磷系水质稳定剂的合成和应用

介绍了国内外磷系水质稳定剂的现状和发展，重点讨论了作为水质稳定剂的聚磷酸钠、有机多元膦酸、膦羧酸以及磷酸酯的合成和应用。     

Synthesizing Energy-Efficient Embedded Systems with LOPOCOS

In this paper, we introduce the LOPOCOS (Low Power Co-synthesis) system, a prototype CAD tool for system level co-design. LOPOCOS targets the design of energy-efficient embedded systems implemented as heterogeneous distributed architectures. In particular, it is designed to solve the specific problems involved in architectures that include dynamic voltage scalable (DVS) processors. The aim of this paper is to demonstrate how LOPOCOS can support the system designer in identifying energy-efficient hardware/software implementations for the desired embedded systems. Hence, highlighting the necessary optimization steps during design space exploration for DVS enable architectures. The optimization steps carried out in LOPOCOS involve component allocation and task/communication mapping as well as scheduling and dynamic voltage scaling. LOPOCOS has the following key features, which contribute to this energy efficiency. During the voltage scaling valuable power profile information of task execution is taken into account, hence, the accuracy of the energy estimation is improved. A combined optimization for scheduling and communication mapping based on genetic algorithm, optimizes simultaneously execution order and communication mapping towards the utilization of the DVS processors and timing behaviour. Furthermore, a separation of task and communication mapping allows a more effective implementation of both task and communication mapping optimizationsteps. Extensive experiments are conducted to demonstrate the efficiency of LOPOCOS. We report up to 38% higher energy reductions compared to previous co-synthesis techniques for DVS systems. The investigations include a real-life example of an optical flow detection algorithm.     

聚苯硫醚酰胺的合成与表征

用4-氯苯甲酰4′-氯苯胺和硫化钠为原料在常压下合成了聚苯硫醚酰胺,并对其进行了表征。结果表明所合成的产物为结晶性聚合物,并且有较高的热稳定性。     

一种新型有机锗化合物的合成及其抗癌性

癌症是当今人类疾病中的第一杀手,寻找新的药物预防和医治癌症是21世纪有机化学的重要研究课题之一。本文报道了一种新型有机锗化合物的合成,它对肺腺癌细胞生长抑制率达88%。     

重新认识摩天大楼的安全性--9·11撞击事件给人的反思

9·11恐怖撞击事件,促使人们重新认识摩天大楼的安全性,由于这类建筑规模越大,其安全性受到的损害就越大,同时也带来其他方面的问题.因此,为减少灾害发生后的损失,必须控制其规模,确保摩天楼建设有序进行.     

Al2O3基耐磨陶瓷涂层的燃烧合成与应用

介绍了燃烧合成表面涂层技术的基本原理 ,开发了相应的制备工艺 ,并在此基础上研制了内覆陶瓷涂层的复合钢管、弯管及弯头。陶瓷涂层主要由α Al2 O3相、部分FeO·Al2 O3相和 3Al2 O3·2SiO2 相组成 ,采用添加剂可以有效提高熔体的流动性 ,使陶瓷的凝固和结晶过程得到进一步控制 ,有助于减少孔隙 ,提高陶瓷涂层的致密度。现场应用试验表明 ,涂层具有较好的耐磨性能 ,可使设备的使用寿命大为延长     

Synthesis, structure and fluorescence properties of a highly stable indium(III)-2,5-pyridinedicarboxylate coordination polymer

The hydrothermal reaction of 2,5-pyridinedicarboxylic acid (H₂PDC), diethylene triamine and In(NO₃)₃·4.5H₂O gave rise to a two-dimensional (2D) coordination polymer In(OH)(2,5-PDC). This compound crystallizes in the orthorhombic space group Iba2, with cell parameters, a = 12.656(3) Å, b = 20.114(4) Å, c = 6.2216(1) Å, V = 1583.9(5) Å³ and Z = 8. Its structure contains one-dimensional In–O–In–O– chains, which are further linked by 2,5-PDC ligands into a 2D supramolecular neutral framework. The adjacent 2D layers are parallel with each other and construct a three-dimensional framework via hydrogen bands. At room temperature, the compound exhibits intense photoluminescence. On the basis of the results of TG/DTA analyses, the structure is thermally stable up to 390 °C.     

Hydrothermal synthesis and in situ surface modification of boehmite nanoparticles in supercritical water

In situ surface modification of boehmite (AlOOH) nanoparticles during hydrothermal synthesis in supercritical water was examined by adding CH₃(CH₂)₄CHO and CH₃(CH₂)₅NH₂ as modifier reagents to the reactants. Changes in surface properties of the nanoparticles by surface modification was observed by FTIR, dispersion in solvents and TEM analyses, which demonstrated that reagents chemically binded onto the surface of the AlOOH nanoparticles. The results of SEM and TEM pictures show that the surface modification affects crystal growth and reduces the particle size and changes the morphology of the particles.     

蒸馏与减粘热联合装置的设备腐蚀及防护

介绍了锦西石化分公司南蒸馏与减粘热联合装置炼制辽河高酸值原油及带炼高硫进口油在 2 0 0～40 0℃范围内对设备、管线和阀门的腐蚀特点、腐蚀机理以及针对高温环烷酸腐蚀所采取的防护措施。通过试验和理论分析 ,提出了应用新材料和新工艺解决减粘后高温渣油系统的腐蚀及低温露点腐蚀的建议     

杂氮硅三环化合物的合成与生物活性

综述了近10年来杂氮硅三环化合物的合成方法和生物活性研究进展，并简要介绍了生物活性和化合物结构的关系。