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121.
122.
The reaction between the Sn-Ag-Cu solders and Ni at 250°C for 10 min and 25 h was studied. Nine different Sn-Ag-Cu solders,
with the Ag concentration fixed at 3.9 wt.% and Cu concentrations varied between 0.0–3.0 wt.%, were used. When the reaction
time was 10 min, the reactions strongly depended on the Cu concentration. At low-Cu concentrations (≦0.2 wt.%), only a continuous
(Ni1−xCux)3Sn4 layer formed at the interface. When the Cu concentration increased to 0.4 wt.%, a continuous (Ni1−xCux)3Sn4 layer and a small amount of discontinuous (Cu1−yNiy)6Sn5 particles formed at the interface. When the Cu concentration increased to 0.5 wt.%, the amount of (Cu1−yNiy)6Sn5 increased and (Cu1−yNi6)6Sn5 became a continuous layer. Beneath this (Cu1−yNiy)6Sn5 layer was a very thin but continuous layer of (Ni1−xCux)3Sn4. At higher Cu concentrations (0.6–3.0 wt.%), (Ni1−xCux)3Sn4 disappeared, and only (Cu1−yNiy)6Sn5 was present. The reactions at 25 h also depended strongly on the Cu concentration, proving that the strong concentration
dependence was not a transient phenomenon limited to a short reaction time. The findings of this study were rationalized using
the Cu-Ni-Sn isotherm. This study shows that precise control over the Cu concentration in solders is needed to produce consistent
results. 相似文献
123.
124.
V. V. Tcherdyntsev S. D. Kaloshkin A. I. Salimon E. A. Leonova I. A. Tomilin J. Eckert F. Schurack V. D. Rogozin S. P. Pisarev Yu. P. Trykov 《Materials and Manufacturing Processes》2002,17(6):825-841
Al-Cu-Fe alloys were prepared from elemental powders in a high-energy planetary ball mill. A sequence of solid state reactions resulting in quasicrystal (QC) phase formation takes place during heating of the as-milled powder. These reactions were studied by both differential scanning calorimetry and x-ray diffraction methods. Mechanically alloyed powders were consolidated by cold and hot pressing, as well as by explosive compaction. After annealing at sufficiently high temperatures, the consolidated samples are single-phase QC, except the ones consolidated by explosion. The high reactivity of the as-milled alloys causes the appearance of high porosity of the consolidated samples after the annealing. 相似文献
125.
以花岗岩类的硬质岩作为建筑物基础持力层,具有承载力高、稳定性好,抗震性强的特点,被许多重要建筑物所采用,尤其是沿海地区的高层建筑物。但往往此类基岩的层面不够“平整”,基岩层面的变化对基础的设计、施工,尤其是桩基础影响很大。本文通过对某高层建筑进行地基勘察的实例,总结了花岗岩地区风化岩层的几个特征及其在工程勘察中需注意的一些问题。 相似文献
126.
We present the design and realization of cylindrical dielectric resonators operating in the 40–60 GHz frequency range, designed
for the measurement of the surface resistance and of the surface reactance shift in High-T
c Superconductors (HTS) thin films in a dc magnetic field. The resonators are single tone, based on the TE
011 mode, and multiple tone, the latter allowing in principle to exploit the simultaneous determination of the surface impedance
at different frequencies. As an application example, we report the temperature and field dependencies of the effective surface
impedance of some cuprate superconductors thin films. The results are compared with those obtained through the use of a standard
metal cavity with a similar Q-factor and operating in the same frequency range. The comparison highlights a superior stability and a higher sensitivity,
resulting in an increase of about two orders of magnitude in the resolution of the surface impedance measurement. By contrast,
the dissipative part of the superconducting transition (above T/T
c = 0.97) is better studied with the metal cavity. We also present measurements in the vortex state in YBaCa2Cu3O7−δ and Tl2Ba2CaCu2O8+x
that show significantly different physics.
PACS: 74.25 Nf. 相似文献
127.
NiTi形状记忆合金激光气体氮化层表面特征 总被引:2,自引:0,他引:2
为改善NiTi合金的表面性能,利用2kW连续波Nd:YAG对NiTi合金进行激光气体氮化处理。采用SEM、TEM、XRD、XPS和纳米压痕研究了氮化层的显微组织及表面特征.结果表明:激光气体氮化可以在NiTi合金表面制备连续、无裂纹、厚度为2μm的TiN表面层,该表面层中基本不合有Ni元素且具有很高的硬度,其纳米压痕硬度为29.28GPa. 相似文献
128.
Magnesiumandmagnesiumalloyshavebeenin vestigatedashydrogenstoragematerialsforseveralde cadesbecausefarmorehydrogenbyweightcanbestoredinthemthaninmostoftheothercurrentlyknownhydrogenstoragealloys .Moreover ,thehighnaturalabundanceofMg ,itslightmassandenviron mentalcompatibilitypotentiallymakemagnesiumoneofthemostprospectivecandidatesforfuturehydrogenstoragematerials .Unfortunately ,thepracticalappli cationofMganditsalloyshasbeenlimitedonlytocertainstoragedevicebecauseoftheirpoorhydriding dehydr… 相似文献
129.
130.
吴桂金 《河南机电高等专科学校学报》2004,12(5):64-65
由于过烧石灰的存在和消解不当等原因,造成消石灰安定性不合格,当石灰稳定类路面结构成型或投入使用后,消石灰中的生石灰颗粒开始吸收周围水分,慢慢消解,消解过程中发生体积膨胀,对路面产生破坏。解决石灰安定性问题对防止公路前修后坏,延长路面使用寿命具有积极的现实意义。 相似文献