Preparation and Properties of Sintering Additives Coated Si3N4 from Heterogeneous Nucleation Processing

The sintering additives such as Al2O3 and /or Y2O3 were coated on the surfaces of Si3N4 particles via heterogeneous nucleation processing using a buffered pH solution as the precipitation reagent .They nucleated and grew only on the surfaces of Si3N4 and did not form sol particles in solution by TEM observation .The isoelectric point(IEP) of coated Si3N4 was different from that of as-received Si3N4.The IEP of Al(OH)3-coated Si3N4 occurred at pH8.4, which is close to that of alumina .When Al(OH)3-coated Si3N4 particles were coated with Y(OH)3,the IEP of coated Si3N4 powder shifted from pH8.4 to pH9.2 ,similar to that of yttria.In addition ,the rheological data showed that Al2O3 and /or Y2O3 coated Si3N4 suspension is nearly Newtonian and that added Si3N4 suspension shows a shear rate thinning behavior.     

用废旧橡胶生产精细胶粉的空气涡轮制冷低温粉碎法

利用先进的空气涡轮制冷系统，在低温条件下，将废旧橡胶进行冷冻，粉碎，制成60目以上细度的精细胶粉，此法简称ATCG法，它的冷冻能耗成本仅为国际上通用的液氮法的十分之一，整个工艺过程不产生二次污染，为精细胶粉的制取开辟了一条新途径。     

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本文结合实际资料,对内蒙古赤峰热水镇温泉天然气的地球化学特征进行了分析和研究。结果表明:上述天然气由多种成因气体组合而成。其中He属壳源放射性成因,CO_2属有机成因,CH_4属无机合成,N_2属大气成因。     

Failure analysis of a hot extrusion die used for Al-Li alloy processing

Al-Li alloys being developed as lighter, substitutes for conventional high strength Al alloys are to be processed by routine methods. During extrusion of a 8090 Al-Li alloy, the extrusion die container failed causing some alarm. This failed die container was analysed to examine if the failure was caused by interaction of Li diffusing out of Al-Li alloy with the carbides of die steel. The evidence, although not conclusive, is sufficient to exercise caution during such processing.     

抗高温磨损高铬铸铁的研究

经Mo、B、V、Ti合金化和RE变质处理的高铬铸铁，具有优良的抗高温磨损性能和强韧性，用于制造筛分高温烧结矿的振动筛筛板，使用寿命比ZG30Cr18Mn12Si2N耐热钢筛板提高2倍以上。多元高铬铸铁筛板制造工艺简单，成本低，值得在筛分领域推广使用。     

连铸铝镇静钢的钢水准备

在连铸生产铝镇静钢时,水口絮流一直是困扰工程技术人员的一个难题.从絮流的原因入手,分析了Al2O3生成的控制.并介绍了几种钢水钙化的方法,从中比较出用复合造渣材料来解决浇铸铝镇静钢的优点.     

HAP陶瓷合成的研究

本文对生物陶瓷材料－羟基磷灰石的合成进行了研究。试验将激光合成与湿法合成对比分析，着重探讨了在激光辐照下生物陶瓷的形貌，粒度，化学组成和结构等的变化规律，对激光涂敷生物陶瓷涂层有一定的指导意义。     

Li2O在保护渣中的作用

采用在不同玻璃性的两种基渣中加入Ｌｉ２Ｏ为研究Ｌｉ２Ｏ对保护渣粘度，熔化温度及玻璃性能的影响，并对Ｌｉ２Ｏ改善保护渣玻璃性的机理进行了探讨，提出了寻找高速连铸保护渣中Ｌｉ２Ｏ的代用物的一种方法。     

Recrystallization/precipitation behaviour in microalloyed steels

Microalloyed high-strength low-alloy (HSLA) steels contain additions of Nb, V, Ti, or in combination, in amounts of 0.01 to 0.1 weight percent to improve mechanical properties, which are strongly dependent on the thermomechanical interaction taking place in the course of rolling mill processes. The recrystallizatian of hat-twisted austenite has been investigated in a cylindrical specimen (f 6×50 mm) machined from hat rolled plates of 0,052 wt % Niobium microalloyed steel. Continuous and interrupted torsion test were carried out in the temperature range 1123 K to 1173 K after a solution treatment of 1.5 minutes at 1423 K and torque-twist data were analysed. The various methods were discussed for obtaining results from torsion tests. The effect of precipitation kinetics was appreciated by way of connection t_p/t_p(red), where t_p is the experimental measured time for the peak stress and t_p(red) is the newly defined reduced time. The softening ratio X and time t_0.05R for start of static recrystallization were established.

The correlation between precipitation and recrystallization is presented as a graphs for chosen requirements (temperature of austenitization, carbon and niobium content and strain rate). If temperature goes below 850°C, the restoration processes are hardly suppressed, both are limited by diffusion and Nb(CN) precipitation, which are extended dynamically in the range of strains rates 10⁻² to 1 s⁻¹.

In the present paper, an attempt is made to derive the PRTT diagram and to define all mathematical equations for describing recrystallization times t_0.05R, t_0.5R, t_0.95R and t_0.05P for the start of precipitation. In real metal forming processes such as the hot rolling of plates or strips the knowledge of these parameters and results is extremely important for the the correct microstructure and sheet quality to be obtained.     

XH－Ⅰ型岩石铵梯炸药研究

文章论述利用过期火药的一种新途径。在２号岩石铵梯炸药中加入粉碎的过期火药以代替部分梯恩梯，制成一种ＸＨ－Ⅰ型岩石铵梯炸药，适用于各种爆破工程。并具有较高的经济效益和社会效益。