengthening treatment by using the arc-added glow discharge plasmas non-hydrogen carburization technique. High purity and high strength graphite is selected as cooling cathode arc source for supplying carbon atoms and particle, which migrate to the titanium alloy(Ti6Al4V) surface and form modified layer. Thus, the hydrogen embrittlement is avoided while the tfibological behavior of the titanium alloy surface is improved in the respects of anti-friction and anti-wear ability.The tribological behavior of the modified layer under dry sliding against SAE52100 steel was evaluated on a ball-on-disc test rig. The results showed that the modified layer obtained a thickness of 30μm at 980℃, 30minutes. The microhardness of the Ti6Al4V alloy surface attained 936 HV, which was much larger than that of the Ti6AI4V alloy. The Ti6AI4V alloy was characterized by adhesion wear and scuffing under dry sliding against the steel, while the surface modified layer experienced much abated adhesion wear and scuffing under the same testing condition. This could be attributed to the carbon dement with different modalities exists in the modified layer.The modified layer showed good friction-reducing and fair anti-wear ability in dry sliding against the steel. Using the SEM,XRD and XPS, the phase structure and morphology of the carburization modified layer was analyzed. 相似文献
35.
研究了Ni-Cr-B-Si合金粉末等离子喷涂层的高温抗氧化性能、耐磨性、热稳定性,并介绍了其在连杆毛坯滚锻模上的应用.结果表明,这种涂层的某些高温性能大大优于5CrNiMo钢,在冲击载荷不大的场合,可以作为热锻模的强化方法. 相似文献
36.
Microwave plasma is studied as an alternative to oil or gas fuel for ignition and stabilisation of burning of lean coal. The study is performed on an experimental set-up, which includes a burner with a microwave plasma generator, coal and air supply systems, and measurement equipment. Power and thermochemical characteristics of the coal-plasma interaction have been measured and analysed. The obtained results indicate an essential intensification of ignition and combustion processes in the microwave burner compared to those in conventional burners. In particular, it has been demonstrated that the microwave energy consumption is only about 10% of the required expenditure of oil or gas, measured in heat equivalent. A design of an industrial microwave-plasma burner is proposed. Prospects of such burner for applications at industrial boilers of power plants are discussed. 相似文献
37.
38.
Rapid Reactive Synthesis and Sintering of Submicron TiC/SiC Composites through Spark Plasma Sintering 总被引:1,自引:0,他引:1
Lianjun Wang Wan Jiang Lidong Chen Shengqiang Bai 《Journal of the American Ceramic Society》2004,87(6):1157-1160
Submicrometer TiC/SiC composites were fabricated by a rapid reactive sintering process through spark plasma sintering (SPS) technique using the carbon, titanium, and nanosized-SiC powders without any additive. It was found that the composite could be sintered in a relatively short time (8 min at 1480°C) to 97.9% of theoretical density. After sintering, the phase constituents and microstructures of the samples were analyzed by X-ray diffraction techniques and observed by scanning electron microscopy. The effect of nanosized and microsized SiC additives on the microstructure of TiC/SiC composites was investigated. 相似文献
39.
Several low‐powered gas plasmas were employed to treat a biomedical poly(ester)urethane using the treatment gases of CO2, O2, NH3, and SO2 with different treatment time (2, 5, 10, and 15 min). The changes of the physical and chemical characteristics of the biopolymer surface were studied. Surface morphology was evaluated by scanning probe microscopy, which showed increased roughness of the surface after plasma treatment. The wettability of the surface was examined by static water contact angle (SCA) measurements, which presented that there was a decrease of SCA in all plasma treatments compared with the untreated surface and that each gas plasma had an optimum treatment time accompanied by a minimum contact angle. X‐ray photoelectron spectroscopy indicated the changes of the surface functional groups. The data demonstrated that CO2 and O2 plasmas resulted in the incorporation of oxygen‐containing groups, while NH3 plasma resulted in the combination of nitrogen‐containing groups, and SO2 plasma resulted in the formation of sulfur‐containing groups. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 1273–1282, 2006 相似文献
40.
等离子体煤热解与气化工艺的研究进展 总被引:11,自引:1,他引:11
介绍了煤在热等离子体中转化为小分子化合物的2个重要过程,即等离子体煤热解和气化的基本原理、应用及发展状况。在非氧化性气氛中,煤热解生成的气体产物主要是乙炔、氢气、一氧化碳,此外还有甲烷和乙烯等小分子烃,乙炔的收率与煤种、粉煤粒度、反应器结构、粉煤进料方式、进料速度及操作条件密切相关,等离子体中氢的存在有利于乙炔的产生;在氧化性气氛中,煤气化产物主要是一氧化碳和氢气,煤中碳的转化率达95%,合成气体积分数约85%,二氧化碳体积分数低于5%。指出等离子体应用于煤转化过程是煤洁净利用的有效方式,具有潜在的工业化应用前景。 相似文献