无水乙醇生产工艺的探讨

分子筛固定床吸附法生产无水乙醇,工艺简单可靠,产品质量优,是一种环保、节能型工艺。     

油纸屏障对变压器局部放电超高频检测信号的影响

受变压器内部复杂结构的影响,局部放电超高频信号在变压器内部的传播特性非常复杂。笔者通过变压器局部放电超高频实验研究,分析了油纸屏障对变压器局部放电被测超高频信号的影响。设计了油中气隙放电、油中沿面放电和油中电晕放电3种局部放电模型,在实验油箱中进行局部放电实验,采用超高频小环天线进行放电信号检测,在有无油纸屏障情况下获得了局部放电超高频信号实测数据,对所测局部放电超高频信号在时域和频域上进行了对比分析。结果表明,油纸屏障对超高频信号幅值衰减及信号功率谱有一定影响。     

Research Profiling of Nano-enchanced Molecular Imaging Technology

Molecular imaging, as an emerging technique in current medical diagnostics, therapy and biology science, has received more and more attention in academia, industry, as well as medical practices. And the applications of nanotechnology in this field stimulate its development. This paper explores the development of the basic research and applied research on nano-enhanced molecular imaging, and does the in-depth analysis by adopting the bibliometrics method. The results show that the US is the leader in this field, who has the absolute advantages. Germany, UK and France and Japan are the followed ones. The rapidly developing Asian countries , China and South Korea might become the potential competitors. Research network analysis draws the conclusion that the other countries and regions share the same research interests with the US. The US not only take the lead in the researching number, but also directing the future orientation of this field. However, the US has not much international collaboration. The collaboration within the country and regions show that collaboration in this field is limited to the regional adjacency. Disciplinary analysis reveals that the major subjects which relate intimately to the nano-enhanced molecular imaging are chemistry, biomedical science and material science.     

Effect of niobium on thermal stability and impact toughness of Nd-Fe-B magnets with ultra-high intrinsic coercivity

The effects of Nb on the thermal stability and impact toughness of ultra-high intrinsic coercivity of Nd-Fe-B magnets were investigated.The results showed that the addition of Nb could improve the thermal stability,and obviously increased the impact toughness of sintered Nd-Fe-B magnets.The optimum thermal stability of sintered Nd-Fe-B magnets was obtained when the content of Nb was 1.0 at.%.The maximum impact toughness of sintered Nd-Fe-B magnets was obtained when the content of Nb was 1.5 at.%,but the magnetic properties of sintered Nd-Fe-B magnets drastically deteriorated when the content of Nb increased from 1.0 at.% to 1.5 at.%.The microstructure showed that overfull Nb addition made many ultra-fine grains get together,which led to the density of sintered Nd-Fe-B magnets decline and drastically deteriorated the magnetic properties of sintered Nd-Fe-B magnets.     

铁尾矿为原料微波法制备介孔分子筛

以鞍山铁尾矿为硅源,CTAB为模板剂,采用微波辐照法合成出全硅介孔分子筛MCM-41。用N2低温吸附、FT-IR、XRD和TEM等表征手段考察了其比表面积、孔径分布、晶体形貌等特性。结果表明:微波辐射法合成的MCM-41分子筛诱导期极短,晶化速度很快,具有典型的按六方对称性排列的孔道结构,FT-IR证明了分子筛具有硅氧四面体骨架。     

电子衡器在中铝广西分公司矿山生产中的应用

电子衡器目前在国内工业企业中得到了广泛使用,文章从其原理出发,结合电子衡器在中国铝业广西分公司矿山部实际运行状况,阐述了该称重设备的使用与维护要领。     

Molecular dynamics simulations of the interaction between OH radicals in plasma with poly-β-1–6-N-acetylglucosamine

Cold atmospheric plasma shows a satisfactory ability to inactivate bacterial biofilms that are difficult to remove using conventional methods in some cases. However, the researches on the inactivation mechanism are not quite sufficient. Poly-β-1–6-N-acetylglucosamine (PNAG), which is one of the important components in some biofilms, was used as the research subject, and the related mechanism of action triggered by different concentrations of the OH in plasma was studied using reactive molecular dynamics simulations. The results showed that OH radicals could not only trigger the hydrogen abstraction reaction leading to cleavage of the PNAG molecular structure, but undergo an OH addition reaction with PNAG molecules. New reaction pathways appeared in the simulations as the OH concentration increased, but the reaction efficiency first increased and then decreased. The simulation study in this paper could, to some extent, help elucidate the microscopic mechanism of the interaction between OH radicals in plasma and bacterial biofilms at the atomic level.     

基于非截断小波有限元的BLT正向问题研究

针对自发荧光断层成像,提出了一种非截断小波有限元算法.该算法采用单元间非截断组合小波基来逼近未知函数,从理论上解决了二维和三维下复杂形状体的剖分,并成功地应用于自发荧光断层成像正向问题中圆柱和圆球仿体的研究.理论分析和数值仿真结果表明,与传统有限元的数值解相比,该算法在获得同样有效解的情况下减少了单元剖分数,降低了计算的复杂度.     

NKChemSQL——针对MySQL的化学信息学扩展

化学数据库是进行化学信息学研究的重要资源,分子属性与指纹计算、分子结构格式转换、分子相似度匹配、精确匹配和子结构匹配以及分子结构图片导出等,都是必需的基本服务内容。应用广泛的数据库系统MySQL却缺乏这些功能,难以满足化学信息处理、网站开发等开发的需求。NKChemSQL是自行编制的MySQL扩展库,通过对开源软件OpenBabel的功能进行包装,以SQL语言的格式完成相应操作。NKChemSQL具有良好的运行表现,经过对含26万余条分子结构信息的NCI数据库进行的测试,全结构匹配只需不到1秒而子结构匹配达300个结构/秒,相似度匹配则达1万个结构/秒。NKChemSQL为开发化学信息学软件和网站提供了非常便利的新方式。     

Effect of postmolding heat treatment on in vitro properties of a polyanhydride implant containing gentamicin sulfate

A polyanhydride implant containing gentamicin sulfate was fabricated using a laboratory-scale injection-molding machine. After injection molding, the implants were subject to heat treatment at 60°C for various time periods with or without nitrogen protection. The impact of this heat treatment on the in vitro properties of the implants including copolymer molecular weights, mechanical properties, and in vitro drug-release profiles was investigated. This heat treatment caused a drastic drop in the molecular weight of the copolymer. Heating without nitrogen protection resulted in the hardening of the implant, but heating in the presence of nitrogen rendered the implant less rigid. It was also found that a faster in vitro drug release profile was shown by implants heated without nitrogen protection and a pronounced slowing down in drug release was exhibited by implants heated with nitrogen protection.