Dielectric Resonators for the Measurement of Superconductor Thin Films Surface Impedance in Magnetic Fields at High Microwave Frequencies

We present the design and realization of cylindrical dielectric resonators operating in the 40–60 GHz frequency range, designed for the measurement of the surface resistance and of the surface reactance shift in High-T _c Superconductors (HTS) thin films in a dc magnetic field. The resonators are single tone, based on the TE ₀₁₁ mode, and multiple tone, the latter allowing in principle to exploit the simultaneous determination of the surface impedance at different frequencies. As an application example, we report the temperature and field dependencies of the effective surface impedance of some cuprate superconductors thin films. The results are compared with those obtained through the use of a standard metal cavity with a similar Q-factor and operating in the same frequency range. The comparison highlights a superior stability and a higher sensitivity, resulting in an increase of about two orders of magnitude in the resolution of the surface impedance measurement. By contrast, the dissipative part of the superconducting transition (above T/T _c = 0.97) is better studied with the metal cavity. We also present measurements in the vortex state in YBaCa₂Cu₃O_7−δ and Tl₂Ba₂CaCu₂O_8+x that show significantly different physics. PACS: 74.25 Nf.     

NiTi形状记忆合金激光气体氮化层表面特征

为改善NiTi合金的表面性能，利用2kW连续波Nd：YAG对NiTi合金进行激光气体氮化处理。采用SEM、TEM、XRD、XPS和纳米压痕研究了氮化层的显微组织及表面特征．结果表明：激光气体氮化可以在NiTi合金表面制备连续、无裂纹、厚度为2μm的TiN表面层，该表面层中基本不合有Ni元素且具有很高的硬度，其纳米压痕硬度为29．28GPa．     

试论安定性不合格消石灰对柔性路面质量的影响

由于过烧石灰的存在和消解不当等原因，造成消石灰安定性不合格，当石灰稳定类路面结构成型或投入使用后，消石灰中的生石灰颗粒开始吸收周围水分，慢慢消解，消解过程中发生体积膨胀，对路面产生破坏。解决石灰安定性问题对防止公路前修后坏，延长路面使用寿命具有积极的现实意义。     

Preparation of Compound Ultrafine CeO2 by Wet-Solid-Phase Mechanochemical Modification

To satisfy practical requirements from industrial applications, an alternate route for synthesis compound ultrafine CeO2 powders by wet-solid-phase mechanochemical modification using industrial grade hydrated cerium carbonate as raw material was proposed.The effect of modifier reaction percentage, reaction time, calcining temperature and modifier amount on particle size, density, suspensibility, and hardness of compound CeO2 powder was investigated.The phase evolutions of preparation process were characterized by XRD.SEM micrograph of the final product shows that compound CeO2 powders obtained are well-dispersed, spherically-shaped, uniformly-sized and submicron-sized particles.The method is readily available in raw material, low in cost, simple in process, and has great potential for industrialization.The compound CeO2 powders of different physical properties can be synthesized by controlling the above-mentioned influence factors in preparation process.     

催化裂化装置结焦问题的探讨

针对中国石化股份公司所属56套催化裂化装置近两年半以来由于结焦造成非计划停工的原因，进行分析、探讨并提出了解决办法。指出催化裂化装置的结焦虽然是不可避免的、但通过采取有效措施，可以把结焦对装置安全生产的危害降低到最小程度。     

大规格圆钢质量分析和控制

针对湘钢棒材厂生产大规格圆钢出现的表面质量问题，重点介绍了在成品轧机后采用U形辊道和立活套替换棍道；冷床输入辊道采用镶WT合金套；增设高压水除鳞装置；中间轧件尺寸精度控制等措施，成功的解决了大规格圆钢表面擦伤、“麻面”、尺寸超差等表面质量问题，产品质量显著提高。     

Effect of RE－Al－N on Structures and Properties of M2 Cast High Speed Steel

M 2highspeedsteel (M 2steel)isamaterialwidelyusedintoolsanddies[1,2 ] .M 2steelischarac terizedbyalongsolidificationrangeandcomplexeu tecticreactions ,whichresultsinsegregationofalloy ingelementsandformationofseveraldifferenttypesofcarbidesduringsolidification[3,4 ] .Forconventionallyprocessedhigh speedsteels ,itisinevitablethatacoarsecarbidenetworkwillbeformedduringsolidifi cation .Coarseprimarycarbidestendtoresultinun evencarbidebandsdistributionafterasubstantialamountofhotprocessing[5] .Ma…     

套管钻井用套管外表面磨损后剩余强度分析

在分析讨论套管钻井管柱磨损形态的基础上,结合API5C5实物试验尺寸要求,通过有限元计算分析方法,对钻井套管完钻后含有外表面磨损缺陷的套管柱的极限剩余抗挤强度和极限剩余抗拉强度进行了研究,分别获得了均匀磨损和偏磨条件下,套管钻井套管柱外表面磨损缺陷的临界长度尺寸数值,以及不同破坏失效准则条件下的剩余抗挤强度和剩余抗拉强度的计算方程,为套管钻井中套管柱的设计、计算奠定了理论基础。     

锆酸铅薄膜的生长特性与表面化学态

以醋酸铅和异丙醇锆为原料，乙二醇甲醚为溶剂。通过溶胶-凝胶法和快速退火工艺在Pt(111)／Ti／SiO2／Si(100)基片成功地制备出不开裂的钙钛矿PbZrO3薄膜。用XRD和原子力显微镜测量了薄膜随退火温度变化的结构和表面形貌特征，用XPS测试了650℃退火PbZrO3薄膜的表面化学态。