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Poroussilicon(PS)wasfoundtoemitvisibleluminescenceatroomtemperaturebyCanhamin1990[1].Thisphenomenonimpliedapotentialapplicati... 相似文献
35.
通过对某特钢厂破裂的结晶器铜管进行金相实验、扫描电镜和能谱分析,并结合结晶器的生产、使用及失效过程情况,综合受力分析,认为铜管破裂原因主要是环境介质硫渗入形成硫化物,在拉应力作用下,裂纹沿脆性质点扩展导致的破坏。 相似文献
36.
lpcvd polycrystalline silicon films were deposited on thermally oxidized silicon as well as onlpcvd silicon nitride deposited on silicon. Acw argon ion laser was used to recrystallize the polysilicon film into large grains (grain size from 5μm to 40μm). Boron was then implanted and standard N-channel silicon gate process and N-channel metal gate process were carried out
to realisemosfets on this material. Channel mobilities upto 450 cm2/V-sec for electrons have been measured. This thin filmmosfet has a four-terminal structure with a top and a bottom gate and the influence of one gate on the drain current due to the
other gate has been investigated. Comparison of theI
D
v-V
D
curves of the devices with physical models was found in good agreement. 相似文献
37.
The oxidation behavior of Ti-Si alloys (0.25, 0.5, and 1 Wt. % Si) was investigated between 550 and 700°C; in oxygen by continuous thermogravimetry for a maximum duration of about 500 hr and, in air by daily weighing for durations from a few hundred to several thousand hours. The kinetics results revealed that the presence of silicon leads to a decrease in oxidation rate which is more evident when the temperature is raised and the silicon content is increased. Morphological and structural examinations revealed that silicon modifies the internal architecture of oxide layers when compared with unalloyed titanium; in particular, reduced porosity in the layers is observed. Analysis showed that silicon is uniformly distributed in the oxide layer. However, while part of the silicon is in solid solution in the rutile, some is also precipitated as small crystals ( <1 m at 850°C) of SiO2, of cristobalite structure. The adherence of oxide layers to the metal substrate was measured after cooling of samples; the addition of silicon has been observed to modify, in a manner dependent on its content, the adherence of oxide layers. 相似文献
38.
Silicon Nitride Derived from an Organometallic Polymeric Precursor: Preparation and Characterization 总被引:1,自引:0,他引:1
Wayde R. Schmidt Vijay Sukumar William J. Hurley Jr. Roberto Garcia Robert H. Doremus Leonard V. Interrante Gary M. Renlund 《Journal of the American Ceramic Society》1990,73(8):2412-2418
Partially crystalline Si3 N4 , with nanosized crystals and a specific surface area greater than 200 m2 /g, is obtained by pyrolysis of a commercially available vinylic polysilane in a stream of anhydrous NH3 to 1000°C. This polymer does not contain N initially. Crystallization to high-purity α-Si3 N4 proceeds with additional heating above 1400°C under N2 . The changes in crystallinity, powder morphology, infrared spectra, and elemental compositions, for samples annealed from 1000° to 1600°C under N2 , are consistent with an amorphous-to-crystalline transformation. Although macroscopic consolidation and local densification occur at 1400°C, volatilization and accompanying weight loss limit bulk densification. The effect of temperature on specific surface area is examined and related to the sintering process. These results are applicable to pyrolysis, decomposition, and crystallization studies of ceramics synthesized by polymeric precursor routes. 相似文献
39.
Preparation of Silicon Carbide/Aluminum Nitride Ceramics Using Organometallic Precursors 总被引:1,自引:0,他引:1
Corinna L. Czekaj Michael L. J. Hackney William J. Hurley Jr. Leonard V. Interrante Gary A. Sigel Paul J. Schields Glen A. Slack 《Journal of the American Ceramic Society》1990,73(2):352-357
Solid solutions of 2H -SiC/AlN can be prepared at temperatures less than 1600°C by rapid pyrolysis ("hot drop") of mixtures of [(Me3 Si)0.80 ((CH2 =CH)MeSi)1.0 (MeHSi)0.35 ] n (VPS) or [MeHSiCH2 ] n (MPCS) with [R2 AlNH2 ]3 , where R=Et, i -Bu or simply by slow pyrolysis of the precursor mixture in the case of [Et2 AlNH2 ]3 . In contrast, slow pyrolysis of mixtures of VPS or MPCS with [ i -Bu2 AlNH2 ]3 yields a composite of 2 H -AlN and 3 C -SiC at 1600°C, which transforms into a single 2 H -SiC/AlN solid solution on heating to 2000°C. The influences of the nature of the precursor and processing conditions on the structure, composition, and purity of the SiC/AlN materials are discussed. 相似文献
40.